CN103462038B - Propolis corn-oil softgel and preparation method thereof - Google Patents
Propolis corn-oil softgel and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of health food, and specifically relates to a propolis corn-oil softgel and a preparation method thereof. The propolis corn-oil softgel is composed of a softgel shell and contents packaged in the soft capsule shell, wherein the contents comprise the following materials in parts by weight: 150-300 parts of propolis, 600-800 parts of corn oil, 10-70 parts of Chinese angelica oil and 5-15 parts of vitamin C; and the softgel shell comprises the following materials in parts by weight: 80-180 parts of polyethylene glycol, 260-330 parts of gelatin, 140-200 parts of glycerin, 0.5-1.6 parts of fumaric acid, 0.2-0.8 part of ethyl p-hydroxybenzoate and 300-390 parts of water. The propolis corn-oil softgel helps to extremely enhance the auxiliary hpyerglycemic effect of propolis by adding Chinese angelica oil and corn oil both with functions of invigorating blood circulation and enriching blood into propolis.
Description
Technical field
The invention belongs to technical field of health care food, be specifically related to a kind of propolis corn-oil softgel and preparation method thereof.
Background technology
Corn oil processes obtained vegetable fat by maize, forms primarily of unrighted acid.Its Linoleic acid is essential fatty acid, is to form the part of human body cell, can combine in human body with cholesterol, in mobility with eubolism, has the effect of preventing and treating the angiocardiopathies such as atherosclerotic.Sitosterol in corn oil has the effect reducing cholesterol, is rich in vitamin E, Wheat Protein, can prevents and treats the several functions such as scheroma, yctalopia, dermatitis, bronchiectasis, and have certain antitumaous effect.Due to corn oil, and also because it is of high nutritive value, the sense of taste is good, not perishable, thus deeply popular to people.In American-European countries, corn oil is extensively eaten by as a kind of table oil, enjoys the laudatory title such as " healthy oil ", " relieved oil ", " long life oil ".
Propolis be honeybee for maintaining the active principle of whole Population Health, the bee colony of 5 ~ 60,000 can only produce propolis 100-150 gram in 1 year, is described as " purple gold ".Recent studies proves, enriching and the bioactivator of uniqueness contained by propolis, make it have antibacterial, anti-inflammatory, antipruritic, anti-oxidant, strengthen immune, hypoglycemic, reducing blood lipid, the several functions such as antitumor, medical treatment, health-care effect is widely had to human body, now become the focus of various countries' scientific research, and become emerging health products and extremely praise highly.
Pungent, the sweet and slightly warm in nature of Radix Angelicae Sinensis taste, the thoughts of returning home, liver, spleen three warp, enrich blood and invigorate blood circulation, menstruction regulating and pain relieving, the effect relaxed bowel, and is one of Chinese medicine that Clinical practice frequency is the highest, have the title of " ten side's rules for doing division with a one-digit divisor on the abacus ".In " notice about further specification healthy food material management " that the Ministry of Public Health announces, when being classified as the article that can be used for health food.The chemical composition of plurality of classes has been isolated to, as taken lactone as the volatile ingredient, organic acid, polysaccharide, amino acids etc. of representative in Radix Angelicae Sinensis.Wherein volatile ingredient is the Chinese medicine constituent of Radix Angelicae Sinensis.Chinese angelica volatile oil at isolated uterine smooth muscle, relieving asthma, CNS inhibition, analgesia and have pharmacologically active widely in impact of immunologic function etc.In Angelica oil, main component has (Z)-Ligustilide, (E)-Ligustilide, (Z)-normal-butyl furan lactone, palmitic acid, β-sitosterol, forulic acid etc.
Be raw material with three, compound is prepared into health products, and there is not been reported.
Summary of the invention
The invention provides a kind of propolis corn-oil softgel and preparation method thereof.This propolis corn-oil softgel with the addition of the Angelica oil and corn oil with blood circulation promoting and enriching effect in by propolis, greatly strengthen the effect of the auxiliary hyperglycemic of propolis.
The present invention is realized by following technical scheme:
A kind of propolis corn-oil softgel, be made up of soft capsule rubber and the content be wrapped in rubber, described content comprises the following material with parts by weight:
Propolis 150-300 part
Corn oil 600-800 part
Angelica oil 10-70 part
Vitamin C 5-15 part
Described soft capsule rubber comprises the following material with parts by weight:
Polyethylene glycol 80-180 part
Gelatin 260-330 part
Glycerine 140-200 part
Fumaric acid 0.5-1.6 part
Ethyl-para-hydroxybenzoate 0.2-0.8 part
Water 300-390 part.
