CN103417443A - Oleum menthae toothpaste - Google Patents
Oleum menthae toothpaste Download PDFInfo
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- CN103417443A CN103417443A CN201310374713XA CN201310374713A CN103417443A CN 103417443 A CN103417443 A CN 103417443A CN 201310374713X A CN201310374713X A CN 201310374713XA CN 201310374713 A CN201310374713 A CN 201310374713A CN 103417443 A CN103417443 A CN 103417443A
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- China
- Prior art keywords
- toothpaste
- oleum menthae
- whitening agent
- sorbitol
- lauroyl
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Abstract
The invention relates to oleum menthae toothpaste. The oleum menthae toothpaste is composed of the following constituents, by weight, 0.5-1.5% of oleum menthae, 20-30% of magnesium carbonate, 20-30% of calcium carbonate, 14-18% of sorbitol, 1-2% of sodium alginate, 2-3% of lauroyl amphoteric sodium malonate and the balance of water. The oleum menthae toothpaste can nurse the oral cavity comprehensively, protect health of the oral cavity and teeth, and give out fragrance like that of refreshing mint, and is good in taste.
Description
Technical field
The present invention relates to a kind of toothpaste, be specifically related to a kind of Oleum menthae toothpaste.
Background technology
Toothpaste is to be used from cleaning teeth with toothbrush one, and the protection oral hygiene, to a kind of daily necessities of human-body safety.Along with the raising of people's living standard, to the also progressively raising of quality requirement of toothpaste.At aspect of performance General Requirements toothpaste: (1) can remove the thin film of dental surface and bacterial plaque and not damage enamel and dentin; (2) there is good cleaning oral cavity and effect on every side thereof; (3) avirulence, non-stimulated to oral mucosa; (4) comfortable fragrance and taste are arranged, cool and sweet-smelling sensation is arranged after use.
Summary of the invention
For above shortcomings in prior art, technical problem to be solved by this invention is to provide a kind of Oleum menthae toothpaste.
The present invention seeks to be achieved through the following technical solutions:
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: the 0.5-1.5% Oleum menthae, and the 20-30% magnesium carbonate, the 20-30% calcium carbonate, the 14-18% sorbitol, the 1-2% sodium alginate, 2-3% lauroyl both sexes base disodium beclomethasone, surplus is water.
Preferably,
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: the 0.5-1.5% Oleum menthae, and the 20-30% magnesium carbonate, the 20-30% calcium carbonate, the 14-18% sorbitol, the 1-2% sodium alginate, 2-3% lauroyl both sexes base disodium beclomethasone, the 1-3% whitening agent, surplus is water.
Described whitening agent is a kind of or its mixture in sodium phytate, aloin, glycyrrhizin and glucoseoxidase.
Best, described whitening agent consists of by weight following component: 40-60 part sodium phytate, 10-20 part aloin, 10-20 part glycyrrhizin and 15-25 part glucoseoxidase.
In the present invention,
Sodium phytate, English name: Sodium phytate, CAS accession number: 14306-25-3.
Aloin, English name: Aloin, CAS accession number: 5133-19-7.
Glycyrrhizin, English name: Glycyrrhizic acid, CAS accession number: 1405-86-3.
Glucoseoxidase, No. CAS: 9001-37-0, name of commodity in English: EC1.1.3.4, EINECS:232-601-0.
Compared with prior art, Oleum menthae toothpaste energy total care of the present invention oral cavity, protection oral cavity and dental health, and there is refrigerant minty note, special mouthfeel is good.
The specific embodiment
Embodiment 1
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: 1% Oleum menthae, and 25% magnesium carbonate, 25% calcium carbonate, 16% sorbitol, 1.5% sodium alginate, 2.5% lauroyl both sexes base disodium beclomethasone, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of aloins, 15 parts of glycyrrhizins and 20 parts of glucoseoxidases.
Oleum menthae toothpaste of the present invention can adopt the conventional method preparation of this area fully, as " detergent compositions workshop manual ", (Xu Baocai etc. write, Chemical Industry Press, chemistry and applied chemistry publishing centre, January in 2006 the 1st edition) the disclosed toothpaste production technology of 594-597 page is prepared.Concrete, the preparation method of the present embodiment Oleum menthae toothpaste is: after the above-mentioned raw materials component is weighed, disperse in pre-dispersed still, mix, open cream still vacuum pump processed and suck above-mentioned liquid material, then open scraper, agitator and colloid mill, close colloid mill, agitator and scraper successively after 50 minutes, vacuum breaker, obtain Oleum menthae toothpaste.
