CN103385303A - Wheat germ milk tea drink and preparation method thereof - Google Patents
Wheat germ milk tea drink and preparation method thereof Download PDFInfo
- Publication number
- CN103385303A CN103385303A CN2013102588102A CN201310258810A CN103385303A CN 103385303 A CN103385303 A CN 103385303A CN 2013102588102 A CN2013102588102 A CN 2013102588102A CN 201310258810 A CN201310258810 A CN 201310258810A CN 103385303 A CN103385303 A CN 103385303A
- Authority
- CN
- China
- Prior art keywords
- wheat embryo
- powder
- parts
- ultramicro
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention belongs to the technical field of agricultural product processing, and particularly relates to a wheat germ milk tea drink and a preparation method thereof. The wheat germ milk tea drink comprises the following ingredients, by weight: 16 to 20 parts of ultrafine wheat germ powders, 7 to 9 parts of black tea powders, 9 to 11 parts of milk powders, 6 to 8 parts of white sugar, 0.4 to 0.6 parts of honey, 0.3 to 0.5 parts of citric acid, and 60 to 80 parts of water. The preparation method comprises the following steps: (1) preparation of the ultrafine wheat germ powders; (2) blending; (3) emulsification; (4) homogenization; (5) filtering; and (6) sterilization. The wheat germ milk tea drink is rich in nutrition, good in taste, beneficial to human health, free of food additives, easy to prepare, and low in costs.
Description
Technical field
The invention belongs to the technical field of processing of farm products, be specifically related to a kind of wheat embryo milk tea beverage and preparation method thereof.
Background technology
Wheat embryo claims again malt flour, plumule, golden yellow graininess, it is the organ of wheat germination and growth, account for 2.5% of whole wheat, due to high ash content, the color and luster of wheat embryo, be rich in fat and enzyme affects flower characters, in pulverizing process, plumule often is removed, major part is thrown away as leftover bits and pieces, small part is as feed, and China's wheat embryo annual production reaches two or three hundred ten thousand tons, has caused the very large waste of grain resource.
Wheat embryo contains the multiple nutrients material, and wheat plantule protein content is about 30%, belongs to full price albumen, and is suitable with the amino acid ligand ratio of beef, egg, is better than rice, zein.The wheat embryo oil content surpasses 10%, belongs to the plant fat acid lipid of high-quality, is rich in the multiple unrighted acids such as oleic acid, linoleic acid, leukotrienes, and content is about 84%.Wheat-germ oil is rich in vitamin E in addition, is 0.25%～0.55%, has the raising immunity of organisms, and the balance the body function, to anti-ageing and promote other hormone secretions etc. to have good curative effect.Wheat embryo contains mineral matter, phosphatide, senior carbene alcohol and some unknown micro-physiologically active ingredients in addition, and nutritive value accounts for 97% of whole wheat.In recent years, along with going deep into of research, the intensive processing of wheat embryo more and more receives publicity.
The beverage that contains wheat embryo in prior art all adopts the wheat embryo defibrination in preparation, can cause like this maximal destruction of nutritional labeling structure in wheat embryo and the maximum loss of active ingredient.
The food additives such as many sweeteners, emulsifying agent, thickener have been added at present in beverage, it is conditional using in standard GB/T 2760 for food additives at food additives, for example thickener in beverage consumption generally below 3/1000, these food additives also have certain influence to health, for example thickener is polysaccharose substance, consumption increases can affect patients with diabetes mellitus, and it is healthy that many foods can affect people's normal body.In addition, the increase of thickener consumption can affect sensory properties and the local flavor of product, as is applied to fruit drink, can cause the negative effects such as the product viscosity increases, mobility descends, transparency reduces, mouthfeel degenerates.
Summary of the invention
The object of the invention is to for the defect of above-mentioned existence and a kind of wheat embryo milk tea beverage and preparation method thereof is provided, this wheat embryo milk tea beverage is nutritious, excellent taste, be conducive to health, do not contain food additives, the preparation method is simple, and cost is low.
