CN103283869B - Tea-seed oil extract and soft capsule as well as preparation methods thereof - Google Patents
Tea-seed oil extract and soft capsule as well as preparation methods thereof Download PDFInfo
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- CN103283869B CN103283869B CN201310229656.6A CN201310229656A CN103283869B CN 103283869 B CN103283869 B CN 103283869B CN 201310229656 A CN201310229656 A CN 201310229656A CN 103283869 B CN103283869 B CN 103283869B
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Abstract
The invention discloses a tea-seed oil extract and a soft capsule as well as preparation methods thereof. The tea-seed oil extract is obtained by the following steps of: placing the tea-seed oil in a refrigerator of -80 to -20 DEG C for 8-24 hours, adding an organic solvent the weight of which is 10 to 20 times that of the tea-seed oil into the tea-seed oil, and stirring at 0-10 DEG C for 0.5-2 hours; filtering the resulting solution, recycling the solvent from the filtrating solution at reduced pressure to obtain the tea-seed oil extract. The tea-seed oil extract soft capsule comprises the following raw materials in parts by weight: 70-93 parts of tea-seed oil extract, 1-10 parts of vitamin E, 5-2 0 parts of DHA (Docosahexaenoic Acid), and 1-10 parts of coenzyme Q10. The preparation method of the oft capsule comprises the following steps of: uniformly mixing, heating, preserving the temperature, cooling to room temperature, and preparing the soft capsule by taking gelatin and glycerin as capsule wall materials. The tea-seed oil extract disclosed by the invention is enriched in effective ingredients and is suitable for being directly taken without cooking; and the tea-seed oil extract, the DHA, the vitamin E and the coenzyme Q10 are combined rationally, so that a synergetic effect and a physiological equilibrium effect are reached, stability is improved, in-vivo oxidation resistance is promoted, in-vivo free radicals are effectively eliminated, and physical function is improved.
Description
Technical field
The present invention relates to healthcare field, particularly a kind of there is anti-aging effects tea-seed oil extract and soft capsule and preparation method.
Background technology
Aging is a kind of naturally physiological phenomenon, because disease, environment, diet and habits and customs etc. cause old and feeble acceleration to be then a kind of morbid state.Doctor trained in Western medicine adopts the drug therapy such as hormone to delay senility, but aging is a kind of physiology and pathological change of complexity, is difficult to reach antidotal object with the chemicals of single target spot, and likely forms dependence and toxic and side effect.
In order to delay senility, people attempt various " tonic " and retain youthful vitality.For negative and positive of qi and blood virtual loss, reinforcing method can be adopted, but the stagnation of the circulation of vital energy based on real example, blood stasis, phlegm are wet is then advisable with catharsis.Long-term sub-health state causes hyperlipemia, hypertension, atherosclerotic, and unsound life style and the too tired gastrointestinal dysfunction that causes and endocrinopathy, is accelerate old and feeble key factor.These belong to the real example of the traditional Chinese medical science, should not adopt reinforcing method.
Modern medicine is thought, old and feeble close with Relationship between Free Radical.Remove interior free yl composition and can play anti-aging effects.Numerous food product and Chinese medicine, all contain effect of the outer free radical composition of purged body, but absorption difference, interior free yl elimination effect is bad.
Tea-seed oil be from xylophyta tea seed be extract grease, there is the effects such as lipopenicillinase, defaecation, adjustment gastrointestinal function, at present as edible oil, can long-term safety use.Containing the composition such as polyunsaturated fatty acid and Tea Polyphenols in tea-seed oil, be easily absorbed by the body, again there is effect of scavenging radical, thus possess senile-resistant efficacy.But the content of above-mentioned active ingredient is not high in tea-seed oil, needs to carry out richness and gather.Poly-with the principle active component richness in tea-seed oil, in conjunction with auxiliary element, be prepared into antidotal health product, have no report at present.
Summary of the invention
The object of the present invention is to provide a kind of tea-seed oil extract and soft capsule thereof and preparation method.
For achieving the above object, the present invention is by the following technical solutions:
Tea-seed oil is placed in-80 to-20 DEG C of refrigerators to place 8 to 24 hours, adds the organic solvent of tea-seed oil 10 to 20 times by weight, stir 0.5 to 2 hour at 0 to 10 DEG C; Filter, filtrate decompression recycling design, obtains tea-seed oil extract.
With the soft capsule that tea-seed oil extract is raw material, be made up of by weight ratio following raw material: tea-seed oil extract is 70-93, vitamin E is 1-10, DHA is 5-20, Co-Q10 is 1-10.
With the soft capsule that tea-seed oil extract is raw material, each raw material by weight preferred proportioning is: tea-seed oil extract is 80, vitamin E is 2, DHA 15, Co-Q10 are 3.
The preparation method of tea-seed oil extract soft capsule comprises the following steps successively: take formula material in described ratio, and mixing, and is heated to 50 to 60 DEG C, is incubated 1 to 3 hour, is cooled to room temperature, with gelatin and glycerine for capsule material, makes soft capsule.
