CN114600961A - High-calcium milk and preparation method thereof - Google Patents
High-calcium milk and preparation method thereof Download PDFInfo
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- CN114600961A CN114600961A CN202210228950.4A CN202210228950A CN114600961A CN 114600961 A CN114600961 A CN 114600961A CN 202210228950 A CN202210228950 A CN 202210228950A CN 114600961 A CN114600961 A CN 114600961A
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- Prior art keywords
- calcium
- milk
- soluble
- phosphate
- product
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- 239000011575 calcium Substances 0.000 title claims abstract description 66
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 66
- 235000013336 milk Nutrition 0.000 title claims abstract description 66
- 239000008267 milk Substances 0.000 title claims abstract description 66
- 210000004080 milk Anatomy 0.000 title claims abstract description 66
- 238000002360 preparation method Methods 0.000 title abstract description 17
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 34
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 14
- 159000000007 calcium salts Chemical class 0.000 claims abstract description 14
- 239000010452 phosphate Substances 0.000 claims abstract description 14
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 14
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000011574 phosphorus Substances 0.000 claims abstract description 6
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract description 6
- 239000004615 ingredient Substances 0.000 claims abstract description 4
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229960005069 calcium Drugs 0.000 claims description 60
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 12
- 230000001954 sterilising effect Effects 0.000 claims description 11
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 9
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical group [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims description 6
- 239000001527 calcium lactate Substances 0.000 claims description 6
- 229960002401 calcium lactate Drugs 0.000 claims description 6
- 235000011086 calcium lactate Nutrition 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 239000001488 sodium phosphate Substances 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 5
- 235000020247 cow milk Nutrition 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 4
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 4
- 229910000406 trisodium phosphate Inorganic materials 0.000 claims description 4
- 235000019801 trisodium phosphate Nutrition 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 3
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 3
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 3
- 230000007935 neutral effect Effects 0.000 claims description 2
- 238000005728 strengthening Methods 0.000 claims 1
- 235000013365 dairy product Nutrition 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 230000003014 reinforcing effect Effects 0.000 abstract description 3
- 239000000047 product Substances 0.000 description 33
- 239000000463 material Substances 0.000 description 10
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 238000011049 filling Methods 0.000 description 4
- 235000016709 nutrition Nutrition 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- 235000020185 raw untreated milk Nutrition 0.000 description 4
- 238000004659 sterilization and disinfection Methods 0.000 description 4
- 229910000019 calcium carbonate Inorganic materials 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 235000014048 cultured milk product Nutrition 0.000 description 2
- 206010006956 Calcium deficiency Diseases 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 102000014171 Milk Proteins Human genes 0.000 description 1
- 108010011756 Milk Proteins Proteins 0.000 description 1
- 239000006057 Non-nutritive feed additive Substances 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- 208000003217 Tetany Diseases 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 235000001465 calcium Nutrition 0.000 description 1
- 229940069978 calcium supplement Drugs 0.000 description 1
- 230000019771 cognition Effects 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 235000015140 cultured milk Nutrition 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 229910000397 disodium phosphate Inorganic materials 0.000 description 1
- 235000019800 disodium phosphate Nutrition 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 235000020774 essential nutrients Nutrition 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 235000021243 milk fat Nutrition 0.000 description 1
- 235000021239 milk protein Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 230000004118 muscle contraction Effects 0.000 description 1
- 206010029410 night sweats Diseases 0.000 description 1
- 230000036565 night sweats Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000003002 pH adjusting agent Substances 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 208000007442 rickets Diseases 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 235000008939 whole milk Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1522—Inorganic additives, e.g. minerals, trace elements; Chlorination or fluoridation of milk; Organic salts or complexes of metals other than natrium or kalium; Calcium enrichment of milk
Abstract
The invention relates to high-calcium milk and a preparation method thereof, belonging to the technical field of dairy product preparation. The high-calcium milk disclosed by the invention uses soluble phosphate and soluble calcium salt as reinforcing sources of calcium element and phosphorus element in product ingredients, and the calcium content is more than or equal to 170mg/100 g. The high-calcium milk provided by the invention has the advantages that the calcium content is obviously higher than the existing level, the product taste is excellent, an additional stable system is not used, the production cost is controllable, and the eating population is not limited; the invention also provides a simple and convenient preparation method, which is suitable for industrial application.
