CN104224635A - Preparation method and application of calendula extract - Google Patents
Preparation method and application of calendula extract Download PDFInfo
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- CN104224635A CN104224635A CN201410517417.5A CN201410517417A CN104224635A CN 104224635 A CN104224635 A CN 104224635A CN 201410517417 A CN201410517417 A CN 201410517417A CN 104224635 A CN104224635 A CN 104224635A
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- flos inulae
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Abstract
The invention belongs to the field of daily chemicals and in particular relates to a preparation method and application of calendula extract. The preparation method comprises the following steps: mixing calendula with 50%-70% alcohol, performing tissue crushing, filtering by a membrane to obtain liquid, distilling in a distiller to obtain a concentrated material, and separating the concentrated material in an oil-water separator to obtain the calendula extract. Lip cream comprises the following components in parts by mass: 25-45.0 parts of a bonder, 30.0-50.0 parts of a moisturizing agent, 0.5-2 parts of an antioxidant, 5-10 parts of a conditioner and 0.2-2 parts of the calendula extract prepared by the method. Due to the addition of the calendula extract, the lip cream has the effects of repairing and healing cracked or dry molted lip, diminishing inflammation, stopping bleeding and the like, and can effectively aim at the phenomena of molting, dry crack, bleeding and the like of the lip caused by dry climate and high sand wind in autumn and winter.
Description
Technical field
The invention belongs to household chemicals field, be specifically related to a kind of preparation method and the application of this extract in lip gloss of Flos Inulae extract.
Background technology
Flos Inulae has another name called Calendula officinalis, and it is rich in multivitamin, especially vitamin A and vitamin C; Almost each position can eat; Its petal has the function of beauty treatment, and flower is containing carotenoid, lycopene, violaxanthin, rubixanthin, volatile oil, resin, lymphatic temperament, malic acid etc.Root contains amaroid, mountain gold east glycol; Seed is containing glyceride, ceryl alcohol and alkaloid.Calendula officinalis nature and flavor are light flat, and flower, leaf have antiinflammatory, antibacterial action.Root energy promoting flow of QI and blood, flower can removing heat from blood, hemostasis.The Europe outer various inflammation for skin, mucosa among the people, also can the various inflammation of orally taken for curing and ulcer.Fresh flowers can be placed in salad and eat.Flos Inulae is rich in flavonoid active component, and this composition has antioxidation, antiangiogenic, antiinflammatory, anti-allergy and antiviral effect.
The preparation method of Flos Inulae extract in the past, adopts supercritical extraction and solvent method is used in combination or a kind of way of distillation of single use, and this method productive rate is low, somewhat expensive, and solvent contamination is large, is difficult to industrialization.Along with the development of society, people more and more focus on the protection of environment, pay close attention to low-carbon environment-friendly, pay close attention to the saving of production cost, therefore explore a kind of productivity ratio high, low cost, add solvent few, environmental protection, and can the method for heavy industrialization quite urgent.
Modern study shows, lip is dry and cracked is due to lip skin natural moisture preserving structure disequilibrium, and especially in autumn and winter season, main cause is that autumn and winter dry, dust storm is large, and loses moisture content in a large number, and in skin corium, moisture content can not get supplementing timely and causes; Along with the development of society, a lot of people substantially wants for a long time facing to computer or be in the environment of dry air-conditioned room for a long time, and the more slim children of lip skin is thin, lip is easy to be burnt by computer radiate or lose moisture content, and causes dry and cracked decortication; Dietary habit, monophagia, drinking-water is few, insomnia, causes vitamin B2 in human body, vitamin A intake not enough, can not get supplementing timely; Dry skin, self behavior causes dry and cracked hemorrhage.
Find through investigation, especially in autumn and winter season, main cause is that the autumn and winter are dry, dust storm is large, there is the dry and cracked phenomenon such as hemorrhage of lip decortication in increasing people, in view of Flos Inulae oil has so good moisturizing to lip skin, the effects such as maintenance healing, and lip gloss is moisturizing on the market, there is not maintenance healing breach or dry decortication lip, the Flos Inulae oil lip gloss that the lip gloss of anti-inflammation hemostasia and content are very large, so the application of Flos Inulae extract in lip gloss holds out broad prospects, the lip gloss of what a kind of quality stability was superior comprise golden small cup extract, one surely fast open ward off lip pomade new markets! just conventional extracting method step is complicated, and production capacity is lower.
Summary of the invention
It is high that the technical problem to be solved in the present invention is to provide a kind of productivity ratio, low cost, add solvent few, environmental protection, and can large-scale industrial production Flos Inulae extract method, the Flos Inulae extract that the method is extracted can apply in lip gloss, and lip gloss can be made to have effect of maintenance healing breach or dry decortication lip concurrently.
Technical problem to be solved by this invention is achieved by the following technical programs:
A preparation method for Flos Inulae extract, this preparation method comprises the following steps:
A () is collected Flos Inulae and is positioned in pulverizer cylinder body, add concentration be 50 ~ 70% ethanol mix with Flos Inulae, carry out historrhexis 1 ~ 4 time with the rotating speed of 8000-15000 r/min, each 5 ~ 30 minutes, then standing 2 ~ 8 hours; Obtain mixed liquor.
