CN103478254A - High-calcium milk as well as raw material composition and preparation method thereof - Google Patents
High-calcium milk as well as raw material composition and preparation method thereof Download PDFInfo
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Abstract
The invention discloses high-calcium milk as well as a raw material composition and a preparation method thereof. The preparation method comprises the following steps of (1) dissolving an annion calcic compound, emulsifying salt and an emulsifier into drinking water so as to obtain a reaction liquid, wherein the temperature of the reaction liquid is 40-55 DEG C; (2) raising the temperature of the milk to be 40-55 DEG C, uniformly adding the reaction liquid prepared in the step (1) into the milk, and stirring for 5-15 minutes; (3) evaporating the moisture, wherein the mass of the moisture is equal to the amount of the drinking water in the step (1); and (4) homogenizing, sterilizing and cooling so as to obtain the high-calcium milk. The high-calcium milk disclosed by the invention is good in stability, free of protein flocculation and free of protein scaling phenomenon after being produced and boiled.
Description
Technical field
The present invention relates to a kind of high calcium milk and feedstock composition thereof and preparation method.
Background technology
Calcium is one of most important mineral element in human body, and wherein 99% calcium is present in bone and tooth, and all the other 1% are present in soft tissue and body fluid.When human calcium's intake is not enough, can cause various diseases, also can affect health when serious.According to investigations, in the daily meals of China resident, the content of calcium only reaches half of recommended amounts, the general calcium deficiency of all kinds of crowds.The expert points out, by adjustment of diet, particularly by dairy produce, supplementing calcium content is a good approach.Therefore, in milk, strengthening calcium is a kind of effective way that solves the calcium intake deficiency.
At present, stipulate the compound source for the Calcium In Food strengthening in national standard, wherein be no lack of the ionic calcium containing compound of some common solubilities as the calcium source.BIOLOGICAL CALCIUM source and organic calcium source are compared in these ionic calcium sources, and low price and calcium content are high, in milk, can not precipitate, and can not increase human liver kidney burden, are easy to absorb.But the introducing in ionic calcium source can destroy the rock-steady structure of original protein, generate calcium caseinate, make product flocculation occur; Even condense without obvious albumen, the product heating albumen fouling occurs by the chamber wall of being everlasting, and makes production equipment clean difficulty, and loss is large.Therefore, produce stable ionic calcium source dairy products, universal significant for the high calcium dairy products.
Summary of the invention
Technical problem to be solved by this invention is to overcome ionic high calcium dairy products of the prior art to be prone to protein flocculation and fouling, the poor defect of product stability, and high calcium milk and feedstock composition and the preparation method that a kind of stability is strong is provided.
The invention provides a kind of feedstock composition of high calcium milk, it comprises following component: milk 99.3%～99.71%, ionic calcium containing compound 0.2%～0.45%, emulsification salt 0.07%～0.15%, emulsifying agent 0.02%～0.1%; Described emulsification salt is the mass ratio citrate that is (2:1)～(3:1) and the mixture of sodium phosphate trimer, or citrate; Described percentage is mass percent.
Wherein, the natural mammal gland secretion of forcing down from the normal breast of healthy ox body that described milk is this area routine, can be the whole milk and process fats portion or whole low fat or skim milk separated separated without fat.
Wherein, described ionic calcium containing compound be this area routine soluble, take the compound of ionic calcium as the calcium source, preferably for regulation in GB GB14880 " food enrichment Application standard " be allowed for modulating one or more in newborn calcium lactate, Pfansteihl calcium and calcium monohydrogen phosphate, be more preferably calcium lactate.The consumption of described ionic calcium containing compound is preferably 0.24%～0.36%.
Wherein, the consumption of described emulsification salt is preferably 0.08%～0.12%.
Wherein, described citrate is this area routine, is preferably natrium citricum and/or potassium citrate.When mixture that described emulsification salt is citrate and sodium phosphate trimer, the mass ratio of described citrate and sodium phosphate trimer is preferably 2:1.
Wherein, described emulsifying agent is this area routine, is preferably single, one or more in diglycerine fatty acid ester, sucrose fatty ester and phosphatide.
The present invention also provides and has adopted the aforementioned base materials composition to prepare the preparation method of high calcium milk, and it comprises the steps:
(1) by ionic calcium containing compound, emulsification salt and emulsifiers dissolve in drinking water, obtain reactant liquor; The temperature of described reactant liquor is 40 ℃～55 ℃;
(2) milk is warming up to 40 ℃～55 ℃, the reactant liquor of step (1) gained is evenly added in milk, stir 5min～15min;
(3) transpiring moisture; The consumption that the quality of described moisture is drinking water in step (1);
(4) homogeneous, sterilization, cooling, get final product.
