CN103478254B - High calcium milk and feedstock composition thereof and preparation method - Google Patents
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Abstract
The invention discloses a kind of high calcium milk and feedstock composition thereof and preparation method.This preparation method comprises the steps: (1) by ionic calcium containing compound, emulsification salt and emulsifiers dissolve in drinking water, obtains reactant liquor; The temperature of described reactant liquor is 40 DEG C ~ 55 DEG C; (2) milk is warming up to 40 DEG C ~ 55 DEG C, the reactant liquor of step (1) gained is evenly added in milk, stir 5min ~ 15min; (3) transpiring moisture; The quality of described moisture is the consumption of drinking water in step (1); (4) homogeneous, sterilization, cooling.The high calcium milk good stability that the present invention obtains, without albumen flocculation, produces and boils rear all without albumen scale formation.
Description
Technical field
The present invention relates to a kind of high calcium milk and feedstock composition thereof and preparation method.
Background technology
Calcium is one of most important mineral element in human body, and wherein the calcium of 99% is present in bone and tooth, and all the other 1% are present in soft tissue and body fluid.When human calcium's intake is not enough, various disease can be caused, time serious, also can affect health.According to investigations, in China resident ordinary meal, the content of calcium only reaches the half of recommended amounts, the general calcium deficiency of all kinds of crowd.Expert points out, by adjustment of diet, particularly supplementing calcium content by dairy produce is a good approach.Therefore, in milk, strengthen calcium is a kind of effective way solving calcium intake deficiency.
At present, define the compound source for Calcium In Food strengthening in national standard, be wherein no lack of the ionic calcium containing compound of some common solubilities as calcium source.BIOLOGICAL CALCIUM source and organic calcium source are compared in these ionic calcium sources, low price and calcium content is high, can not precipitate, can not increase human liver kidney burden in milk, are easy to absorb.But the introducing in ionic calcium source can destroy the rock-steady structure of original protein, generate calcium caseinate, make product occur flocculation; Even if condense without obvious albumen, occur albumen fouling after product heating through chamber wall of being everlasting, make production equipment clean difficulty, loss is large.Therefore, the ionic calcium source dairy products of administration measure, universal significant for high calcium dairy products.
Summary of the invention
Technical problem to be solved by this invention overcomes the defect that protein flocculation and fouling, product stability difference easily appear in ionic high dairy of the prior art, and provides the high calcium milk and feedstock composition thereof and preparation method that a kind of stability is strong.
The invention provides a kind of feedstock composition of high calcium milk, it comprises following component: milk 99.3% ~ 99.71%, ionic calcium containing compound 0.2% ~ 0.45%, emulsification salt 0.07% ~ 0.15%, emulsifying agent 0.02% ~ 0.1%; Described emulsification salt is mass ratio is (the 2:1) ~ citrate of (3:1) and the mixture of sodium phosphate trimer, or citrate; Described percentage is mass percent.
Wherein, described milk is the natural mammal gland secretion forced down from healthy ox body Normal breast of this area routine, can be the whole milk that is separated without fat with through fats portion or the low fat be all separated or skim milk.
Wherein, described ionic calcium containing compound be this area routine solvable, take ionic calcium as the compound in calcium source, preferably for regulation in GB GB14880 " food enrichment use standard " be allowed for modulate in the calcium lactate of breast, L-calcium lactate and calcium monohydrogen phosphate one or more, be more preferably calcium lactate.The consumption of described ionic calcium containing compound is preferably 0.24% ~ 0.36%.
Wherein, the consumption of described emulsification salt is preferably 0.08% ~ 0.12%.
Wherein, described citrate is that this area is conventional, is preferably natrium citricum and/or potassium citrate.When described emulsification salt is the mixture of citrate and sodium phosphate trimer, described citrate and the mass ratio of sodium phosphate trimer are preferably 2:1.
Wherein, described emulsifying agent is that this area is conventional, be preferably singly, one or more in diglycerine fatty acid ester, sucrose fatty ester and phosphatide.
Present invention also offers the preparation method adopting aforementioned base materials composition to prepare high calcium milk, it comprises the steps:
(1) by ionic calcium containing compound, emulsification salt and emulsifiers dissolve in drinking water, obtain reactant liquor; The temperature of described reactant liquor is 40 DEG C ~ 55 DEG C;
(2) milk is warming up to 40 DEG C ~ 55 DEG C, the reactant liquor of step (1) gained is evenly added in milk, stir 5min ~ 15min;
(3) transpiring moisture; The quality of described moisture is the consumption of drinking water in step (1);
(4) homogeneous, sterilization, cooling.