Preferably, above-mentioned propolis corn-oil softgel, the predominant amount following material by weight of described content:
Propolis 200 parts
Corn oil 750 parts
Angelica oil 50 parts
Vitamin C 10 parts
Described soft capsule rubber comprises the following material in weight ratio part:
Polyethylene glycol 100 parts
295 parts, gelatin
Glycerine 172 parts
Fumaric acid 1.0 parts
Ethyl-para-hydroxybenzoate 0.6 part
350 parts, water.
In propolis corn-oil softgel of the present invention, if each composition weight in grams, make preparation, can be made into 1000 doses.Described 1000 doses of dosage forms referring to UD, specifically refer to soft capsule 1000.
More than composition is by weight as proportioning, can increase according to corresponding proportion when producing or reduce, as large-scale production can in units of kg, or with t(ton) be unit; Preparation also can in units of g on a small scale.Weight can increase or reduce, but the constant rate of raw medicinal herbs weight proportion between each composition.
In above-mentioned propolis corn-oil softgel, described corn oil is one-level corn oil.
In above-mentioned propolis corn-oil softgel, general flavone content > 5% in described propolis.
In above-mentioned propolis corn-oil softgel, content >=60% of Ligustilide in described Angelica oil.
In above-mentioned propolis corn-oil softgel, described Angelica oil preparation method is: the preparation method of Angelica oil is: Radix Angelicae Sinensis pulverizing medicinal materials, granularity is 20-40 order, carries out SCF-CO 2, and extraction kettle pressure is 25mpa, extraction temperature is 40-50 DEG C, CO2 flow is 15L/h, and extraction time is 2h, resolution temperature 50 DEG C, resolve pressure 6Mpa, obtain Angelica oil.
The preparation method of upper described propolis corn-oil softgel, comprises following steps:
The preparation method of propolis corn-oil softgel according to claim 1, comprises following steps:
The preparation of (a) softgel shell glue: change the water adding recipe quantity in glue tank, after being warming up to 50 DEG C, add gelatin, glycerine, polyethylene glycol, ethyl-para-hydroxybenzoate, fumaric acid, water by weight proportion, stir, be warming up to 70 DEG C, after band gelatin all dissolves, vacuum sloughs unnecessary water, pumpdown time is 1-1.5h, 100 order net filtrations, 40-60 DEG C insulation leave standstill more than 1.5 hours for subsequent use;
The preparation of (b) soft capsule content: by the corn oil of recipe quantity, Angelica oil, propolis heating and melting, mixing, lets cool, slowly adds vitamin C, and limit edged stirs, and makes it fully mix, obtains soft capsule content;
C () is filling: move in the fluid reservoir of encapsulating machine by content liquid rotating, regulates loading amount, is pressed into ball;
D () is shaped: the soft capsule pressed through encapsulating machine is sent in rotating cage by conveyer belt, and blow on sizing more than 1.5 hours, goes in soft capsule sizing machine, low-temperature shaped 5 hours;
E () washes ball: defend by the soft capsule after sizing in drying machine, carry out drying, drying time is 10 hours, is dried to softgel shell moisture at 7%-12%.
The preparation method of above-mentioned propolis corn-oil softgel, detailed step is as follows:
The preparation of (a) softgel shell glue: change in glue tank the water adding 100 parts, after being warming up to 50 DEG C, add 295 parts, gelatin, glycerine 172 parts, polyethylene glycol 100 parts, ethyl-para-hydroxybenzoate 0.6 part, fumaric acid 1.0 parts, 250 parts, water, stir, be warming up to 70 DEG C, after treating that gelatin all melts, vacuum sloughs unnecessary moisture, and the pumpdown time is 1-1.5h, 80 order net filtrations, 50 DEG C insulation leave standstill more than two hours for subsequent use;
The preparation of (b) soft capsule content: by the corn oil 750 parts of recipe quantity, Angelica oil 50 parts, propolis 200 parts of heating and meltings, mixing, lets cool, slowly adds vitamin C 10 parts, and limit edged stirs, and makes it fully mix, obtains soft capsule content;
C () is filling: move in the fluid reservoir of encapsulating machine by content liquid rotating, regulates loading amount, is pressed into ball;
D () is shaped: the soft capsule pressed through encapsulating machine is sent in rotating cage by conveyer belt, and blow on sizing more than 1.5 hours, goes in soft capsule sizing machine, low-temperature shaped 5 hours;
E () washes ball: defend by the soft capsule after sizing in drying machine, carry out drying, drying time is 10 hours, is dried to softgel shell moisture at 7%-12%.