The mode of operation that the mode of operation of described step (1) is this area routine is preferably mode one: in the drinking water by ionic calcium containing compound, emulsification salt and emulsifiers dissolve after heating, the more cooling reactant liquor that obtains; Or mode two: ionic calcium containing compound, emulsification salt and emulsifying agent are placed in to drinking water, heating for dissolving, the more cooling reactant liquor that obtains.Heating described in mode one and mode two is preferably for being heated to more than 60 ℃, more preferably for being heated to more than 80 ℃.Especially emulsification salt and ionic calcium containing compound are dissolved in the water of higher temperature fully in the present invention, make calcium ion in the ionic calcium containing compound and the anion combination in advance in emulsification salt, prevent that casein in calcium ion and milk is in conjunction with producing flocculation.
In step (1), described drinking water is for meeting the water of GB5749-2006 " drinking water sanitary standard ".
In step (2), described milk before intensification according to this area routine, generally need through standardization, described standardization refers to the index stable and consistent such as protein in order to guarantee each batch of product, fat, in the scope allowed at alimentary codex, index adjusted such as protein, fat are reached to the indices scope of described raw milk: protein content >=2.9wt%, fat content >=3.1wt% and non-fat solid content >=8.1wt%, can or remove a certain material by extra interpolation, or concentrate or dilute the animal breast and carry out.
In step (2), described intensification is preferably for being warming up to 45 ℃～50 ℃.Milk temperature when control adds batching, to guarantee that neither activating unnecessary calcium ion can make again milk and reactant liquor fully mix.
In step (2), the described mode evenly added is this area routine, preferably for spray, adds.The speed that described spray adds is preferably≤5m/s.
In step (2), the time of described stirring is this area routine, is preferably 10min.
In step (3), described transpiring moisture be operating as this area routine techniques, be preferably that flash concentration and/or falling liquid film are concentrated.The quality of described transpiring moisture is for the consumption of the drinking water of dissolved ions type calcium containing compound, emulsification salt and emulsifying agent in step (1).
In step (4), described homogeneous is this area routine operation, and the temperature of described homogeneous is preferably 65 ℃～75 ℃, and the pressure of described homogeneous is preferably 18Mpa～20Mpa.
In step (4), described sterilization is this area routine operation, is preferably pasteurize and/or UHTS.Described pasteurize is this area routine operation, is preferably sterilization 15s～30s under 70 ℃～85 ℃ conditions, is more preferably 85 ℃ of lower sterilization 15s.Described UHTS is this area routine operation, is preferably sterilization 3s～6s under 130 ℃～137 ℃ conditions, is more preferably 137 ℃ of lower sterilization 4s.
In step (4), described this area routine operation that is cooled to, described cooling temperature is preferably below 7 ℃, is more preferably 2 ℃～6 ℃.
In step (1), described dissolving is preferably for continuing stirring and dissolving.
In step (4), after the high calcium milk made is carried out to cooling processing, also need to high calcium milk, carry out filling according to conventional method.
The present invention also provides the high calcium milk that adopts above-mentioned preparation method to make.
On the basis that meets this area general knowledge, above-mentioned each optimum condition, but any combination obtains the preferred embodiments of the invention.
Agents useful for same of the present invention and raw material be commercially available obtaining all.
Positive progressive effect of the present invention is:
That the present invention uses is cheap, solubility, the good ionic calcium containing compound absorbed be as the calcium source, for the calcium source of high calcium milk has increased a kind of selection.The high calcium milk product stability made is good, without the albumen flocculation, produces and boils rear all without the albumen scale formation.Simultaneously, preparation method of the present invention solved in high calcium milk production equipment pipeline the albumen fouling serious, clean difficulty and the large problem of loss.
The specific embodiment
Mode below by embodiment further illustrates the present invention, but does not therefore limit the present invention among described scope of embodiments.The experimental technique of unreceipted actual conditions in the following example, according to conventional method and condition, or select according to catalogue.
In following embodiment, raw materials used source is: milk: Shanghai Bright Dairy & Food Co., Ltd.'s dairy products two factories; All the other batchings: upper sea blue island food additives company.
In following embodiment, if no special instructions, described percentage is mass percent.
Embodiment 1
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 1.
