CN103482692B - 以TiOSO4和沥青分别为钛源和碳源制备TiCN粉体的方法 - Google Patents
以TiOSO4和沥青分别为钛源和碳源制备TiCN粉体的方法 Download PDFInfo
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- CN103482692B CN103482692B CN201310449156.3A CN201310449156A CN103482692B CN 103482692 B CN103482692 B CN 103482692B CN 201310449156 A CN201310449156 A CN 201310449156A CN 103482692 B CN103482692 B CN 103482692B
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- 239000000843 powder Substances 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims abstract description 23
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title abstract description 14
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract description 12
- 239000010936 titanium Substances 0.000 title abstract description 12
- 229910052719 titanium Inorganic materials 0.000 title abstract description 12
- 229910052799 carbon Inorganic materials 0.000 title abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 238000002360 preparation method Methods 0.000 claims abstract description 10
- 238000005516 engineering process Methods 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000012298 atmosphere Substances 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000007864 aqueous solution Substances 0.000 claims abstract description 4
- 239000013064 chemical raw material Substances 0.000 claims abstract description 4
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 4
- 229960000935 dehydrated alcohol Drugs 0.000 claims abstract description 4
- 239000008367 deionised water Substances 0.000 claims abstract description 4
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 4
- 239000004615 ingredient Substances 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 claims abstract description 4
- 239000012299 nitrogen atmosphere Substances 0.000 claims abstract description 4
- 239000000243 solution Substances 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 3
- 238000004090 dissolution Methods 0.000 claims abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract description 3
- 238000003786 synthesis reaction Methods 0.000 abstract description 3
- 239000011295 pitch Substances 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 229910010413 TiO 2 Inorganic materials 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 150000003609 titanium compounds Chemical class 0.000 description 1
Abstract
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CN201310449156.3A CN103482692B (zh) | 2013-09-27 | 2013-09-27 | 以TiOSO4和沥青分别为钛源和碳源制备TiCN粉体的方法 |
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CN201310449156.3A CN103482692B (zh) | 2013-09-27 | 2013-09-27 | 以TiOSO4和沥青分别为钛源和碳源制备TiCN粉体的方法 |
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CN103482692A CN103482692A (zh) | 2014-01-01 |
CN103482692B true CN103482692B (zh) | 2015-09-23 |
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3661524A (en) * | 1970-04-14 | 1972-05-09 | Ppg Industries Inc | Preparation of titanium carbide |
CN101486462A (zh) * | 2009-02-23 | 2009-07-22 | 潍坊学院 | 一种碳化钛微粉的制备方法 |
CN103274409A (zh) * | 2013-06-01 | 2013-09-04 | 桂林理工大学 | 以TiOSO4和酚醛树脂分别为钛源和碳源制备超细TiC粉体的方法 |
-
2013
- 2013-09-27 CN CN201310449156.3A patent/CN103482692B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3661524A (en) * | 1970-04-14 | 1972-05-09 | Ppg Industries Inc | Preparation of titanium carbide |
CN101486462A (zh) * | 2009-02-23 | 2009-07-22 | 潍坊学院 | 一种碳化钛微粉的制备方法 |
CN103274409A (zh) * | 2013-06-01 | 2013-09-04 | 桂林理工大学 | 以TiOSO4和酚醛树脂分别为钛源和碳源制备超细TiC粉体的方法 |
Non-Patent Citations (2)
Title |
---|
以酚醛树脂为碳源碳热还原制备TiC 的研究;李鹏飞等;《硅酸盐通报》;20121031;全文 * |
高钛渣提取碳氮化钛的研究;李慈颖等;《钢铁钒钛》;20060930;第7页右栏第2段以及第2.2节 * |
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Effective date of registration: 20240424 Address after: 541199 Baoshan High end Equipment Intelligent Manufacturing Industrial Park (Phase I), Lingui District, Guilin City, Guangxi Zhuang Autonomous Region Plant 1 and 2 Patentee after: GUILIN GUIYE HEAVY INDUSTRIES CO.,LTD. Country or region after: China Address before: 541006 Yanshan Street 319, Yanshan District, Guilin, the Guangxi Zhuang Autonomous Region, Guilin University of Technology (Yanshan campus) Patentee before: GUILIN University OF TECHNOLOGY Country or region before: China |