Technical scheme of the present invention is: a kind of wheat embryo milk tea beverage comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 16～20 parts;
Black tea powder: 7～9 parts;
Milk powder: 9～11 parts;
White sugar: 6～8 parts;
Honey: 0.4～0.6 part;
Citric acid: 0.3～0.5 part;
Water: 60～80 parts.
Described wheat embryo milk tea beverage comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 17～19 parts;
Black tea powder: 7.5～8.5 parts;
Milk powder: 9.5～10.5 parts;
White sugar: 6.5～7.5 parts;
Honey: 0.5～0.6 part;
Citric acid: 0.4～0.5 part;
Water: 70～80 parts.
Described wheat embryo milk tea beverage comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 20 parts;
Black tea powder: 8 parts;
Milk powder: 10 parts;
White sugar: 7 parts;
Honey: 0.6 part;
Citric acid: 0.5 part;
Water: 80 parts.
A kind of preparation method of described wheat embryo milk tea beverage comprises the following steps:
(1) preparation of wheat embryo Ultramicro-powder: a. stable state processing: at first selected wheat embryo is carried out under 100～105 ℃ of conditions the xeothermic enzyme 15～20 minutes of going out, then be cooled to room temperature;
B. ultramicro grinding: the wheat embryo that will be cooled to room temperature is positioned in micronizer and carries out ultramicro grinding, makes the wheat embryo Ultramicro-powder;
(2) allotment: by weight ratio wheat embryo Ultramicro-powder, black tea powder, milk powder, white sugar are added in mixer, stirred 6～8 minutes, mix, obtain mixed powder;
(3) emulsification: first water is added in mixed powder by weight ratio, and then adds honey, citric acid, be heated to 60～85 ℃, constantly stir, until form uniform emulsion;
(4) homogeneous: emulsion by high pressure homogenizer under 20-25MPa, 60-70 ℃ condition, homogeneous 2-3 time;
(5) filter: the emulsion of step (4) gained is filtered, remove large granular impurity;
(6) sterilizing: as after the emulsion after filtering carries out pasteurization, namely to obtain the wheat embryo milk tea beverage.
The wheat embryo Ultramicro-powder that makes in described step (1) b is 800～1000 orders.
In described step (2), the rotating speed of mixer is 15～20 rev/mins.
Filter in described step (5) and adopt the nylon drinking filter bag.
The preparation method of described wheat embryo milk tea beverage comprises the following steps:
(1) preparation of wheat embryo Ultramicro-powder: a. stable state processing: at first selected wheat embryo is carried out under 102 ℃ of conditions the xeothermic enzyme 16 minutes of going out, then be cooled to room temperature;
B. ultramicro grinding: the wheat embryo that will be cooled to room temperature is positioned in micronizer and carries out ultramicro grinding, makes the wheat embryo Ultramicro-powder;
(2) allotment: by weight ratio wheat embryo Ultramicro-powder, black tea powder, milk powder, white sugar are added in mixer, stirred 7 minutes, mix, obtain mixed powder;
(3) emulsification: first water is added in mixed powder by weight ratio, and then adds honey, citric acid, be heated to 70 ℃, constantly stir, until form uniform emulsion;
(4) homogeneous: emulsion by high pressure homogenizer under 20-25MPa, 60-70 ℃ condition, homogeneous 2-3 time;
(5) filter: the emulsion of step (4) gained is filtered, remove large granular impurity;
(6) sterilizing: as after the emulsion after filtering carries out pasteurization, namely to obtain the wheat embryo milk tea beverage.
beneficial effect of the present invention is: wheat embryo milk tea beverage of the present invention, what the materials of wheat plumule adopted is the wheat embryo Ultramicro-powder, the wheat embryo Ultramicro-powder has following advantage: in the situation that do not destroy its institutional framework, can make fineness up to 1000 orders, wheat embryo Ultramicro-powder specific area is large, porosity is high, pardon is strong, the look that keeps wheat embryo, fragrant, flavor, nutritional labeling, its inherent quality is fully improved, the original natural flavor of wheat embryo is able to further performance, wheat embryo is after ultramicro grinding, its particle diameter diminishes, it is more stable in liquid, obviously improve its dispersiveness and dissolubility, nutritional labeling more easily absorbs simultaneously.