The feedstock composition of the high calcium milk of table 1 embodiment 1
| Composition | Consumption (%) |
| Milk | 99.3 |
| Calcium lactate | 0.45 |
| Natrium citricum | 0.1 |
| Sodium phosphate trimer | 0.05 |
| Single, diglycerine fatty acid ester | 0.1 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 85 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 45 ℃;
(2) milk is warming up to 45 ℃, the solution spraying of step (1) gained is added to rear stirring 10min;
(3) flash method evaporates the moisture that dissolves batching in step (1);
(4) be warming up to 65 ℃, the 20MPa homogeneous, 85 ℃, 15s pasteurize, be cooled to 2 ℃～6 ℃, filling, gets final product.
Embodiment 2
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 2.
The feedstock composition of the high calcium milk of table 2 embodiment 2
| Composition | Consumption (%) |
| Milk | 99.58 |
| Pfansteihl calcium | 0.3 |
| Natrium citricum | 0.08 |
| Single, diglycerine fatty acid ester | 0.04 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 80 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 50 ℃;
(2) milk is warming up to 50 ℃, the solution spraying of step (1) gained is added to rear stirring 15min;
(3) flash method evaporates the moisture that dissolves batching in step (1);
(4) be warming up to 75 ℃, the 18MPa homogeneous, 75 ℃, 15s pasteurize, be cooled to 2 ℃～6 ℃, filling, gets final product.
Embodiment 3
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 3.
The feedstock composition of the high calcium milk of table 3 embodiment 3
| Composition | Consumption (%) |
| Milk | 99.44 |
| Calcium lactate | 0.4 |
| Natrium citricum | 0.08 |
| Potassium citrate | 0.04 |
| Single, diglycerine fatty acid ester | 0.02 |
| Sucrose fatty ester | 0.02 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 80 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 50 ℃;
(2) milk is warming up to 50 ℃, the solution spraying of step (1) gained is added to rear stirring 10min;
(3) the falling liquid film concentration method is removed the moisture that dissolves batching in step (1);
(4) be warming up to 75 ℃, the 18MPa homogeneous, 130 ℃, 4s UHTS, be cooled to 2 ℃～6 ℃, filling, gets final product.
Embodiment 4
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 4.
The feedstock composition of the high calcium milk of table 4 embodiment 4
| Composition | Consumption (%) |
| Milk | 99.71 |
| Calcium lactate | 0.2 |
| Natrium citricum | 0.07 |
| Single, diglycerine fatty acid ester | 0.02 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 60 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 55 ℃;
(2) milk is warming up to 55 ℃, stirs the solution that slowly adds step (1) gained simultaneously, stir afterwards 15min;
(3) flash method evaporates the moisture that dissolves batching in step (1);
(4) be warming up to 65 ℃, the 20MPa homogeneous, 137 ℃, 4s ultra high temperature sterilization, be cooled to 2 ℃～6 ℃, filling, gets final product.
Embodiment 5
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 5.
The feedstock composition of the high calcium milk of table 5 embodiment 5
| Composition | Consumption (%) |
| Milk | 99.49 |
| Calcium lactate | 0.36 |
| Natrium citricum | 0.08 |
| Sodium phosphate trimer | 0.04 |
| Single, diglycerine fatty acid ester | 0.02 |
| Sucrose fatty ester | 0.01 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 90 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 40 ℃;
(2) milk is warming up to 40 ℃, the solution spraying of step (1) gained is added to rear stirring 5min;
(3) flash method evaporates the moisture that dissolves batching in step (1);
(4) be warming up to 75 ℃, the 20MPa homogeneous, 85 ℃, 15s pasteurize, be cooled to 2 ℃～6 ℃, filling, gets final product.
Embodiment 6
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 6.
The feedstock composition of the high calcium milk of table 6 embodiment 6
| Composition | Consumption (%) |
| Milk | 99.3 |
| Calcium lactate | 0.4 |
| Natrium citricum | 0.15 |
| Sodium phosphate trimer | 0.05 |
| Single, diglycerine fatty acid ester | 0.1 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 80 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 40 ℃;
(2) milk is warming up to 40 ℃, the solution spraying of step (1) gained is added to rear stirring 10min;
(3) flash method evaporates the moisture that dissolves batching in step (1);
(4) be warming up to 65 ℃, the 20MPa homogeneous, 85 ℃, 15s pasteurize, be cooled to 2 ℃～6 ℃, filling, gets final product.