The mode of operation of described step (1) is the mode of operation of this area routine, is preferably mode one: by drinking water after heating of ionic calcium containing compound, emulsification salt and emulsifiers dissolve, then cool to obtain reactant liquor; Or mode two: ionic calcium containing compound, emulsification salt and emulsifying agent are placed in drinking water, heating for dissolving, then cool to obtain reactant liquor.Mode one and the heating described in mode two preferably for being heated to more than 60 DEG C, more preferably for being heated to more than 80 DEG C.Especially emulsification salt and ionic calcium containing compound are dissolved completely in the water of higher temperature in the present invention, the anion in the calcium ion in ionic calcium containing compound and emulsification salt is combined in advance, prevent the casein in calcium ion and milk from combining and produce flocculation.
In step (1), described drinking water is for meeting the water of GB5749-2006 " standards for drinking water quality ".
In step (2), described milk is conventional according to this area before intensification, generally need through standardization, described standardization refers to the index stable and consistent such as protein, fat in order to ensure each batch of product, in the scope that alimentary codex allows, the indices scope reaching described raw milk is adjusted to the index such as protein, fat: protein content >=2.9wt%, fat content >=3.1wt% and nonfat milk solids content >=8.1wt%, by additionally adding or removing a certain material, or concentrated or dilution animal breast carries out.
In step (2), described intensification is preferably for being warming up to 45 DEG C ~ 50 DEG C.Control milk temperature when adding batching, to ensure that neither activating unnecessary calcium ion can make again milk and reactant liquor fully mix.
In step (2), the described mode evenly added is that this area is conventional, preferably for spray adds.The speed that described spray adds is preferably≤5m/s.
In step (2), the time of described stirring is that this area is conventional, is preferably 10min.
In step (3), described transpiring moisture be operating as this area routine techniques, be preferably flash concentration and/or falling film concentration.The quality of described transpiring moisture is the consumption for the drinking water of dissolved ions type calcium containing compound, emulsification salt and emulsifying agent in step (1).
In step (4), described homogeneous is this area routine operation, and the temperature of described homogeneous is preferably 65 DEG C ~ 75 DEG C, and the pressure of described homogeneous is preferably 18Mpa ~ 20Mpa.
In step (4), described sterilization is this area routine operation, is preferably pasteurize and/or UHTS.Described pasteurize is this area routine operation, is preferably sterilization 15s ~ 30s, sterilization 15s at being more preferably 85 DEG C under 70 DEG C ~ 85 DEG C conditions.Described UHTS is this area routine operation, is preferably sterilization 3s ~ 6s, sterilization 4s at being more preferably 137 DEG C under 130 DEG C ~ 137 DEG C conditions.
In step (4), described is cooled to this area routine operation, and the temperature of described cooling is preferably less than 7 DEG C, is more preferably 2 DEG C ~ 6 DEG C.
In step (1), described dissolving is preferably for Keep agitation dissolves.
In step (4), after carrying out cooling processing to obtained high calcium milk, also need conventionally to carry out filling to high calcium milk.
Present invention also offers the high calcium milk adopting above-mentioned preparation method to obtain.
On the basis meeting this area general knowledge, above-mentioned each optimum condition, can be combined, obtain the preferred embodiments of the invention.
Agents useful for same of the present invention and raw material are all commercially.
Positive progressive effect of the present invention is:
The present invention uses cheap, solubility, the good ionic calcium containing compound absorbed as calcium source, and the calcium source for high calcium milk adds a kind of selection.Obtained high calcium milk product stability is good, without albumen flocculation, produces and boils rear all without albumen scale formation.Meanwhile, preparation method of the present invention solves the problem that in high calcium milk production equipment pipeline, albumen fouling is serious, cleaning is difficult and loss is large.
Detailed description of the invention
Mode below by embodiment further illustrates the present invention, but does not therefore limit the present invention among described scope of embodiments.The experimental technique of unreceipted actual conditions in the following example, conventionally and condition, or selects according to catalogue.
In following embodiment, raw materials used source is: milk: Shanghai Bright Dairy & Food Co., Ltd.'s dairy products two factory; All the other batchings: upper sea blue island food additives company.
In following embodiment, if no special instructions, described percentage is mass percent.
Embodiment 1
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 1.
