CN103393565B - Lauroyl lysine silky shampoo - Google Patents
Lauroyl lysine silky shampoo Download PDFInfo
- Publication number
- CN103393565B CN103393565B CN201310307555.6A CN201310307555A CN103393565B CN 103393565 B CN103393565 B CN 103393565B CN 201310307555 A CN201310307555 A CN 201310307555A CN 103393565 B CN103393565 B CN 103393565B
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- CN
- China
- Prior art keywords
- shampoo
- lauroyl lysine
- silky
- antiseptic
- lysine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000002453 shampoo Substances 0.000 title claims abstract description 37
- GYDYJUYZBRGMCC-INIZCTEOSA-N (2s)-2-amino-6-(dodecanoylamino)hexanoic acid Chemical compound CCCCCCCCCCCC(=O)NCCCC[C@H](N)C(O)=O GYDYJUYZBRGMCC-INIZCTEOSA-N 0.000 title claims abstract description 31
- ZKWJQNCOTNUNMF-QXMHVHEDSA-N 2-[dimethyl-[3-[[(z)-octadec-9-enoyl]amino]propyl]azaniumyl]acetate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O ZKWJQNCOTNUNMF-QXMHVHEDSA-N 0.000 claims abstract description 9
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 24
- 230000002421 anti-septic effect Effects 0.000 claims description 17
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- DNKGZSOYWMQDTK-UHFFFAOYSA-N 3-iodoprop-1-ynyl N-butylcarbamate Chemical compound CCCCNC(=O)OC#CCI DNKGZSOYWMQDTK-UHFFFAOYSA-N 0.000 claims description 10
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims description 10
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 10
- 235000013824 polyphenols Nutrition 0.000 claims description 10
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 9
- 239000004330 calcium propionate Substances 0.000 claims description 9
- 235000010331 calcium propionate Nutrition 0.000 claims description 9
- 239000004302 potassium sorbate Substances 0.000 claims description 9
- 235000010241 potassium sorbate Nutrition 0.000 claims description 9
- 229940069338 potassium sorbate Drugs 0.000 claims description 9
- 244000018633 Prunus armeniaca Species 0.000 claims description 8
- 235000009827 Prunus armeniaca Nutrition 0.000 claims description 8
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 8
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 8
- 235000011152 sodium sulphate Nutrition 0.000 claims description 8
- 244000269722 Thea sinensis Species 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 abstract description 2
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 abstract 1
- 235000011130 ammonium sulphate Nutrition 0.000 abstract 1
- 239000010477 apricot oil Substances 0.000 abstract 1
- 230000007797 corrosion Effects 0.000 abstract 1
- 238000005260 corrosion Methods 0.000 abstract 1
- 239000006260 foam Substances 0.000 abstract 1
- 229940051841 polyoxyethylene ether Drugs 0.000 abstract 1
- 229920000056 polyoxyethylene ether Polymers 0.000 abstract 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 239000003755 preservative agent Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 230000000813 microbial effect Effects 0.000 description 3
- 210000004761 scalp Anatomy 0.000 description 3
- 208000001840 Dandruff Diseases 0.000 description 2
- 201000004624 Dermatitis Diseases 0.000 description 2
- OPVLOHUACNWTQT-UHFFFAOYSA-N azane;2-dodecoxyethyl hydrogen sulfate Chemical compound N.CCCCCCCCCCCCOCCOS(O)(=O)=O OPVLOHUACNWTQT-UHFFFAOYSA-N 0.000 description 2
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 description 2
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 2
- 230000002147 killing effect Effects 0.000 description 2
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- JLHMJWHSBYZWJJ-UHFFFAOYSA-N 1,2-thiazole 1-oxide Chemical compound O=S1C=CC=N1 JLHMJWHSBYZWJJ-UHFFFAOYSA-N 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 description 1
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- ZCTXEAQXZGPWFG-UHFFFAOYSA-N imidurea Chemical compound O=C1NC(=O)N(CO)C1NC(=O)NCNC(=O)NC1C(=O)NC(=O)N1CO ZCTXEAQXZGPWFG-UHFFFAOYSA-N 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 1
- 229960002216 methylparaben Drugs 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- GYCKQBWUSACYIF-UHFFFAOYSA-N o-hydroxybenzoic acid ethyl ester Natural products CCOC(=O)C1=CC=CC=C1O GYCKQBWUSACYIF-UHFFFAOYSA-N 0.000 description 1
- CHHHXKFHOYLYRE-STWYSWDKSA-M potassium sorbate Chemical compound [K+].C\C=C\C=C\C([O-])=O CHHHXKFHOYLYRE-STWYSWDKSA-M 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a lauroyl lysine silky shampoo, which is composed of the following components by weight percent: 8-12% of lauryl polyoxyethylene ether ammonium sulfate, 2-4% of wild apricot oil oleamidopropyl betaine, 2-6% of propanediol, 0.4-0.6% of lauroyl lysine, 0.1-0.3% of corrosion remover and the balance of water. The lauroyl lysine silky shampoo disclosed by the invention has rich foam, enables the hair to be glossed, smooth, fine and soft like silk.