Effect embodiment 1
The high calcium milk that embodiment 1～6 is obtained carries out the calcium content test, and method of testing is with reference to the atomic absorption spectrophotometry in GB GB5413.21-2010 " mensuration of calcium, iron, zinc, sodium, potassium, magnesium, copper and manganese in food security national standard-infant food and dairy products ".
Test result shows, the calcium content of high calcium milk of the present invention reaches 120mg/100mL～150mg/100mL, is more than or equal to the high calcium for milk in GB GB28050-2011 and requires: every 100mL milk can meet 15%～19% of human body calcium every day demand.And technique of the present invention and formula, product in process of production without albumen flocculation, without particle, sticky wall or plugging phenomenon; Product is stable in the shelf-life internal state, without the albumen flocculation, boils afterwards without the albumen fouling, and mouthfeel is fine and smooth.
Comparative Examples 1
This Comparative Examples will have high calcium milk now, and (Shanghai Bright Dairy & Food Co., Ltd. produces, the calcium source of this high calcium milk is newborn mineral salt) carry out Performance Ratio with the high calcium milk of embodiments of the invention 1, test item comprises in production process that deposit-free, product sensory are arranged at the pill tank bottom, the end of term packing of product bottom of guaranteeing the quality has or not precipitation, and adding heat endurance, result is as shown in table 7.
The performance comparison result of the high calcium milk of the existing high calcium milk of table 7 and embodiment 1
Visible, high calcium milk provided by the invention is compared with existing high calcium milk, and mouthfeel is better, in stability, be significantly increased on the storage life.
Comparative Examples 2
The feedstock composition of the high calcium milk of this Comparative Examples is as shown in table 8.
The feedstock composition of the high calcium milk of table 8 Comparative Examples 2
| Composition | Consumption (%) |
| Milk | 99.71 |
| Calcium lactate | 0.2 |
| Natrium citricum | 0.07 |
| Single, diglycerine fatty acid ester | 0.02 |
The preparation method of the high calcium milk of this Comparative Examples comprises following processing step:
(1) a certain amount of drinking water is heated to 60 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 55 ℃;
(2) milk is warming up to 65 ℃, stirs, slowly add the solution of step (1) gained, then stir 15min, find the albumen precipitation thing to occur at the bottom of pill tank simultaneously;
(3) flash method evaporates the moisture that dissolves batching in step (1);
(4) be warming up to 65 ℃, the 20MPa homogeneous, 85 ℃, 15s pasteurize, for the filter pipe obstruction of bar sterilization, high calcium milk can't carry out sterilization smoothly.
Comparative Examples 3
The feedstock composition of the high calcium milk of this Comparative Examples is as shown in table 9.
The feedstock composition of the high calcium milk of table 9 Comparative Examples 3
| Composition | Consumption (%) |
| Milk | 99.71 |
| Calcium lactate | 0.2 |
| Natrium citricum | 0.07 |
| Single, diglycerine fatty acid ester | 0.02 |
The preparation method of the high calcium milk of this Comparative Examples comprises following processing step:
(1) a certain amount of drinking water is heated to 60 ℃, adds all the other batchings except milk in above-mentioned formula, be stirred to abundant dissolving, be cooled to 55 ℃;
(2) milk is warming up to 4 ℃, stirs the solution that slowly adds step (1) gained simultaneously, stir afterwards 15min;
(3) flash method evaporates the moisture that dissolves batching in step (1);
(4) be warming up to 65 ℃, the 20MPa homogeneous, 85 ℃, 15s pasteurize, be cooled to 2～6 ℃, filling, gets final product.
Finished product is poured in beaker, beaker bottom is warming up to product boiling in cup, find that there is the sticky end phenomenon and occur.And the product of embodiment 1 is while carrying out boiling test, result is good, without the sticky end phenomenon.
Claims (10)
1. the feedstock composition of a high calcium milk, is characterized in that, it comprises following component: milk 99.3%～99.71%, ionic calcium containing compound 0.2%～0.45%, emulsification salt 0.07%～0.15%, emulsifying agent 0.02%～0.1%; Described emulsification salt is the mass ratio citrate that is (2:1)～(3:1) and the mixture of sodium phosphate trimer, or citrate; Described percentage is mass percent.
2. the feedstock composition of high calcium milk as claimed in claim 1, is characterized in that, described ionic calcium containing compound be calcium lactate, Pfansteihl calcium or and calcium monohydrogen phosphate in one kind of multiple; The consumption of described ionic calcium containing compound is 0.24%～0.36%.
