CN103432026A - Hydrolat containing calendula petals and preparation method of hydrolat - Google Patents

Hydrolat containing calendula petals and preparation method of hydrolat Download PDF

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Publication number
CN103432026A
CN103432026A CN2013103290872A CN201310329087A CN103432026A CN 103432026 A CN103432026 A CN 103432026A CN 2013103290872 A CN2013103290872 A CN 2013103290872A CN 201310329087 A CN201310329087 A CN 201310329087A CN 103432026 A CN103432026 A CN 103432026A
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petal
flos inulae
deionized water
hydrosol
added
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CN2013103290872A
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CN103432026B (en
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康向群
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Abstract

The embodiment of the invention discloses hydrolat containing calendula petals, which comprises the following raw materials by weight percentage: 76-85% of deionized water, 0.05-0.2% of calendula petals, 1-3% of oat glucan, 1-3% of collagen extracting solution, 0.05-0.2% of dipotassium glycyrrhizinate, 1-3% of purslane extracting solution, 12-14% of humectant, and 0.5-0.6% of preservative. The embodiment of the invention further provides a preparation method of the hydrolat containing the calendula petals. The preparation method comprises the steps that the deionized water is added to an emulsification pot; a carbomer U20 is added slowly, dispersed well, and heated to 80-85 DEG C; propylene glycol and hyaluronic acid are mixed uniformly, added to the emulsification pot, and dispersed well; 1,3-butylene glycol, methylparaben, lubrajel and lubrajel oil are added in sequence; the temperature is kept constant at 80-85 DEG C; cooling is started after a period of time; the temperature is dropped; the rest of raw materials are added in sequence; sampling inspection is conducted; filtering and discharging are conducted after the sampling inspection is qualified; a pH value is controlled to be 5.5-6.5; and the treated calendula petals are added and mixed uniformly. According to the hydrolat and the preparation method, the calendula petals serve as the main raw materials for producing the hydrolat, so that a using effect is good, a production technology is simple and easy to operate, and the production efficiency is high.