Propolis corn-oil softgel of the present invention, has the effect of good auxiliary hyperglycemic.Usage and dosage is every day 2-3 time, each 2-5 grain.
The invention has the beneficial effects as follows:
1. the present invention with the addition of the Angelica oil and corn oil with blood circulation promoting and enriching in propolis, have been surprisingly found that, significantly enhances the effect of the auxiliary hyperglycemic of propolis.
2. test-meal result of the test shows, takes tested material one month, and propolis group and test-meal group clinical symptoms have had obvious improvement, compare with control group, significant difference (P < 0.05) or extremely remarkable (P < 0.01); Wherein soft capsule better effects if of the present invention, compared with propolis group, significant difference (P < 0.05).Compare with before test-meal after the test-meal of test-meal group, fasting blood-glucose declines to some extent, and difference extremely significantly (P < 0.01); Fasting blood-glucose no significant difference before two groups of test-meals, after test-meal, propolis group and food group fasting blood-glucose, fall and decline percentage compare with control group, difference all extremely significantly (P < 0.01), and test-meal group is compared with propolis group, average fasting blood-glucose fall and the equal significant difference of decline percentage (P < 0.05), illustrate that this propolis corn-oil softgel is by the effect reducing fasting blood-glucose significantly.
3. propolis corn-oil softgel of the present invention, is convenient to take and carry.
4. propolis corn-oil softgel of the present invention, preparation technology is simple, and with short production cycle, production cost is low.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described, so that those skilled in the art more understands the present invention, but does not therefore limit the present invention.
In embodiments of the invention, corn oil used is the one-level corn oil that Shandong Sanxing Corn Technology Co., Ltd. produces, and propolis is purchased from, general flavone content > 8.37%.
Embodiment 1: the preparation of Angelica oil
Get Radix Angelicae Sinensis medicinal material 10kg, pulverize, grinding particle size is 30 orders, carries out supercritical CO
2extraction, extraction kettle pressure is 25mpa, and extraction temperature is 45 DEG C, CO
2flow is 15L/h, and extraction time is 2h, resolution temperature 50 DEG C, resolves pressure 6Mpa, obtains Angelica oil.Prepare Angelica oil 0.154kg altogether, wherein the content of Ligustilide is 71.3%
Embodiment 2:
Soft capsule content prescription:
Propolis 200g
Corn oil 750g
Angelica oil 50g
Vitamin C 10g
Soft capsule shell prescription:
Polyethylene glycol 100g
Gelatin 295g
Glycerine 172g
Fumaric acid 1.0g
Ethyl-para-hydroxybenzoate 0.6g
Water 350g
Preparation method:
The preparation of (a) softgel shell glue: change the water adding recipe quantity in glue tank, after being warming up to 50 DEG C, add gelatin, glycerine, polyethylene glycol, ethyl-para-hydroxybenzoate, fumaric acid, water by weight proportion, stir, be warming up to 70 DEG C, after band gelatin all dissolves, vacuum sloughs unnecessary water, pumpdown time is 1.5h, 100 order net filtrations, 50 DEG C insulation leave standstill more than 1.5 hours for subsequent use;
B the preparation of () soft capsule content: by the corn oil of recipe quantity, Angelica oil, propolis heating and melting, mixing, lets cool, slowly adds vitamin C, and limit edged stirs, and makes it fully mix, obtains soft capsule content.
C () is filling: move in the fluid reservoir of encapsulating machine by content liquid rotating, regulates loading amount, is pressed into ball.
D () is shaped: the soft capsule pressed through encapsulating machine is sent in rotating cage by conveyer belt, and blow on sizing more than 1.5 hours, goes in soft capsule sizing machine, low-temperature shaped 5 hours.
E () washes ball: defend by the soft capsule after sizing in drying machine, carry out drying, drying time is 10 hours, is dried to softgel shell moisture 10%.Prepare 1000 altogether.
Embodiment 3:
Soft capsule content prescription:
Propolis 150g
Corn oil 600g
Angelica oil 70g
Vitamin C 5g
Soft capsule shell prescription:
Polyethylene glycol 80g
Gelatin 330g
Glycerine 200g
Fumaric acid 1.6g
Ethyl-para-hydroxybenzoate 0.5g
Water 390g
Preparation method:
The preparation of (a) softgel shell glue: change the water adding recipe quantity in glue tank, after being warming up to 50 DEG C, add gelatin, glycerine, polyethylene glycol, ethyl-para-hydroxybenzoate, fumaric acid, water by weight proportion, stir, be warming up to 70 DEG C, after band gelatin all dissolves, vacuum sloughs unnecessary water, pumpdown time is 1.2h, 100 order net filtrations, 40 DEG C insulation leave standstill more than 1.5 hours for subsequent use;
B the preparation of () soft capsule content: by the corn oil of recipe quantity, Angelica oil, propolis heating and melting, mixing, lets cool, slowly adds vitamin C, and limit edged stirs, and makes it fully mix, obtains soft capsule content.