Obviously, the preparation method of toothpaste is prior art in the present invention, does not have special character, and main improvement of the present invention just is the difference of formula.
Embodiment 2
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: 1% Oleum menthae, and 25% magnesium carbonate, 25% calcium carbonate, 16% sorbitol, 1.5% sodium alginate, 2.5% lauroyl both sexes base disodium beclomethasone, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of aloins and 20 parts of glucoseoxidases.
According to the preparation method of embodiment 1, obtain the Oleum menthae toothpaste of embodiment 2.
Embodiment 3
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: 1% Oleum menthae, and 25% magnesium carbonate, 25% calcium carbonate, 16% sorbitol, 1.5% sodium alginate, 2.5% lauroyl both sexes base disodium beclomethasone, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of glycyrrhizins and 20 parts of glucoseoxidases.
According to the preparation method of embodiment 1, obtain the Oleum menthae toothpaste of embodiment 3.
Embodiment 4
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: 1% Oleum menthae, and 25% magnesium carbonate, 25% calcium carbonate, 16% sorbitol, 1.5% sodium alginate, 2.5% lauroyl both sexes base disodium beclomethasone, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 50 parts of sodium phytates, 15 parts of aloins and 15 parts of glycyrrhizins.
According to the preparation method of embodiment 1, obtain the Oleum menthae toothpaste of embodiment 4.
Embodiment 5
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: 1% Oleum menthae, and 25% magnesium carbonate, 25% calcium carbonate, 16% sorbitol, 1.5% sodium alginate, 2.5% lauroyl both sexes base disodium beclomethasone, 2% whitening agent, surplus is water.
Described whitening agent consists of by weight following component: 15 parts of aloins, 15 parts of glycyrrhizins and 20 parts of glucoseoxidases.
According to the preparation method of embodiment 1, obtain the Oleum menthae toothpaste of embodiment 5.
Embodiment 6
A kind of Oleum menthae toothpaste is comprised of following compositions in weight percentage: 1% Oleum menthae, and 25% magnesium carbonate, 25% calcium carbonate, 16% sorbitol, 1.5% sodium alginate, 2.5% lauroyl both sexes base disodium beclomethasone, surplus is water.
According to the preparation method of embodiment 1, obtain the Oleum menthae toothpaste of embodiment 6.
Test case
48 adult men and women are divided into to 6 groups, use embodiment 1-5 toothpaste, every day, each was brushed once sooner or later, to reaching the mottle index LSI of use after 3 months continuously before using, tested respectively, method of testing and scoring rule are permitted first 5th～6 pages of 1.4.1 of master thesis " a kind of clinical efficacy evaluation study of novel whitening toothpaste " of son referring to Shanghai Communications University.
The LSI scoring method, concrete scoring rule is as follows:
0 minute-without mottle, exist;
1 minute-mottle size is no more than 1/3 of facing; Degree is slight mottle (yellow or yellowish-brown);
2 minutes-mottle size is no more than 2/3 of facing; Degree is moderate mottle (moderate brown);
3 minutes-mottle size is greater than 2/3 of facing; Degree is severe mottle (dark-brown or black).
LSI value after the statistics experimenter uses front LSI value and uses March, LSI meansigma methods after calculating the front LSI meansigma methods of use and using March, then calculate mottle index LSI rate of descent, the results are shown in Table 1.
Table 1: mottle index LSI test chart
| ? | Mottle index LSI rate of descent, % |
| Embodiment 1 | 27.6 |
| Embodiment 2 | 26.4 |
| Embodiment 3 | 26.2 |
| Embodiment 4 | 21.6 |
| Embodiment 5 | 20.4 |
| Embodiment 6 | 12.1 |
Mottle index LSI rate of descent (%)=[LSI meansigma methods before using-uses is the LSI meansigma methods after March]/use front LSI meansigma methods * 100%.
As seen from the data in Table 1, using embodiment 1-5 toothpaste after 3 months, the obvious decline of LSI value, toothpaste of the present invention has whitening effect preferably.