Described organic solvent is ethanol or acetone.
Colouring agent or the opacifier of capsule material weight ratio 0.01-0.1% can be added in described capsule material.
Beneficial effect of the present invention is:
Camellia seed oil has obvious regulating action to gastrointestinal function, and tea-seed oil is after freezing and solvent extraction, and its content of highly unsaturated fatty acids can bring up to more than 15% by original 7%; Tea Polyphenols brings up to 10 mcg/ml by 1 mcg/ml, and effect strengthens further, and is suitable for directly eating something rare, and avoids unrighted acid to destroy because of heating;
DHA has significant protective effect to nerve cell; vitamin E has significant protective effect to immunocyte; ubiquinone then has significant protective effect to cardiac muscle cell; camellia seed oil passes through coordinating intestines and stomach; the absorption to DHA can be increased; improve the action effect of DHA, unrighted acid and vitamin E, Co-Q10 are liposoluble constituent, can enter in cell.By tea-seed oil extract, DHA, vitamin E and Co-Q10 reasonable compatibility, the effect of synergistic function, physiological equilibrium and raising stability can be played, play interior antioxidation action, effectively remove interior free yl, improve physical function;
Through observing for 100 example ages at 45 to 70 years old ages sub-health population, wherein man 57 example, female 43 example, soft capsule of the present invention is taken for patient, every day 2 times, each 2, take 1 month continuously, the symptoms such as constipation, fatigue, night sweat, soreness and weakness of waist and knees are all clearly better.
Below in conjunction with embodiment, the present invention is described in further detail.
Detailed description of the invention
Tea-seed oil is placed in-80 to-20 DEG C of refrigerators to place 8 to 24 hours, adds ethanol or the acetone of tea-seed oil 10 to 20 times by weight, stir 0.5 to 2 hour at 0 to 10 DEG C; Filter, filtrate decompression recycling design, obtains tea-seed oil extract.Extracting tea seed oil extract is 70-93 by weight ratio, vitamin E is 1-10, DHA is 5-20, Co-Q10 is 1-10, mixing, and is heated to 50 to 60 DEG C, is incubated 1 to 3 hour, is cooled to room temperature, with gelatin and glycerine for capsule material, makes soft capsule.Colouring agent or the opacifier of capsule material weight ratio 0.01-0.1% can be added in capsule material.
Embodiment 1
Formulation by weight forms: tea-seed oil extract 80, vitamin E 2, DHA 15, Co-Q10 3
10kg tea-seed oil is placed in-80 DEG C of refrigerators to place 8 hours; Add 100kg acetone, 0 DEG C is stirred 1 hour; Filter, filtrate decompression recycling design, obtains tea-seed oil extract 2.4kg; Add vitamin E 0.06kg, DHA0.45kg, Co-Q10 0.09kg, mixing, and be heated to 60 DEG C, be incubated 2 hours; Be cooled to room temperature, with gelatin and glycerine for capsule material, make soft capsule with capsule machine.
Embodiment 2
Formulation by weight forms: tea-seed oil extract 93, vitamin E 1, DHA 5, Co-Q10 5
10kg tea-seed oil is placed in-60 DEG C of refrigerators to place 12 hours; Add 200kg ethanol, 5 DEG C are stirred 0.5 hour; Filter, filtrate decompression recycling design, obtains tea-seed oil extract 4.65kg; Add vitamin E 0.05kg, DHA0.25kg, Co-Q10 0.05kg, mixing, and be heated to 50 DEG C, be incubated 1 hour; Be cooled to room temperature, with gelatin and glycerine for capsule material (including quality 0.1% carmine pigment), make soft capsule with capsule machine.
Embodiment 3
Formulation by weight forms: tea-seed oil extract 70, vitamin E 5, DHA 20, Co-Q10 5
10kg tea-seed oil is placed in-40 DEG C of refrigerators to place 16 hours; Add 150kg acetone, 10 DEG C are stirred 2 hours; Filter, filtrate decompression recycling design, obtains tea-seed oil extract 2.8kg; Add vitamin E 0.2kg, DHA0.8kg, Co-Q10 0.2kg, mixing, and be heated to 60 DEG C, be incubated 3 hours; Be cooled to room temperature, with gelatin and glycerine for capsule material (including quality 0.01% titanium dioxide), make soft capsule with capsule machine.
Embodiment 4
Formulation by weight forms: tea-seed oil extract 70, vitamin e1 0, DHA10, Co-Q10
10kg tea-seed oil is placed in-20 DEG C of refrigerators to place 24 hours; Add 100kg ethanol, 0 DEG C is stirred 2 hours; Filter, filtrate decompression recycling design, obtains tea-seed oil extract 2.1kg; Add vitamin E 0.3kg, DHA0.3kg, Co-Q10 0.3kg, mixing, and be heated to 60 DEG C, be incubated 3 hours; Be cooled to room temperature, with gelatin and glycerine for capsule material (including quality 0.05% lemon yellow), make soft capsule with capsule machine.