Description
Technical field
The present invention relates to a kind of shampoo, be specifically related to a kind of Lauroyl lysine silky shampoo.
Background technology
Shampoo is indispensable requisites in people's daily life, can remove greasy dirt and the scurf on surface, and have no adverse effects to hair, scalp and health of human body during use from hair and scalp.Shampoo is of a great variety, divides mainly contain transparent hair shampoo, paste shampoo, bead light shampoo, recuperating shampoo, scalp care hair shampoo, special shampoo etc. by dosage form and function.
In recent years, due to the raising of people's quality of the life, increasing of shampoos, it is also proposed increasing requirement to shampoo.Both needed shampoo to have the anti-dandruff effect of good decontamination, and needed again it to have good abnormal smells from the patient, and also needed the gloss keeping hair quality simultaneously, there is the longer shelf-life.
In order to extend the shelf-life of shampoo, its long-term placement after Kaifeng uses still is never degenerated, usual meeting adds a certain amount of antiseptic in shampoo, but the efficient antiseptic that shampoo at present is on the market conventional has methyl parahydroxybenzoate (i.e. methyl hydroxybenzoate), ethylparaben (i.e. ethyl hydroxybenzoate), sodium benzoate, isothiazolone etc., they have certain zest to skin and eyes, with eye contact after, need to rinse with a large amount of clear water immediately; Even can cause part population skin allergy, the symptom such as dermatitis occurs, therefore its consumption in shampoo is also subject to strict control.
In addition, imidazolidinyl urea and in uride be all as formaldehyde donor as the principle of antiseptic, reached the effect of killing microorganisms by release formaldehyde, also can cause damage to human body skin when release formaldehyde exceeds standard, all strictly limit its content in a lot of country and even prohibit the use.
Summary of the invention
For above shortcomings in prior art, one of technical problem to be solved by this invention provides a kind of Lauroyl lysine silky shampoo.
The present invention seeks to be achieved through the following technical solutions:
A kind of Lauroyl lysine silky shampoo, is made up of following compositions in weight percentage: lauryl polyethenoxy ether sodium sulfate 8-12%, wild apricot oleamidopropyl betaine 2-4%, propylene glycol 2-6%, lauroyl lysine 0.4-0.6%, antiseptic 0.1-0.2%, surplus is water.
Preferably,
Described antiseptic is made up of by weight following component: tea polyphenols 10-15 part, potassium sorbate 10-15 part, calcium propionate 10-15 part, butyl carbamic acid iodopropynyl ester 5-10 part.
In the present invention,
Lauryl polyethenoxy ether sodium sulfate, English name: Ammonium lauryl ether sulfate, No. CAS: 32612-48-9.
Wild apricot oleamidopropyl betaine, No. CAS: 133934-08-4.
Propylene glycol, No. CAS: 26264-14-2.
Lauroyl lysine, CAS accession number: 52315-75-0.
Tea polyphenols, Tea Polyphenols, No. CAS: 84650-60-2.
Potassium sorbate, CAS:24634-61-5.
Calcium propionate, No. CAS: 4075-81-4.