The feedstock composition of the high calcium milk of table 1 embodiment 1
| Composition | Consumption (%) |
| Milk | 99.3 |
| Calcium lactate | 0.45 |
| Natrium citricum | 0.1 |
| Sodium phosphate trimer | 0.05 |
| Single, diglycerine fatty acid ester | 0.1 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 85 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 45 DEG C;
(2) milk is warming up to 45 DEG C, the solution spraying of step (1) gained is added rear stirring 10min;
(3) flash method evaporates the moisture dissolving batching in step (1);
(4) be warming up to 65 DEG C, 20MPa homogeneous, 85 DEG C, 15s pasteurize, be cooled to 2 DEG C ~ 6 DEG C, filling.
Embodiment 2
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 2.
The feedstock composition of the high calcium milk of table 2 embodiment 2
| Composition | Consumption (%) |
| Milk | 99.58 |
| L-calcium lactate | 0.3 |
| Natrium citricum | 0.08 |
| Single, diglycerine fatty acid ester | 0.04 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 80 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 50 DEG C;
(2) milk is warming up to 50 DEG C, the solution spraying of step (1) gained is added rear stirring 15min;
(3) flash method evaporates the moisture dissolving batching in step (1);
(4) be warming up to 75 DEG C, 18MPa homogeneous, 75 DEG C, 15s pasteurize, be cooled to 2 DEG C ~ 6 DEG C, filling.
Embodiment 3
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 3.
The feedstock composition of the high calcium milk of table 3 embodiment 3
| Composition | Consumption (%) |
| Milk | 99.44 |
| Calcium lactate | 0.4 |
| Natrium citricum | 0.08 |
| Potassium citrate | 0.04 |
| Single, diglycerine fatty acid ester | 0.02 |
| Sucrose fatty ester | 0.02 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 80 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 50 DEG C;
(2) milk is warming up to 50 DEG C, the solution spraying of step (1) gained is added rear stirring 10min;
(3) falling film concentration method removes the moisture dissolving batching in step (1);
(4) be warming up to 75 DEG C, 18MPa homogeneous, 130 DEG C, 4s UHTS, be cooled to 2 DEG C ~ 6 DEG C, filling.
Embodiment 4
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 4.
The feedstock composition of the high calcium milk of table 4 embodiment 4
| Composition | Consumption (%) |
| Milk | 99.71 |
| Calcium lactate | 0.2 |
| Natrium citricum | 0.07 |
| Single, diglycerine fatty acid ester | 0.02 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 60 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 55 DEG C;
(2) milk is warming up to 55 DEG C, stirs the solution simultaneously slowly adding step (1) gained, stir 15min afterwards;
(3) flash method evaporates the moisture dissolving batching in step (1);
(4) be warming up to 65 DEG C, 20MPa homogeneous, 137 DEG C, 4s ultra high temperature sterilization, be cooled to 2 DEG C ~ 6 DEG C, filling.
Embodiment 5
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 5.
The feedstock composition of the high calcium milk of table 5 embodiment 5
| Composition | Consumption (%) |
| Milk | 99.49 |
| Calcium lactate | 0.36 |
| Natrium citricum | 0.08 |
| Sodium phosphate trimer | 0.04 |
| Single, diglycerine fatty acid ester | 0.02 |
| Sucrose fatty ester | 0.01 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 90 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 40 DEG C;
(2) milk is warming up to 40 DEG C, the solution spraying of step (1) gained is added rear stirring 5min;
(3) flash method evaporates the moisture dissolving batching in step (1);
(4) be warming up to 75 DEG C, 20MPa homogeneous, 85 DEG C, 15s pasteurize, be cooled to 2 DEG C ~ 6 DEG C, filling.
Embodiment 6
The feedstock composition of the high calcium milk of the present embodiment is as shown in table 6.
The feedstock composition of the high calcium milk of table 6 embodiment 6
| Composition | Consumption (%) |
| Milk | 99.3 |
| Calcium lactate | 0.4 |
| Natrium citricum | 0.15 |
| Sodium phosphate trimer | 0.05 |
| Single, diglycerine fatty acid ester | 0.1 |
The preparation method of the high calcium milk of the present embodiment comprises following processing step:
(1) a certain amount of drinking water is heated to 80 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 40 DEG C;
(2) milk is warming up to 40 DEG C, the solution spraying of step (1) gained is added rear stirring 10min;
(3) flash method evaporates the moisture dissolving batching in step (1);
(4) be warming up to 65 DEG C, 20MPa homogeneous, 85 DEG C, 15s pasteurize, be cooled to 2 DEG C ~ 6 DEG C, filling.