Claims (4)
1. an Oleum menthae toothpaste, is characterized in that, following compositions in weight percentage, consists of: the 0.5-1.5% Oleum menthae, the 20-30% magnesium carbonate, 20-30% calcium carbonate, 14-18% sorbitol, the 1-2% sodium alginate, 2-3% lauroyl both sexes base disodium beclomethasone, surplus is water.
2. an Oleum menthae toothpaste, is characterized in that, following compositions in weight percentage, consists of: 0.5-1.5% Oleum menthae, 20-30% magnesium carbonate, the 20-30% calcium carbonate, 14-18% sorbitol, 1-2% sodium alginate, 2-3% lauroyl both sexes base disodium beclomethasone, the 1-3% whitening agent, surplus is water.
3. Oleum menthae toothpaste as claimed in claim 2, it is characterized in that: described whitening agent is a kind of or its mixture in sodium phytate, aloin, glycyrrhizin and glucoseoxidase.
4. Oleum menthae toothpaste as claimed in claim 3, is characterized in that, described whitening agent consists of by weight following component: 40-60 part sodium phytate, 10-20 part aloin, 10-20 part glycyrrhizin and 15-25 part glucoseoxidase.
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| CN201310374713.XA CN103417443B (en) | 2013-08-24 | 2013-08-24 | Oleum menthae toothpaste |
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| CN201310374713.XA CN103417443B (en) | 2013-08-24 | 2013-08-24 | Oleum menthae toothpaste |
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| CN103417443A true CN103417443A (en) | 2013-12-04 |
| CN103417443B CN103417443B (en) | 2016-02-03 |
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| CN201310374713.XA Active CN103417443B (en) | 2013-08-24 | 2013-08-24 | Oleum menthae toothpaste |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105769623A (en) * | 2016-05-20 | 2016-07-20 | 海门市东大能源科技有限公司 | Toothpaste for children |
| CN105997720A (en) * | 2016-07-09 | 2016-10-12 | 青岛大学 | Skin whitening toothpaste |
| CN107787217A (en) * | 2015-06-12 | 2018-03-09 | 宝洁公司 | Perfume composition and application thereof |
| CN107811919A (en) * | 2017-11-27 | 2018-03-20 | 钱卫萍 | A kind of toothpaste |
| CN110538117A (en) * | 2019-10-18 | 2019-12-06 | 上海中医药大学 | Condensed toothpaste formula |
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| CN101890118A (en) * | 2010-07-21 | 2010-11-24 | 曾华林 | Smoking cessation pure natural plant tobacco substituting extract, product thereof and preparation method thereof |
| CN102614090A (en) * | 2012-04-24 | 2012-08-01 | 苏州维蒂卡科技有限公司 | Toothpaste composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101890118A (en) * | 2010-07-21 | 2010-11-24 | 曾华林 | Smoking cessation pure natural plant tobacco substituting extract, product thereof and preparation method thereof |
| CN102614090A (en) * | 2012-04-24 | 2012-08-01 | 苏州维蒂卡科技有限公司 | Toothpaste composition |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107787217A (en) * | 2015-06-12 | 2018-03-09 | 宝洁公司 | Perfume composition and application thereof |
| CN105769623A (en) * | 2016-05-20 | 2016-07-20 | 海门市东大能源科技有限公司 | Toothpaste for children |
| CN105997720A (en) * | 2016-07-09 | 2016-10-12 | 青岛大学 | Skin whitening toothpaste |
| CN105997720B (en) * | 2016-07-09 | 2019-01-29 | 青岛大学 | A kind of whitening toothpaste |
| CN107811919A (en) * | 2017-11-27 | 2018-03-20 | 钱卫萍 | A kind of toothpaste |
| CN110538117A (en) * | 2019-10-18 | 2019-12-06 | 上海中医药大学 | Condensed toothpaste formula |
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| Publication number | Publication date |
|---|---|
| CN103417443B (en) | 2016-02-03 |
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Inventor after: Wang Baiqiao Inventor before: Song Fanhua |
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Effective date of registration: 20170627 Address after: 510540, 18 South Industrial Park, Taihe Town, Baiyun District, Guangdong, Guangzhou Patentee after: Guangzhou still Cosmetics Manufacturing Co., Ltd. Address before: 201107 Shanghai city Minhang District Minhang Road 88 Lane No. 1-30 building twenty-second room T159 Patentee before: Shanghai Fangmu Fine Chemical Co., Ltd. |