Butyl carbamic acid iodopropynyl ester, No. CAS: 55406-53-6.
Lauroyl lysine silky shampoo of the present invention, foaming abundancy, order increases hair gloss, smooth exquisiteness, as fine as silk.Lauroyl lysine silky shampoo of the present invention, selects the antiseptic that the compatibility of tea polyphenols, potassium sorbate, calcium propionate and butyl carbamic acid iodopropynyl ester is made, but there is good Synergistic kill effect and security performance.
Detailed description of the invention
Embodiment further illustrates of the present invention below, instead of limit the scope of the invention.In the present invention, if no special instructions, each raw material all in working substance content for 100%.
Embodiment 1
A kind of Lauroyl lysine silky shampoo, is made up of following compositions in weight percentage: lauryl polyethenoxy ether sodium sulfate 10%, wild apricot oleamidopropyl betaine 3%, propylene glycol 4%, lauroyl lysine 0.5%, antiseptic 0.2%, surplus is water.
Foregoing preservatives, is made up of by weight following component: tea polyphenols 10 parts, potassium sorbate 10 parts, calcium propionate 10 parts, butyl carbamic acid iodopropynyl ester 10 parts.Tea polyphenols, potassium sorbate, calcium propionate and butyl carbamic acid iodopropynyl ester are uniformly mixed, namely can be made into mixing antiseptic.
Get appropriate water, be heated to 80-90 DEG C, in whipping process, add lauryl polyethenoxy ether sodium sulfate and wild apricot oleamidopropyl betaine in described ratio, after stirring, reduce temperature to 50-60 DEG C, add propylene glycol, lauroyl lysine and mixing antiseptic, stir after 1.5 hours, be cooled to room temperature, obtain Lauroyl lysine silky shampoo.
Embodiment 2
A kind of Lauroyl lysine silky shampoo, is made up of following compositions in weight percentage: lauryl polyethenoxy ether sodium sulfate 10%, wild apricot oleamidopropyl betaine 3%, propylene glycol 4%, lauroyl lysine 0.5%, antiseptic 0.2%, surplus is water.
Foregoing preservatives, is made up of by weight following component: potassium sorbate 20 parts, calcium propionate 10 parts, butyl carbamic acid iodopropynyl ester 10 parts.
Be prepared by the method for embodiment 1, obtain Lauroyl lysine silky shampoo.
Embodiment 3
A kind of Lauroyl lysine silky shampoo, is made up of following compositions in weight percentage: lauryl polyethenoxy ether sodium sulfate 10%, wild apricot oleamidopropyl betaine 3%, propylene glycol 4%, lauroyl lysine 0.5%, antiseptic 0.2%, surplus is water.
Foregoing preservatives, is made up of by weight following component: tea polyphenols 10 parts, calcium propionate 20 parts, butyl carbamic acid iodopropynyl ester 10 parts.
Be prepared by the method for embodiment 1, obtain Lauroyl lysine silky shampoo.
Embodiment 4
A kind of Lauroyl lysine silky shampoo, is made up of following compositions in weight percentage: lauryl polyethenoxy ether sodium sulfate 10%, wild apricot oleamidopropyl betaine 3%, propylene glycol 4%, lauroyl lysine 0.5%, antiseptic 0.2%, surplus is water.
Foregoing preservatives, is made up of by weight following component: tea polyphenols 20 parts, potassium sorbate 10 parts, butyl carbamic acid iodopropynyl ester 10 parts.
Be prepared by the method for embodiment 1, obtain Lauroyl lysine silky shampoo.
Test case
The Lauroyl lysine silky shampoo of embodiment 1-4 is put into couveuse (40 DEG C, 95% humidity), place and carry out Microbial Challenge test in 28 days, select Hu Mei, " potentiation of formulation preservative for cosmetic " of Chen Yijun (" household chemicals science " the 29th volume the 12nd phase, in December, 2006) test strain of page 4 table 6, with reference to the evaluation criterion of document 2.3.2.3, when Microbial Challenge tests 0 day, the initial strains concentration of mixed cell and mixing mycete is 5 × 10
5cfu/g (ml).