Effect example 1
Carry out calcium content test to the high calcium milk that embodiment 1 ~ 6 obtains, method of testing is with reference to the atomic absorption spectrophotometry in the GB GB5413.21-2010 mensuration of calcium, iron, zinc, sodium, potassium, magnesium, copper and manganese " in national food safety standard-infant food and the dairy products ".
Test result shows, the calcium content of high calcium milk of the present invention reaches 120mg/100mL ~ 150mg/100mL, and the high calcium be more than or equal to for milk in GB GB28050-2011 requires: every 100mL milk can meet 15% ~ 19% of human body calcium every day demand.And technique of the present invention and formula, product flocculates without albumen in process of production, without particle, glue wall or plugging phenomenon; Product is in stable condition within the shelf-life, without albumen flocculation, boils rear without albumen fouling, smoother taste.
Comparative example 1
By existing high calcium milk, (Shanghai Bright Dairy & Food Co., Ltd. produces this comparative example, the calcium source of this high calcium milk is newborn mineral salt) carry out Performance comparision with the high calcium milk of embodiments of the invention 1, test item comprises in production process to be had bottom pill tank bottom deposit-free, product sensory, the end of term packing of product of guaranteeing the quality with or without precipitation, and thermal-stable, result is as shown in table 7.
The performance comparison result of the high calcium milk of the existing high calcium milk of table 7 and embodiment 1
Visible, high calcium milk provided by the invention is compared with existing high calcium milk, and mouthfeel is better, in stability, the storage life is significantly increased.
Comparative example 2
The feedstock composition of the high calcium milk of this comparative example is as shown in table 8.
The feedstock composition of the high calcium milk of table 8 comparative example 2
| Composition | Consumption (%) |
| Milk | 99.71 |
| Calcium lactate | 0.2 |
| Natrium citricum | 0.07 |
| Single, diglycerine fatty acid ester | 0.02 |
The preparation method of the high calcium milk of this comparative example comprises following processing step:
(1) a certain amount of drinking water is heated to 60 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 55 DEG C;
(2) milk is warming up to 65 DEG C, stirs, slowly add the solution of step (1) gained simultaneously, then stir 15min, find to occur albumen precipitation thing at the bottom of pill tank;
(3) flash method evaporates the moisture dissolving batching in step (1);
(4) be warming up to 65 DEG C, 20MPa homogeneous, 85 DEG C, 15s pasteurize, block for the filter pipe clinging to sterilization, high calcium milk cannot carry out sterilization smoothly.
Comparative example 3
The feedstock composition of the high calcium milk of this comparative example is as shown in table 9.
The feedstock composition of the high calcium milk of table 9 comparative example 3
| Composition | Consumption (%) |
| Milk | 99.71 |
| Calcium lactate | 0.2 |
| Natrium citricum | 0.07 |
| Single, diglycerine fatty acid ester | 0.02 |
The preparation method of the high calcium milk of this comparative example comprises following processing step:
(1) a certain amount of drinking water is heated to 60 DEG C, adds all the other batchings in above-mentioned formula except milk, be stirred to abundant dissolving, be cooled to 55 DEG C;
(2) milk is warming up to 4 DEG C, stirs the solution simultaneously slowly adding step (1) gained, stir 15min afterwards;
(3) flash method evaporates the moisture dissolving batching in step (1);
(4) be warming up to 65 DEG C, 20MPa homogeneous, 85 DEG C, 15s pasteurize, be cooled to 2 ~ 6 DEG C, filling.
Finished product is poured in beaker, product boiling in cup is warming up to beaker bottom, finds that there is sticky end phenomenon and occur.And the product of embodiment 1 is when carrying out boiling test, result is good, without sticky end phenomenon.
Claims (12)
1. the preparation method of a high calcium milk, it is characterized in that, the feedstock composition of described high calcium milk is composed of the following components: milk 99.3% ~ 99.71%, ionic calcium containing compound 0.2% ~ 0.45%, emulsification salt 0.07% ~ 0.15%, emulsifying agent 0.02% ~ 0.1%; Described emulsification salt is the mixture of citrate and sodium phosphate trimer, or citrate, and in the mixture of described citrate and sodium phosphate trimer, the mass ratio of citrate and sodium phosphate trimer is (2:1) ~ (3:1); Described percentage is mass percent;
Described preparation method comprises the steps:
(1) by ionic calcium containing compound, emulsification salt and emulsifiers dissolve in drinking water, obtain reactant liquor; The temperature of described reactant liquor is 40 DEG C ~ 55 DEG C;
(2) milk is warming up to 40 DEG C ~ 55 DEG C, the reactant liquor of step (1) gained is evenly added in milk, stir 5min ~ 15min;
(3) transpiring moisture; The quality of described moisture is the consumption of drinking water in step (1);
(4) homogeneous, sterilization, cooling.