B mixed liquor membrane filtration that step (a) obtains by (), obtains feed liquid;
C feed liquid that step (b) obtains by () is positioned in distillator distills, and obtains concentrate; Concrete distillating method and step are the common practise of this area, therefore do not repeat.
D concentrate is placed in oil water separator and is separated by (), obtain Flos Inulae extract.
Further, the film described in step (b) is one in fibrous membrane, polysulfone membrane, polyvinylidene chlorida film or inoranic membrane or two kinds.
A kind of lip gloss, includes the component of following mass fraction:
The binding agent of 25 ~ 45.0 parts;
The moisturizing agent of 30.0 ~ 50.0 parts;
The antioxidant of 0.5 ~ 2 part;
The conditioner of 5 ~ 10 parts;
The Flos Inulae extract prepared by said method of 0.2 ~ 2 part.
Further, described binding agent is selected from polyethylene, Brazil wax, cetostearyl alcohol, Cera Flava, candelilla wax, synthetic wax, ceresine, paraffin, one or more in microwax.
Further, described moisturizing agent is selected from lanoline, synthesis squalane, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, shea butter, Jojoba oil, macadamia oil, 1.2-pentanediol, caprylic/capric triglyceride, white mineral oil, hydrogenation gathers certain herbaceous plants with big flowers alkene, octyldodecanol, one or more in Oleum Helianthi.
Further, described antioxidant is at least one in Vitamin E acetate Flos Carthami oil.
Further, described conditioner is plant sterol, synthetic fat, aloe, one or more in Flos Inulae oil.
Also can insert mass fraction in described component is the essence additive of 0.5 ~ 2.0 part and the antiseptic of 0 ~ 1 part.The common practise inserted as this area of spice and antiseptic, therefore do not repeat.
Compared with prior art, tool of the present invention has the following advantages:
1. in the present invention, the preparation method productivity ratio of Flos Inulae extract is high, low cost, and add solvent few, only have ethanol, in the Flos Inulae extract finally obtained, impurity is less, ensure that extract applies to the safety of cosmetics.
2. contain Flos Inulae extract in lip gloss of the present invention, the lip gloss originally only with moisture-keeping efficacy is made to have maintenance healing breach or dry effect such as decortication lip, anti-inflammation hemostasia etc. concurrently, can effectively dry for the autumn and winter, dust storm large, and there is the dry and cracked phenomenon such as hemorrhage of lip decortication in the increasing crowd caused.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, and the preparation method of wherein said Flos Inulae extract comprises the following steps:
A () is collected Flos Inulae and is positioned in pulverizer cylinder body, add concentration be 67% ethanol mix with Flos Inulae, carry out historrhexis 3 times with the rotating speed of 12000 r/min, each 20 minutes, then standing 6 hours, obtain mixed liquor.
Ceramic membrane combination in b mixed liquor fibrous membrane that step (a) obtains by () and inoranic membrane is filtered, and obtains feed liquid.
C feed liquid that step (b) obtains by () is placed in distillator, utilizes vacuum distillation method, obtains concentrate.
D concentrate is placed in oil water separator and is separated by (), obtain Flos Inulae extract.
A kind of lip gloss, includes the component of following mass fraction:
The binding agent of 25 ~ 45 parts; The moisturizing agent of 30 ~ 50 parts; The antioxidant of 0.5 ~ 2 part; The conditioner of 5 ~ 10 parts; The Flos Inulae extract prepared by said method of 0.2 ~ 2 part.
Described binding agent is selected from polyethylene, Brazil wax, cetostearyl alcohol, Cera Flava, candelilla wax, synthetic wax, ceresine, paraffin, one or more in microwax.Preferably wherein five kinds of binding agent collocation use, to reach optimum thickening effect.
Described moisturizing agent is selected from lanoline, synthesis squalane, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, shea butter, Jojoba oil, macadamia oil, 1.2-pentanediol, caprylic/capric triglyceride, white mineral oil, hydrogenation gathers certain herbaceous plants with big flowers alkene, octyldodecanol, one or more in Oleum Helianthi, preferably wherein more than at least 3 kinds wetting agents collocation use, to reach better moisturizing effect.
Antioxidant selects the collocation of Vitamin E acetate Flos Carthami oil to use.
Described conditioner preferred plant sterol, synthetic fat, aloe, in Flos Inulae oil at least two kinds used in combination.
Also can insert mass fraction in above component is the essence additive of 0.5 ~ 2.0 part and the antiseptic of 0 ~ 1 part.The common practise inserted as this area of spice and antiseptic, therefore do not repeat.
The synthetic method of this application is conventional configuration and hybrid technology, does not elaborate at this.
This application to be further described below in conjunction with embodiment for the ease of it will be appreciated by those skilled in the art that.Embodiment is only the preferred implementation of this application, is not the restriction to this application.