Description

Hydrosol that contains the Flos Inulae petal and preparation method thereof
Technical field
The present invention relates to the hydrosol field, relate in particular to a kind of hydrosol that contains the Flos Inulae petal and preparation method thereof.
Background technology
Hydrosol is a kind of cosmetics of transparent liquid, spread upon the surface of skin, be used for cleaning the health of skin, maintenance skin, the requisite articles for use of the daily beauty and skin care of people, Flos Inulae is the name Calendula officinalis also, and its nature and flavor are light flat, and flower, leaf have antiinflammatory, antibacterial action, Flos Inulae, containing abundant vitamin A, can prevent pigementation, promotes skin gloss and elasticity, delaying senility, avoid the lax wrinkle of giving birth to of skin.
Summary of the invention
Embodiment of the present invention technical problem to be solved is, provides a kind of result of use better to contain the hydrosol of Flos Inulae petal.
The described hydrosol that contains the Flos Inulae petal, it is characterized in that, comprise by weight percentage deionized water 76%-85%, Flos Inulae petal 0.05%-0.2%, oat beta-glucan 1%-3%, collagen protein extracting solution 1%-3%, glycyrrhizic acid dipotassium 0.05%-0.2%, Herba Portulacae extract 1%-3%, wetting agent 12%-14%, antiseptic 0.5%-0.6%.
Described wetting agent mainly comprises: 1,3 butylene glycol, propylene glycol, hyaluronic acid, reed fragrant plant glue and reed fragrant plant oil.
Described antiseptic mainly comprises: methyl hydroxybenzoate and germall BP.
Comprise by weight percentage: 0.15% carbomer U20,4%1,3-butanediol, 3% propylene glycol, 0.08% hyaluronic acid, 0.15% methyl hydroxybenzoate, 3% reed fragrant plant glue, 3% reed fragrant plant oil, 2% oat beta-glucan, 2% collagen protein extracting solution, 0.1% glycyrrhizic acid dipotassium, 2% Herba Portulacae extract, 0.15% triethanolamine, 0.1% Flos Inulae petal, 0.4% germall BP, 0.02% essence, 0.06% polysorbas20,0.0001% pigment, all the other are deionized water.
The embodiment of the present invention also provides a kind of preparation method of simple to operate, the hydrosol that contains the Flos Inulae petal that production efficiency is high;
The preparation method of the described hydrosol that contains the Flos Inulae petal, comprise the steps:
(1) by the required tool of production and emulsifying pot, clean up, disinfect standby;
(2) deionized water is added to the emulsifying pot, more slowly add carbomer U20 scattered, be heated to 80~85 ℃;
(3) propylene glycol, hyaluronic acid are stirred evenly and add the emulsifying pot scattered, then add successively 1,3 butylene glycol, methyl hydroxybenzoate, reed fragrant plant glue, reed fragrant plant oil, 80~85 ℃ of constant temperature, opened and cool after a period of time;
(4), by greenhouse cooling, add successively oat beta-glucan, collagen protein extracting solution, good glycyrrhizic acid dipotassium, Herba Portulacae extract, triethanolamine, germall BP, pigment and essence, the polysorbas20 stirred in advance with deionized water dissolving in advance;
(5) pick test, qualified rear filtration discharging, control pH value 5.5~6.5;
(6) add the Flos Inulae petal of handling well, stir.
Described step (3) a period of time is 30 minutes, and described step cools the temperature to 45 degree in (4), and in described step (5), the pick test temperature is 40 degree.
The processing method of Flos Inulae petal is in described step (6): petal is added in the deionized water boiled of 50 times of petal weight and soak 30min, pick up petal, outwell water, then add in the deionized water boiled of 50 times of petal weight and soak 30min, picking up petal can be standby.
Implement the embodiment of the present invention, there is following beneficial effect:
The embodiment of the present invention adopts the Flos Inulae petal as the main material production hydrosol, Flos Inulae, containing abundant vitamin A, can prevent pigementation, promotes skin gloss and elasticity, delaying senility, avoid the lax wrinkle of giving birth to of skin, and result of use is good, and production technology is simple to operation, production efficiency is high.
The specific embodiment
For making the purpose, technical solutions and advantages of the present invention clearer, below the present invention is described in further detail.
The hydrosol that the embodiment of the present invention contains the Flos Inulae petal, concrete formula is as follows:
Sequence number Material name Percentage ratio Effect Remarks
1 Carbomer U20 0.15 The suspension thickening agent ?
2 Deionized water 82.00 Solvent ?
3 1,3 butylene glycol 4.00 Wetting agent ?
4 Propylene glycol 3.00 Wetting agent ?
5 Hyaluronic acid 0.08 Wetting agent ?
6 Methyl hydroxybenzoate 0.15 Antiseptic ?
7 Reed fragrant plant glue 3.00 Wetting agent ?
8 Reed fragrant plant oil 3.00 Wetting agent ?
9 Oat beta-glucan 2.00 Reparation, moisturizing ?
10 The collagen protein extracting solution 2.00 Nutrient ?
11 Glycyrrhizic acid dipotassium 0.10 Antiallergic ?
12 Deionized water 1.00 Solvent ?
13 Herba Portulacae extract 2.00 Moisturizing, antiallergic ?
14 Triethanolamine 0.15 Nertralizer ?
15 The Flos Inulae petal 0.10 Under effect is shown in Processing method is shown in technique
16 Germall BP 0.40 Antiseptic ?
17 Essence 0.02 Compose fragrant ?
18 Polysorbas20 0.06 Solubilizing agent ?
19 Pigment 0.0001 Modify outward appearance ?
Production technology and requirement
The preparation method of the hydrosol that contains the Flos Inulae petal, comprise the steps:
(1) by the required tool of production and emulsifying pot, clean up, disinfect standby;
(2) deionized water is added to the emulsifying pot, more slowly add carbomer U20 scattered, be heated to 80~85 ℃;
(3) propylene glycol, hyaluronic acid are stirred evenly and add the emulsifying pot scattered, then add successively 1,3 butylene glycol, methyl hydroxybenzoate, reed fragrant plant glue, reed fragrant plant oil, 80~85 ℃ of constant temperature, opened and cool after 30 minutes;
(4) cool the temperature to 45 degree, add successively oat beta-glucan, collagen protein extracting solution, good glycyrrhizic acid dipotassium, Herba Portulacae extract, triethanolamine, germall BP, pigment and essence, the polysorbas20 stirred in advance with deionized water dissolving in advance;
(5) pick test when 40 spend, qualified rear filtration discharging, control pH value 5.5~6.5;
(6) add the Flos Inulae petal of handling well, stir.
The processing method of Flos Inulae petal is in step (6): petal is added in the deionized water boiled of 50 times of petal weight and soak 30min, pick up petal, outwell water, then add in the deionized water boiled of 50 times of petal weight and soak 30min, picking up petal can be standby.
The technology of the present invention can keep petal to be suspended in uniformly in product, can not cause petal to sink and floating limiting the use of in the phase, keeps perfect visual effect.
The embodiment of the present invention adopts the Flos Inulae petal as the main material production hydrosol, Flos Inulae, containing abundant vitamin A, can prevent pigementation, promotes skin gloss and elasticity, delaying senility, avoid the lax wrinkle of giving birth to of skin, and result of use is good, and production technology is simple to operation, production efficiency is high.
Above disclosed is only a kind of preferred embodiment of the present invention, certainly can not limit with this interest field of the present invention, and the equivalent variations of therefore doing according to the claims in the present invention, still belong to the scope that the present invention is contained.