Description
Technical Field
The invention relates to high-calcium milk and a preparation method thereof, belonging to the technical field of dairy product preparation.
Background
In recent years, with the development of socioeconomic, the living standard of people is gradually improved, and the health cognition and the demand are gradually enhanced. The milk as a health food has comprehensive nutrition, natural raw materials and rich taste. The milk contains milk raw materials which have various nutritional functional components such as milk calcium, milk protein, milk fat and the like, and can be absorbed and utilized by human bodies to improve the health level of the human bodies.
Calcium is one of essential nutrients for human body, can control heart rate and blood pressure, and participates in muscular contraction. Calcium deficiency in human body may cause rickets, night sweat, tetany, osteoporosis, cardiovascular diseases, etc. According to investigation, Chinese people are generally lack of calcium, and the biggest concern about functions in dairy product consumption is calcium supplement.
At present, the calcium content of the common commercial high-calcium milk product per 100mL is more than 120-130mg, and the calcium content of the common milk is 100-110 mg. According to the national food nutrition label regulation, the high-calcium milk can be prepared as long as the calcium content of each 100mL of dairy product is higher than 120 mg. Many high calcium milk products have a calcium content that differs by less than 25% from normal whole milk. In addition, calcium carbonate is used in most of the commercially available high-calcium milk products, and the high-calcium technology is the same as that of the commercially available high-calcium milk products, and exogenous calcium is directly added. The product with calcium content higher than 130mg has common diseases with poor taste. The products using calcium carbonate as a calcium source are divided into two products, one product does not use an additional stabilizing system, and the products have serious calcium carbonate precipitation phenomenon; the product has less natural degree owing to more compounding material. In addition, in some products using milk calcium or milk mineral salts as calcium source, too high an amount of calcium source added will affect the ionization balance of the product, resulting in deterioration of the stability of the product.
Disclosure of Invention
The invention aims to provide the high-calcium milk, the calcium content of which is obviously higher than the existing level, the product has excellent taste, an additional stable system is not used, the production cost is controllable, and the eating population is not limited; the invention also provides a simple and convenient preparation method, which is suitable for industrial application.
The high-calcium milk disclosed by the invention uses soluble phosphate and soluble calcium salt as reinforcing sources of calcium element and phosphorus element in product ingredients, and the calcium content is more than or equal to 170mg/100 g.
Preferably, every 1kg of high-calcium milk comprises the following raw materials: 900g of fresh milk 950-one, 5-7g of soluble calcium salt, 0.5-2.0g of soluble phosphate and 0.1-0.5g of pH regulator.
Further preferably, the pH adjuster is sodium hydroxide or potassium hydroxide.
Preferably, the soluble calcium salt is calcium lactate.
Preferably, the soluble phosphate is one or more of trisodium phosphate, monosodium phosphate or disodium phosphate.
The preparation method of the high-calcium milk is based on the conventional processes of purifying milk, mixing, sterilizing, homogenizing and filling used in the preparation of the fermented milk, and the conventional processes of fine adjustment such as process addition or subtraction and the like on the basis. The key process is the use of soluble phosphate and soluble calcium salt as raw materials, namely, premixing the soluble phosphate and the soluble calcium salt in raw milk in a specific proportion, and adding sodium hydroxide and the like as processing aids for pH adjustment as required.
Preferably, the method comprises the following steps:
cleaning fresh cow milk, preheating, sequentially adding soluble calcium salt and soluble phosphate for blending, adjusting pH to neutral with pH regulator, homogenizing, sterilizing, cooling, bottling and storing.
Further preferably, the preheating temperature is 55-60 ℃.
Further preferably, the homogenization temperature is 55-60 ℃ and the pressure is 18-20 MPa.
Further preferably, the sterilization temperature is 80-140 ℃ and the time is 0.5-15 s.
Further preferably, the temperature is reduced to 2-6 ℃.
Further preferably, the warehousing storage temperature is 2-6 ℃.