Table 1 is embodiment 1-3 component and mass fraction:
Choose above-described embodiment enforcement product try out to random 30 consumers and evaluate, (each embodiment 10 people tries out).
Table 2 consumer is to the evaluation score of embodiment 1-3 effect.
Note: the assessment result that consumer evaluation obtains: 10 points best, and 0 point the poorest.
Assessment result shows that the lip gloss of this application Flos Inulae extract can bring good experience effect to consumer.
Table 3 is that 10 consumers use embodiment 1 product after one week, lip to be nourished to the evaluation result of repairing effect.
Assessment result shows, the lip gloss that this application contains Flos Inulae extract has extraordinary nourishing repairing effect to lip.
Table 4 is that 10 consumers use embodiment 1 product after one week, lip water to be moistened to the evaluation result of moistening effect.
Assessment result shows, the lip gloss that this application contains Flos Inulae extract can show extraordinary water profit moistening effect to lip.
Table 5 is that 10 consumers use embodiment 1 product after one week to the evaluation result of maintenance healing effect.
Assessment result shows, the lip gloss of this application Flos Inulae extract can show the effect of extraordinary maintenance healing to lip.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; change, the modification done under other any does not deviate from spirit of the present invention and principle, substitute, combine, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (7)
1. a preparation method for Flos Inulae extract, is characterized in that: described preparation method comprises the following steps:
A () is collected Flos Inulae and is positioned in pulverizer cylinder body, add concentration be 50 ~ 70% ethanol mix with Flos Inulae, carry out historrhexis 1 ~ 4 time with the rotating speed of 8000-15000 r/min, each 5 ~ 30 minutes, then standing 2 ~ 8 hours; Obtain mixed liquor;
B mixed liquor membrane filtration that step (a) obtains by (), obtains feed liquid;
C feed liquid that step (b) obtains by () is positioned in distillator distills, and obtains concentrate;
D concentrate is placed in oil water separator and is separated by (), obtain Flos Inulae extract.
2. the preparation method of a kind of Flos Inulae extract according to claim 1, is characterized in that: the film described in step (b) is one in fibrous membrane, polysulfone membrane, polyvinylidene chlorida film or inoranic membrane or two kinds.
3. a lip gloss, is characterized in that the component including following mass fraction:
The binding agent of 25 ~ 45.0 parts;
The moisturizing agent of 30.0 ~ 50.0 parts;
The antioxidant of 0.5 ~ 2 part;
The conditioner of 5 ~ 10 parts;
The Flos Inulae extract prepared by power 1 method of 0.2 ~ 2 part.
4. a kind of lip gloss according to claim 3, is characterized in that: described binding agent is selected from polyethylene, Brazil wax, cetostearyl alcohol, Cera Flava, candelilla wax, synthetic wax, ceresine, paraffin, one or more in microwax.
5. a kind of lip gloss according to claim 3, is characterized in that: described moisturizing agent is selected from lanoline, synthesis squalane, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, shea butter, Jojoba oil, macadamia oil, 1.2-pentanediol, caprylic/capric triglyceride, white mineral oil, hydrogenation gathers certain herbaceous plants with big flowers alkene, octyldodecanol, one or more in Oleum Helianthi.
6. a kind of lip gloss according to claim 3, is characterized in that: described antioxidant is at least one in Vitamin E acetate Flos Carthami oil.
7. a kind of lip gloss according to claim 3, is characterized in that: described conditioner is plant sterol, synthetic fat, aloe, one or more in Flos Inulae oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410517417.5A CN104224635A (en) | 2014-09-30 | 2014-09-30 | Preparation method and application of calendula extract |
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| CN201410517417.5A CN104224635A (en) | 2014-09-30 | 2014-09-30 | Preparation method and application of calendula extract |
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| CN104224635A true CN104224635A (en) | 2014-12-24 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107789316A (en) * | 2017-12-07 | 2018-03-13 | 广州赛莱拉干细胞科技股份有限公司 | A kind of moisturizing antioxidant composition of extract of stem cell containing pot marigold and its application |
| CN108653076A (en) * | 2018-05-31 | 2018-10-16 | 李应峰 | A kind of production method of herbal medicine shower cream |
| CN111991322A (en) * | 2020-08-26 | 2020-11-27 | 湖南神农国油生态农业发展有限公司 | Multifunctional anti-wrinkle beauty mask and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107789316A (en) * | 2017-12-07 | 2018-03-13 | 广州赛莱拉干细胞科技股份有限公司 | A kind of moisturizing antioxidant composition of extract of stem cell containing pot marigold and its application |
| CN108653076A (en) * | 2018-05-31 | 2018-10-16 | 李应峰 | A kind of production method of herbal medicine shower cream |
| CN111991322A (en) * | 2020-08-26 | 2020-11-27 | 湖南神农国油生态农业发展有限公司 | Multifunctional anti-wrinkle beauty mask and preparation method thereof |
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Application publication date: 20141224 |
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