C () is filling: move in the fluid reservoir of encapsulating machine by content liquid rotating, regulates loading amount, is pressed into ball.
D () is shaped: the soft capsule pressed through encapsulating machine is sent in rotating cage by conveyer belt, and blow on sizing more than 1.5 hours, goes in soft capsule sizing machine, low-temperature shaped 5 hours.
F () washes ball: defend by the soft capsule after sizing in drying machine, carry out drying, drying time is 10 hours, is dried to softgel shell moisture at 7%-12%.Prepare 1000 altogether.
Embodiment 4:
Soft capsule content prescription:
Propolis 300g
Corn oil 800g
Angelica oil 10g
Vitamin C 15g
Soft capsule shell prescription:
Polyethylene glycol 180g
Gelatin 260g
Glycerine 140g
Fumaric acid 0.5g
Ethyl-para-hydroxybenzoate 0.2g
Water 300g
Preparation method:
The preparation of (g) softgel shell glue: change the water adding recipe quantity in glue tank, after being warming up to 50 DEG C, add gelatin, glycerine, polyethylene glycol, ethyl-para-hydroxybenzoate, fumaric acid, water by weight proportion, stir, be warming up to 70 DEG C, after band gelatin all dissolves, vacuum sloughs unnecessary water, pumpdown time is 1.5h, 100 order net filtrations, 60 DEG C insulation leave standstill more than 1.5 hours for subsequent use;
H the preparation of () soft capsule content: by the corn oil of recipe quantity, Angelica oil, propolis heating and melting, mixing, lets cool, slowly adds vitamin C, and limit edged stirs, and makes it fully mix, obtains soft capsule content.
(i) filling: content liquid rotating is moved in the fluid reservoir of encapsulating machine, regulate loading amount, be pressed into ball.
J () is shaped: the soft capsule pressed through encapsulating machine is sent in rotating cage by conveyer belt, and blow on sizing more than 1.5 hours, goes in soft capsule sizing machine, low-temperature shaped 5 hours.
K () washes ball: defend by the soft capsule after sizing in drying machine, carry out drying, drying time is 10 hours, is dried to softgel shell moisture 8%.Prepare 1000 altogether.
For proving the beneficial effect of this law, carried out human feeding trial to propolis corn-oil softgel prepared by embodiment 2, result is as follows:
1.1 test specimens: propolis corn-oil softgel, are produced by Shandong Sanxing Corn Technology Co., Ltd., 1g/ grain.
1.2 experimenters select: undertaken by " health food inspection and assessment technical specification " requirement.
1.3 experimental designs and grouping: balancedly divide blank group, propolis group and test-meal group at random by standard compliant diabetic.Wherein blank group 53 example, propolis group 53 example, test-meal group 53 example.
1.4 test methods: test-meal group takes propolis corn-oil softgel, every day twice, every day 2, blank group takes placebo, and propolis group takes bee glue soft capsule, and every day 2 times, each 2, instructions of taking is identical with test-meal group, Continuous Observation 30d.
2 results
2.1 Symptom Observation
Take tested material one month as seen, propolis group and test-meal group clinical symptoms have had obvious improvement, compare with control group, significant difference (P < 0.05) or extremely significantly (P < 0.01); Wherein soft capsule better effects if of the present invention, compared with propolis group, significant difference (P < 0.05).
From table 2, compare with before test-meal after the test-meal of test-meal group, fasting blood-glucose declines to some extent, and difference extremely significantly (P < 0.01); Fasting blood-glucose no significant difference before two groups of test-meals, after test-meal, propolis group and food group fasting blood-glucose, fall and decline percentage compare with control group, difference all extremely significantly (P < 0.01), and test-meal group is compared with propolis group, average fasting blood-glucose fall and the equal significant difference of decline percentage (P < 0.05), illustrate that this propolis corn-oil softgel is by the effect reducing fasting blood-glucose significantly.