According to the invention, only soluble phosphate and soluble calcium salt are used as reinforced calcium and phosphorus sources for the first time, the stability of the product is stabilized by the soluble phosphate and the soluble calcium salt through a specific addition process, the stable existence of high-concentration calcium of 170mg calcium/100 mL milk in the final product is realized by using an innovative mode different from the prior art in the industry, the excellent taste of the product is ensured, an additional stable system is not used, the nutritive value of the product is better exerted, and the better naturalness of the product is ensured; in addition, the production cost is controllable, and the eating population is not limited.
Compared with the prior art, the invention has the following beneficial effects:
(1) the high-calcium milk disclosed by the invention has the characteristics of reinforcing calcium and phosphorus elements;
(2) according to the high-calcium milk, only soluble calcium salt and soluble phosphate are used as nutrition enhancers in product ingredients, and other stable system components are not added, so that the system stability and the flavor stability in the production process and the shelf life of the product are ensured;
(3) the calcium content of the high-calcium milk product is more than or equal to 170mg/100mL, no precipitate or layering exists, the product has good appearance and tissue state, uniform tissue and good taste, and the calcium source and the phosphorus source mainly exist in the product in a soluble form;
(4) calcium in the final fermented milk product mainly exists in the product in the form of calcium lactate, so that the final fermented milk product is easier to absorb by a human body;
(5) the preparation method provided by the invention is simple and easy to implement, is convenient to implement, and is suitable for industrial production and application.
Detailed Description
The present invention will be described in detail below with reference to specific examples, but the present invention is not limited to these examples.
Example 1
A preparation method of high-calcium milk comprises the following steps:
(1) cleaning milk:
and (3) purifying the qualified raw milk by using a milk purifying machine, and putting the milk after milk purification into a jar for later use.
(2) Preparing materials:
380g of 40 percent of the pre-dissolved material of fresh milk, 0.8g of trisodium phosphate, 0.3g of sodium hydroxide and 4g of calcium lactate are added in sequence.
(3) Homogenizing:
and (3) heating the pre-melted feed liquid obtained after the material preparation in the step (2) to 58 +/-2 ℃ for homogenizing, wherein the homogenizing pressure is 19 +/-1 MPa.
(4) And (3) sterilization:
and (4) heating the milk obtained in the step (3) to 120 +/-10 ℃, sterilizing and preserving heat for 5 s.
(5) Cooling the cow milk obtained in the step (4) to 4 +/-2 ℃, and filling.
The calcium content of the obtained high-calcium milk finished product is 170mg calcium/100 mL milk; after the product is stored for 21 days at 4 ℃, the content of the product does not precipitate or float, and the sensing evaluation of 15 population is good and no abnormity exists.
Example 2
A preparation method of high-calcium milk comprises the following steps:
(1) cleaning milk:
and (3) purifying the qualified raw milk by using a milk purifying machine, and putting the milk after milk purification into a jar for later use.
(2) Preparing materials:
950g of fresh milk pre-melted material, 0.4g of premixed disodium hydrogen phosphate, 0.4g of trisodium phosphate and 0.3g of potassium hydroxide, and 5g of calcium lactate is added.
(3) Homogenizing:
and (3) heating the pre-melted feed liquid obtained after the material preparation in the step (2) to 58 +/-2 ℃ for homogenizing, wherein the homogenizing pressure is 19 +/-1 MPa.
(4) And (3) sterilization:
and (4) heating the milk obtained in the step (3) to 120 +/-10 ℃, sterilizing and preserving heat for 15 s.
(5) Cooling the cow milk obtained in the step (4) to 4 +/-2 ℃, and filling.
The calcium content of the finished high-calcium milk product is 201mg calcium/100 mL milk; the content of the product does not precipitate or float after being stored for 21 days at 4 ℃, and the sensing evaluation of 30 population is good without abnormality.
Example 3
A preparation method of high-calcium milk comprises the following steps:
(1) cleaning milk:
and (3) purifying the qualified raw milk by a milk purifier, and putting the milk after milk purification into a jar for later use.
(2) Preparing materials:
190g of the pre-dissolved fresh milk material, 1g of pre-mixed sodium dihydrogen phosphate, 1g of disodium hydrogen phosphate and 0.5g of sodium hydroxide, and 6g of calcium lactate is added; .