Table 1: Microbial Challenge result of the test (cfu/g (ml))
From table 1 result, the Lauroyl lysine silky shampoo of embodiment 1 after 28 days in test, makes the bacterial strain concentration of mixed cell all be down to 10cfu/g (ml) below, proves that it has stronger inhibitory or killing effect to antibacterial.Antiseptic effect is obviously better than embodiment 2-4.
Therefore the antiseptic that the compatibility of tea polyphenols, potassium sorbate, calcium propionate and butyl carbamic acid iodopropynyl ester is made has been selected, but what have good Synergistic kills effect, the Lauroyl lysine silky shampoo that the present invention selects this antiseptic to make has good anti-corrosive properties and security performance simultaneously.
Claims (1)
1. a Lauroyl lysine silky shampoo, it is characterized in that, be made up of following compositions in weight percentage: lauryl polyethenoxy ether sodium sulfate 8-12%, wild apricot oleamidopropyl betaine 2-4%, propylene glycol 2-6%, lauroyl lysine 0.4-0.6%, antiseptic 0.1-0.2%, surplus is water;
Described antiseptic is made up of by weight following component: tea polyphenols 10-15 part, potassium sorbate 10-15 part, calcium propionate 10-15 part, butyl carbamic acid iodopropynyl ester 5-10 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310307555.6A CN103393565B (en) | 2013-07-20 | 2013-07-20 | Lauroyl lysine silky shampoo |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310307555.6A CN103393565B (en) | 2013-07-20 | 2013-07-20 | Lauroyl lysine silky shampoo |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103393565A CN103393565A (en) | 2013-11-20 |
| CN103393565B true CN103393565B (en) | 2015-03-11 |
Family
ID=49557435
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310307555.6A Active CN103393565B (en) | 2013-07-20 | 2013-07-20 | Lauroyl lysine silky shampoo |
Country Status (1)
| Country | Link |
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| CN (1) | CN103393565B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107648082B (en) * | 2017-10-20 | 2019-10-01 | 广州神采化妆品有限公司 | A kind of composition and its application with the sliding effect of dry and comfortable, silk |
| CN107822914B (en) * | 2017-11-29 | 2021-03-23 | 广州市万千粉丝化妆品有限公司 | Mild hair-care shampoo and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1557156A1 (en) * | 2003-12-23 | 2005-07-27 | Beiersdorf AG | Cosmetic hair-care composition comprising lauroyl lysine |
| WO2010026009A1 (en) * | 2008-09-06 | 2010-03-11 | Henkel Ag & Co. Kgaa | Hair treatment means |
-
2013
- 2013-07-20 CN CN201310307555.6A patent/CN103393565B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1557156A1 (en) * | 2003-12-23 | 2005-07-27 | Beiersdorf AG | Cosmetic hair-care composition comprising lauroyl lysine |
| WO2010026009A1 (en) * | 2008-09-06 | 2010-03-11 | Henkel Ag & Co. Kgaa | Hair treatment means |
Non-Patent Citations (1)
| Title |
|---|
| 《表4化妆品组分中限用防腐剂》;中华人民共和国卫生部;《化妆品卫生规范》;20070131;第72页 * |
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| Publication number | Publication date |
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| CN103393565A (en) | 2013-11-20 |
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| C53 | Correction of patent for invention or patent application | ||
| CB03 | Change of inventor or designer information |
Inventor after: Lv Xueming Inventor after: Wu Hao Inventor before: Chen Longdi |
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| COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: CHEN LONGDI TO: LV XUEMING WU HAO |
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| C14 | Grant of patent or utility model | ||
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| CB03 | Change of inventor or designer information |
Inventor after: Li Jing Inventor before: Lv Xueming Inventor before: Wu Hao |
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Effective date of registration: 20170322 Address after: 526060 Guangdong City, Zhaoqing province high tech Zone, one of the text of the text of the four street, one of the 1 Patentee after: ZHAOQING KAIJOE TECHNOLOGY CO., LTD. Address before: 201111 Shanghai city Minhang District Yuanjiang Road No. 5500 building first room E2128 Patentee before: Shanghai Yanzi Chemical Technology Co., Ltd. |