Embodiment 5
Formulation by weight forms: tea-seed oil extract 80, vitamin E 3, DHA 10, Co-Q10 7
10kg tea-seed oil is placed in-60 DEG C of refrigerators to place 16 hours; Add 200kg acetone, 5 DEG C are stirred 1.5 hours; Filter, filtrate decompression recycling design, obtains tea-seed oil extract 4kg; Add vitamin E 0.15kg, DHA0.5kg, Co-Q10 0.35kg, mixing, and be heated to 50 DEG C, be incubated 2 hours; Be cooled to room temperature, with gelatin and glycerine for capsule material (including quality 0.03% titanium dioxide), make soft capsule with capsule machine.
Embodiment 6
Formulation by weight forms: tea-seed oil extract 85, vitamin E 2, DHA 8, Co-Q10 5
10kg tea-seed oil is placed in-80 DEG C of refrigerators to place 12 hours; Add 150kg ethanol, 10 DEG C are stirred 1 hour; Filter, filtrate decompression recycling design, obtains tea-seed oil extract 2.55kg; Add vitamin E 0.06kg, DHA0.24kg, Co-Q10 0.15kg, mixing, and be heated to 50 DEG C, be incubated 2 hours; Be cooled to room temperature, with gelatin and glycerine for capsule material, make soft capsule with capsule machine.
Claims (3)
1. a preparation method for tea-seed oil extract, is characterized in that: tea-seed oil is placed in-80 to-20 DEG C of refrigerators and places 8 to 24 hours, add ethanol or the acetone of tea-seed oil 10 to 20 times by weight, stir 0.5 to 2 hour at 0 to 10 DEG C; Filter, filtrate decompression recycling design, obtains tea-seed oil extract.
2. an anti-ageing tea-seed oil soft capsule, is characterized in that being made up of the raw material of following weight portion: the tea-seed oil extract that as claimed in claim 1 prepared by preparation method is 70-93, vitamin E is 1-10, DHA is 5-20, Co-Q10 is 1-10.
3.
anti-ageing tea-seed oil soft capsule according to claim 2, is characterized in that: the weight portion of each raw material is: tea-seed oil extract is 80, vitamin E is 2, DHA 15, Co-Q10 are 3.
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| CN201310229656.6A CN103283869B (en) | 2013-06-09 | 2013-06-09 | Tea-seed oil extract and soft capsule as well as preparation methods thereof |
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| CN201310229656.6A CN103283869B (en) | 2013-06-09 | 2013-06-09 | Tea-seed oil extract and soft capsule as well as preparation methods thereof |
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| CN103283869A CN103283869A (en) | 2013-09-11 |
| CN103283869B true CN103283869B (en) | 2015-03-18 |
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| CN106864785A (en) * | 2017-02-28 | 2017-06-20 | 深圳市金田创新科技有限公司 | A kind of packaging eating method of portable camellia oil/tea seed oil |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1709337A (en) * | 2005-06-21 | 2005-12-21 | 蒋伟哲 | Tea-seed oil soft capsule formulation |
| CN101575628A (en) * | 2008-07-01 | 2009-11-11 | 南昌大学 | Method for preparing tea polysaccharide through separation and purification and structural identification thereof |
| CN101810336A (en) * | 2010-04-30 | 2010-08-25 | 广东仙乐制药有限公司 | Chewable soft capsules and method for preparing same |
| CN101845362A (en) * | 2010-06-22 | 2010-09-29 | 中南林业科技大学 | Method for gathering oleic acid from tea-seed oil |
| CN102965187A (en) * | 2012-11-06 | 2013-03-13 | 安徽新世界绿洲茶油有限公司 | Method for preparing tea seed oil in low-temperature cold pressing manner |
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2013
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1709337A (en) * | 2005-06-21 | 2005-12-21 | 蒋伟哲 | Tea-seed oil soft capsule formulation |
| CN101575628A (en) * | 2008-07-01 | 2009-11-11 | 南昌大学 | Method for preparing tea polysaccharide through separation and purification and structural identification thereof |
| CN101810336A (en) * | 2010-04-30 | 2010-08-25 | 广东仙乐制药有限公司 | Chewable soft capsules and method for preparing same |
| CN101845362A (en) * | 2010-06-22 | 2010-09-29 | 中南林业科技大学 | Method for gathering oleic acid from tea-seed oil |
| CN102965187A (en) * | 2012-11-06 | 2013-03-13 | 安徽新世界绿洲茶油有限公司 | Method for preparing tea seed oil in low-temperature cold pressing manner |
Non-Patent Citations (1)
| Title |
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| 郭华等.茶籽油的脂肪酸组成测定.《中国油脂》.2008,第33卷(第7期),71-73. * |
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