(3) Homogenizing:
heating the pre-melted feed liquid obtained after the material preparation in the step (2) to 58 +/-2 ℃ for homogenizing, wherein the homogenizing pressure is 19 +/-1 MPa;
(4) and (3) sterilization:
heating the milk obtained in the step (3) to 120 +/-10 ℃, sterilizing and preserving heat for 10 s.
(5) Cooling the cow milk obtained in the step (4) to 4 +/-2 ℃, and filling.
The calcium content of the obtained high-calcium milk finished product is 171mg/100 mL; after the product is stored for 21 days at 4 ℃, the content of the product does not precipitate or float, and the sensing evaluation of 25 population is good and no abnormity exists.
Claims (10)
1. High-calcium milk, which is characterized in that: soluble phosphate and soluble calcium salt are used as strengthening sources of calcium element and phosphorus element in product ingredients, and the content of calcium is more than or equal to 170mg/100 mL.
2. The high calcium milk of claim 1, wherein: every 1kg of high-calcium milk comprises the following raw materials: 900g of fresh milk 950-one, 5-7g of soluble calcium salt, 0.5-2.0g of soluble phosphate and 0.1-0.5g of pH regulator.
3. The high calcium milk of claim 2, wherein: the pH regulator is sodium hydroxide or potassium hydroxide.
4. The high-calcium milk according to claim 1, characterized in that: the soluble calcium salt is calcium lactate.
5. The high-calcium milk according to claim 1, characterized in that: the soluble phosphate is one or more of trisodium phosphate, sodium dihydrogen phosphate or disodium hydrogen phosphate.
6. A method for preparing high calcium milk according to any one of claims 1 to 5, characterized in that: the method comprises the following steps:
cleaning fresh cow milk, preheating, sequentially adding soluble calcium salt and soluble phosphate for blending, adjusting pH to neutral with pH regulator, homogenizing, sterilizing, cooling, bottling and storing.
7. The method for preparing high-calcium milk according to claim 6, wherein: the preheating temperature is 55-60 ℃.
8. The method for preparing high-calcium milk according to claim 6, wherein: homogenizing at 55-60 deg.C under 18-20 MPa.
9. The method for preparing high-calcium milk according to claim 6, wherein: sterilizing at 80-140 deg.C for 0.5-15 s.
10. The method for preparing high-calcium milk according to claim 6, wherein: cooling to 2-6 deg.C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210228950.4A CN114600961A (en) | 2022-03-10 | 2022-03-10 | High-calcium milk and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210228950.4A CN114600961A (en) | 2022-03-10 | 2022-03-10 | High-calcium milk and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114600961A true CN114600961A (en) | 2022-06-10 |
Family
ID=81861950
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210228950.4A Pending CN114600961A (en) | 2022-03-10 | 2022-03-10 | High-calcium milk and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN114600961A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1422120A (en) * | 2000-03-31 | 2003-06-04 | 澳大利亚食品工业科学中心 | Nutritional mineral fortification of milk |
| CN1915045A (en) * | 2006-09-07 | 2007-02-21 | 广州风行牛奶有限公司 | Method for adding polyunsaturated fatty acid in animal milk |
| CN103478254A (en) * | 2013-09-09 | 2014-01-01 | 光明乳业股份有限公司 | High-calcium milk as well as raw material composition and preparation method thereof |
-
2022
- 2022-03-10 CN CN202210228950.4A patent/CN114600961A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1422120A (en) * | 2000-03-31 | 2003-06-04 | 澳大利亚食品工业科学中心 | Nutritional mineral fortification of milk |
| CN1915045A (en) * | 2006-09-07 | 2007-02-21 | 广州风行牛奶有限公司 | Method for adding polyunsaturated fatty acid in animal milk |
| CN103478254A (en) * | 2013-09-09 | 2014-01-01 | 光明乳业股份有限公司 | High-calcium milk as well as raw material composition and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 余晓红;邵荣;丁爱华;: "牛初乳鲜奶生产中稳定剂的应用研究", 食品科学, no. 09, 15 September 2008 (2008-09-15) * |
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