2. preparation method as claimed in claim 1, it is characterized in that, described ionic calcium containing compound is calcium lactate and/or calcium monohydrogen phosphate; The consumption of described ionic calcium containing compound is 0.24% ~ 0.36%.
3. preparation method as claimed in claim 2, it is characterized in that, described calcium lactate is L-calcium lactate.
4. preparation method as claimed in claim 1, it is characterized in that, the consumption of described emulsification salt is 0.08% ~ 0.12%; Described citrate is natrium citricum and/or potassium citrate; When described emulsification salt is the mixture of citrate and sodium phosphate trimer, described citrate and the mass ratio of sodium phosphate trimer are 2:1.
5. preparation method as claimed in claim 1, is characterized in that, described emulsifying agent be singly, one or more in diglycerine fatty acid ester, sucrose fatty ester and phosphatide.
6. preparation method as claimed in claim 1, it is characterized in that, the mode of operation of described step (1) is the mode of operation of this area routine, specifically carry out in the following manner, mode one: by drinking water after heating of ionic calcium containing compound, emulsification salt and emulsifiers dissolve, then cool to obtain reactant liquor; Or mode two: ionic calcium containing compound, emulsification salt and emulsifying agent are placed in drinking water, heating for dissolving, then cool to obtain reactant liquor; Wherein, described being heated to be is heated to more than 60 DEG C.
7. preparation method as claimed in claim 6, it is characterized in that, described being heated to be is heated to more than 80 DEG C.
8. preparation method as claimed in claim 1, it is characterized in that, in step (2), described intensification is for being warming up to 45 DEG C ~ 50 DEG C; The described mode evenly added is that spray adds, and the speed that described spray adds is≤5m/s; The time of described stirring is 10min.
9. preparation method as claimed in claim 1, is characterized in that, in step (3), described transpiring moisture be operating as flash concentration and/or falling film concentration.
10. preparation method as claimed in claim 1, it is characterized in that, in step (4), the temperature of described homogeneous is 65 DEG C ~ 75 DEG C, and the pressure of described homogeneous is 18Mpa ~ 20Mpa; Described sterilization is pasteurize and/or UHTS; Described pasteurize is sterilization 15s ~ 30s under 70 DEG C ~ 85 DEG C conditions; Described UHTS is sterilization 3s ~ 6s at 130 DEG C ~ 137 DEG C; Described being cooled to is cooled to 2 DEG C ~ 6 DEG C.
11. preparation methods as claimed in claim 10, is characterized in that, described pasteurize is sterilization 15s under 85 DEG C of conditions; Described UHTS is sterilization 4s at 137 DEG C.
The high calcium milk that 12. preparation methods as described in any one of claim 1 ~ 11 obtain.
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| CN105558043B (en) * | 2015-12-16 | 2020-02-07 | 光明乳业股份有限公司 | High-calcium milk and preparation method thereof |
| CN105767189A (en) * | 2016-03-09 | 2016-07-20 | 宁夏金树沅农贸有限公司 | Moringa oleifera high-calcium milk production and processing technology |
| CN106819856A (en) * | 2016-12-14 | 2017-06-13 | 光明乳业股份有限公司 | A kind of pudding and preparation method thereof |
| CN108208173A (en) * | 2016-12-22 | 2018-06-29 | 张影 | It is a kind of to have the fresh milk and dairy produce for adjusting three high effects |
| CN108208174A (en) * | 2016-12-22 | 2018-06-29 | 张影 | It is a kind of to have the fresh milk and dairy produce for improving pipe intestinal digesting function |
| CN112544772A (en) * | 2020-12-08 | 2021-03-26 | 光明乳业股份有限公司 | Raw material composition of calcium-fortified frozen beverage, calcium-fortified frozen beverage and preparation method of calcium-fortified frozen beverage |
| CN114600961A (en) * | 2022-03-10 | 2022-06-10 | 山东得益乳业股份有限公司 | High-calcium milk and preparation method thereof |
| CN115720933A (en) * | 2022-12-06 | 2023-03-03 | 光明乳业股份有限公司 | High-calcium milk containing probiotics and preparation method thereof |
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