3. the feedstock composition of high calcium milk as claimed in claim 1, is characterized in that, the consumption of described emulsification salt is 0.08%～0.12%; Described citrate is natrium citricum and/or potassium citrate; When mixture that described emulsification salt is citrate and sodium phosphate trimer, the mass ratio of described citrate and sodium phosphate trimer is 2:1.
4. the feedstock composition of high calcium milk as claimed in claim 1, is characterized in that, described emulsifying agent is single, one or more in diglycerine fatty acid ester, sucrose fatty ester and phosphatide.
5. an employing feedstock composition as described as claim 1～4 any one prepares the preparation method of high calcium milk, it is characterized in that, described preparation method comprises the steps:
(1) by ionic calcium containing compound, emulsification salt and emulsifiers dissolve in drinking water, obtain reactant liquor; The temperature of described reactant liquor is 40 ℃～55 ℃;
(2) milk is warming up to 40 ℃～55 ℃, the reactant liquor of step (1) gained is evenly added in milk, stir 5min～15min;
(3) transpiring moisture; The consumption that the quality of described moisture is drinking water in step (1);
(4) homogeneous, sterilization, cooling, get final product.
6. preparation method as claimed in claim 5, it is characterized in that, the mode of operation that the mode of operation of described step (1) is this area routine is preferably mode one: in the drinking water by ionic calcium containing compound, emulsification salt and emulsifiers dissolve after heating, the more cooling reactant liquor that obtains; Or mode two: ionic calcium containing compound, emulsification salt and emulsifying agent are placed in to drinking water, heating for dissolving, the more cooling reactant liquor that obtains; Wherein, described heating is preferably for being heated to more than 60 ℃, more preferably for being heated to more than 80 ℃.
7. preparation method as claimed in claim 5, is characterized in that, in step (2), described intensification is for being warming up to 45 ℃～50 ℃; The described mode evenly added adds for spray; The speed that described spray adds is preferably≤5m/s; The time of described stirring is 10min.
8. preparation method as claimed in claim 5, is characterized in that, in step (3), described transpiring moisture to be operating as flash concentration and/or falling liquid film concentrated.
9. preparation method as claimed in claim 5, is characterized in that, in step (4), the temperature of described homogeneous is 65 ℃～75 ℃, and the pressure of described homogeneous is 18Mpa～20Mpa; Described sterilization is pasteurize and/or UHTS; Described pasteurize is preferably sterilization 15s～30s under 70 ℃～85 ℃ conditions, is more preferably 85 ℃ of lower sterilization 15s; Described UHTS is preferably 130 ℃～137 ℃ lower sterilization 3s～6s, is more preferably 137 ℃ of lower sterilization 4s; Described being cooled to is cooled to 2 ℃～6 ℃.
10. the high calcium milk that preparation method as described as claim 5～9 any one makes.
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| CN105558043A (en) * | 2015-12-16 | 2016-05-11 | 光明乳业股份有限公司 | High-calcium milk and production method thereof |
| CN105767189A (en) * | 2016-03-09 | 2016-07-20 | 宁夏金树沅农贸有限公司 | Moringa oleifera high-calcium milk production and processing technology |
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| CN108208174A (en) * | 2016-12-22 | 2018-06-29 | 张影 | It is a kind of to have the fresh milk and dairy produce for improving pipe intestinal digesting function |
| CN112544772A (en) * | 2020-12-08 | 2021-03-26 | 光明乳业股份有限公司 | Raw material composition of calcium-fortified frozen beverage, calcium-fortified frozen beverage and preparation method of calcium-fortified frozen beverage |
| CN114600961A (en) * | 2022-03-10 | 2022-06-10 | 山东得益乳业股份有限公司 | High-calcium milk and preparation method thereof |
| CN115720933A (en) * | 2022-12-06 | 2023-03-03 | 光明乳业股份有限公司 | High-calcium milk containing probiotics and preparation method thereof |
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| CN108208174A (en) * | 2016-12-22 | 2018-06-29 | 张影 | It is a kind of to have the fresh milk and dairy produce for improving pipe intestinal digesting function |
| CN112544772A (en) * | 2020-12-08 | 2021-03-26 | 光明乳业股份有限公司 | Raw material composition of calcium-fortified frozen beverage, calcium-fortified frozen beverage and preparation method of calcium-fortified frozen beverage |
| CN114600961A (en) * | 2022-03-10 | 2022-06-10 | 山东得益乳业股份有限公司 | High-calcium milk and preparation method thereof |
| CN115720933A (en) * | 2022-12-06 | 2023-03-03 | 光明乳业股份有限公司 | High-calcium milk containing probiotics and preparation method thereof |
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