Claims (7)

1. a hydrosol that contains the Flos Inulae petal, it is characterized in that, comprise by weight percentage deionized water 76%-85%, Flos Inulae petal 0.05%-0.2%, oat beta-glucan 1%-3%, collagen protein extracting solution 1%-3%, glycyrrhizic acid dipotassium 0.05%-0.2%, Herba Portulacae extract 1%-3%, wetting agent 12%-14%, antiseptic 0.5%-0.6%.
2. the hydrosol that contains the Flos Inulae petal according to claim 1, is characterized in that, described wetting agent mainly comprises: 1,3 butylene glycol, propylene glycol, hyaluronic acid, reed fragrant plant glue and reed fragrant plant oil.
3. the hydrosol that contains the Flos Inulae petal according to claim 1, is characterized in that, described antiseptic mainly comprises: methyl hydroxybenzoate and germall BP.
4. the hydrosol that contains the Flos Inulae petal according to claim 1, it is characterized in that, comprise by weight percentage: 0.15% carbomer U20,4%1,3-butanediol, 3% propylene glycol, 0.08% hyaluronic acid, 0.15% methyl hydroxybenzoate, 3% reed fragrant plant glue, 3% reed fragrant plant oil, 2% oat beta-glucan, 2% collagen protein extracting solution, 0.1% glycyrrhizic acid dipotassium, 2% Herba Portulacae extract, 0.15% triethanolamine, 0.1% Flos Inulae petal, 0.4% germall BP, 0.02% essence, 0.06% polysorbas20,0.0001% pigment, all the other are deionized water.
5. according to the described preparation method that contains Flos Inulae petal hydrosol of any one in claim 1-4, it is characterized in that, comprise the steps:
(1) by the required tool of production and emulsifying pot, clean up, disinfect standby;
(2) deionized water is added to the emulsifying pot, more slowly add carbomer U20 scattered, be heated to 80~85 ℃;
(3) propylene glycol, hyaluronic acid are stirred evenly and add the emulsifying pot scattered, then add successively 1,3 butylene glycol, methyl hydroxybenzoate, reed fragrant plant glue, reed fragrant plant oil, 80~85 ℃ of constant temperature, opened and cool after a period of time;
(4), by greenhouse cooling, add successively oat beta-glucan, collagen protein extracting solution, good glycyrrhizic acid dipotassium, Herba Portulacae extract, triethanolamine, germall BP, pigment and essence, the polysorbas20 stirred in advance with deionized water dissolving in advance;
(5) pick test, qualified rear filtration discharging, control pH value 5.5~6.5;
(6) add the Flos Inulae petal of handling well, stir.
6. the preparation method that contains Flos Inulae petal hydrosol according to claim 5, is characterized in that, described step (3) a period of time is 30 minutes, and described step cools the temperature to 45 degree in (4), and in described step (5), the pick test temperature is 40 degree.
7. the preparation method that contains Flos Inulae petal hydrosol according to claim 5, it is characterized in that, the processing method of Flos Inulae petal is in described step (6): petal is added in the deionized water boiled of 50 times of petal weight and soak 30min, pick up petal, outwell water, add in the deionized water boiled of 50 times of petal weight again and soak 30min, picking up petal can be standby.
CN201310329087.2A 2013-07-31 2013-07-31 Hydrolat containing calendula petals and preparation method of hydrolat Expired - Fee Related CN103432026B (en)

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Cited By (5)

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CN103735457A (en) * 2013-12-25 2014-04-23 金奇集团金奇日化有限公司 Toner containing herbal components and preparation method thereof
CN104224635A (en) * 2014-09-30 2014-12-24 澳宝化妆品(惠州)有限公司 Preparation method and application of calendula extract
CN104739705A (en) * 2013-12-30 2015-07-01 谢铁强 Four-molecular weights hyaluronic acid stock solution and preparation method thereof
CN109431959A (en) * 2018-12-29 2019-03-08 大连民族大学 A kind of facial mask and preparation method thereof containing pot marigold extracting solution
CN111904905A (en) * 2020-08-04 2020-11-10 广东鑫美鑫化妆品有限公司 A cosmetic lotion containing marigold petal and multiple plant extracts

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103735457A (en) * 2013-12-25 2014-04-23 金奇集团金奇日化有限公司 Toner containing herbal components and preparation method thereof
CN103735457B (en) * 2013-12-25 2017-01-11 广东金奇精化股份有限公司 Toner containing herbal components and preparation method thereof
CN104739705A (en) * 2013-12-30 2015-07-01 谢铁强 Four-molecular weights hyaluronic acid stock solution and preparation method thereof
CN104224635A (en) * 2014-09-30 2014-12-24 澳宝化妆品(惠州)有限公司 Preparation method and application of calendula extract
CN109431959A (en) * 2018-12-29 2019-03-08 大连民族大学 A kind of facial mask and preparation method thereof containing pot marigold extracting solution
CN111904905A (en) * 2020-08-04 2020-11-10 广东鑫美鑫化妆品有限公司 A cosmetic lotion containing marigold petal and multiple plant extracts

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