Claims (7)
1. a propolis corn-oil softgel, be made up of soft capsule rubber and the content be wrapped in rubber, it is characterized in that, described content comprises the following material with parts by weight:
Propolis 150-300 part
Corn oil 600-800 part
Angelica oil 10-70 part
Vitamin C 5-15 part
Described soft capsule rubber comprises the following material with parts by weight:
Polyethylene glycol 80-180 part
Gelatin 260-330 part
Glycerine 140-200 part
Fumaric acid 0.5-1.6 part
Ethyl-para-hydroxybenzoate 0.2-0.8 part
Water 300-390 part.
2. propolis corn-oil softgel according to claim 1, is characterized in that, the predominant amount following material by weight of described content:
Propolis 200 parts
Corn oil 750 parts
Angelica oil 50 parts
Vitamin C 10 parts
Described soft capsule rubber comprises the following material in weight ratio part:
Polyethylene glycol 100 parts
295 parts, gelatin
Glycerine 172 parts
Fumaric acid 1.0 parts
Ethyl-para-hydroxybenzoate 0.6 part
350 parts, water.
3. propolis corn-oil softgel according to claim 1, is characterized in that, described corn oil is one-level corn oil.
4. propolis corn-oil softgel according to claim 1, is characterized in that, general flavone content > 5% in described propolis.
5. propolis corn-oil softgel according to claim 1, is characterized in that, content >=60% of Ligustilide in described Angelica oil.
6. propolis corn-oil softgel according to claim 1, is characterized in that, described Angelica oil preparation method is: the preparation method of Angelica oil is: Radix Angelicae Sinensis pulverizing medicinal materials, and granularity is 20-40 order, carries out supercritical CO
2extraction, extraction kettle pressure is 25MPa, and extraction temperature is 40-50 DEG C, CO
2flow is 15L/h, and extraction time is 2h, resolution temperature 50 DEG C, resolves pressure 6MPa, obtains Angelica oil.
7. the preparation method of propolis corn-oil softgel according to claim 1, comprises following steps:
The preparation of (a) softgel shell glue: change the water adding recipe quantity in glue tank, after being warming up to 50 DEG C, add gelatin, glycerine, polyethylene glycol, ethyl-para-hydroxybenzoate, fumaric acid by weight proportion, stir, be warming up to 70 DEG C, after band gelatin all dissolves, vacuum sloughs unnecessary water, pumpdown time is 1-1.5h, 100 order net filtrations, 40-60 DEG C insulation leave standstill more than 1.5 hours for subsequent use;
The preparation of (b) soft capsule content: by the corn oil of recipe quantity, Angelica oil, propolis heating and melting, mixing, lets cool, slowly adds vitamin C, and limit edged stirs, and makes it fully mix, obtains soft capsule content;
C () is filling: move in the fluid reservoir of encapsulating machine by content liquid rotating, regulates loading amount, is pressed into ball;
D () is shaped: the soft capsule pressed through encapsulating machine is sent in rotating cage by conveyer belt, and blow on sizing more than 1.5 hours, goes in soft capsule sizing machine, low-temperature shaped 5 hours;
E () washes ball: will be put in drying machine by the soft capsule after sizing, carry out drying, drying time is 10 hours, is dried to softgel shell moisture at 7%-12%.
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| CN108813499A (en) * | 2018-07-09 | 2018-11-16 | 武汉康思农生物科技有限公司 | A kind of bee glue soft capsule formula and preparation process |
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| CN101810336B (en) * | 2010-04-30 | 2012-03-21 | 广东仙乐制药有限公司 | Chewable soft capsules and method for preparing same |
| CN101843308B (en) * | 2010-06-07 | 2012-12-12 | 杭州天厨蜜源保健品有限公司 | Propolis soft capsule and preparation method thereof |
| CN101869300A (en) * | 2010-06-11 | 2010-10-27 | 浙江省医学科学院 | Bee glue and perilla herb oil health-care food for assisting blood fat lowering and preparation method thereof |
| CN101912111B (en) * | 2010-07-19 | 2012-09-26 | 马建中 | Method for preparing high-content propolis soft capsules |
| CN102824371B (en) * | 2012-08-23 | 2014-04-16 | 石药集团中奇制药技术（石家庄）有限公司 | Propolis-lycopene composition and preparation method thereof |
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| CN103141845B (en) * | 2013-03-22 | 2014-11-05 | 山东三星玉米产业科技有限公司 | Soft phytosterol capsule and method for preparing same |
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Address after: 256209 private science and Technology Park, Handian Town, Zouping County, Binzhou City, Shandong Province Patentee after: longevity flower food co., ltd. Address before: 256209 private science and Technology Park, Handian Town, Zouping County, Binzhou City, Shandong Province Patentee before: SHANDONG SANXING CORN INDUSTRY TECHNOLOGY Co.,Ltd. |
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