Wheat embryo is after ultramicro grinding, cell membrane is destroyed, in emulsion process, the macromolecular substances such as grease, protein is distributed to water in the wheat embryo cell, because wheat-germ oil has stronger polarity and stickiness, and the germ protein of hydrophilic lipophilic class, add the gelling (emulsification is mainly united realization by this three kinds of effects) of plumule starch, make original immiscible grease, water connect together, be difficult for thoroughly separating, form stable emulsion.Again by high-pressure homogeneous, grain refine in namely making emulsion under the triple role that extruding, thump, decompression expand, make broken more tiny of fat in wheat-germ oil, with unclassified stores can more uniform mutual the mixing, thereby make whole emulsion system more stable.Wheat embryo contains starch, can be very thick after gelling.The present invention utilizes the emulsification of contained grease in the ultramicro grinding wheat germ powder, and the leisure milk tea beverage that exploitation enjoys the teenager to favor, have good market prospects.Thereby this method is considered exploitation wheat embryo milk tea, the added value of raising wheat embryo and nutritional utilization value.
The little yellow uniform liquid of wheat embryo milk tea beverage outward appearance of the present invention, the distinctive fragrance of wheat embryo, delicate mouthfeel, sour and sweet palatability, organize homogeneous without layering.Protein 〉=5%, VE 〉=50 mg/100 mL; 70 ° of T～85 ° T of acidity; Soluble solid 〉=9%; Stabilizing agents etc. meet the GB2760-1996 food additives and use sanitary standard; Content of beary metal is lower than national standard.Total number of bacteria≤250cfu/mL; Pathogenic bacteria must not detect.
The specific embodiment
Below by specific embodiment, the present invention is described in detail.
Embodiment 1
A kind of wheat embryo milk tea beverage comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 20 parts;
Black tea powder: 8 parts;
Milk powder: 10 parts;
White sugar: 7 parts;
Honey: 0.6 part;
Citric acid: 0.5 part;
Water: 80 parts.
The preparation method of described wheat embryo milk tea beverage comprises the following steps:
(1) preparation of wheat embryo Ultramicro-powder: a. stable state processing: at first selected wheat embryo is carried out under 102 ℃ of conditions the xeothermic enzyme 16 minutes of going out, then be cooled to room temperature;
B. ultramicro grinding: the wheat embryo that will be cooled to room temperature is positioned in micronizer and carries out ultramicro grinding, makes the wheat embryo Ultramicro-powder;
(2) allotment: by weight 7 parts of 20 parts of wheat embryo Ultramicro-powders, 8 parts of black tea powders, 10 parts of milk powder, white sugar are added in mixer, stirred 7 minutes, mix, obtain mixed powder;
(3) emulsification: first 80 parts of water are added in mixed powder by weight, and then add 0.6 part of honey, 0.5 part of citric acid, be heated to 70 ℃, constantly stir, until form uniform emulsion;
(4) homogeneous: emulsion by high pressure homogenizer under 20-25MPa, 60-70 ℃ condition, homogeneous 2-3 time;
(5) filter: the emulsion of step (4) gained is filtered, remove large granular impurity;
(6) sterilizing: as after the emulsion after filtering carries out pasteurization, namely to obtain the wheat embryo milk tea beverage.
The wheat embryo Ultramicro-powder that makes in described step (1) b is 900 orders.
In described step (2), the rotating speed of mixer is 20 rev/mins.
Filter in described step (5) and adopt the nylon drinking filter bag.
Embodiment 2
A kind of wheat embryo milk tea beverage comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 18 parts;
Black tea powder: 9 parts;
Milk powder: 10 parts;
White sugar: 7 parts;
Honey: 0.5 part;
Citric acid: 0.6 part;
Water: 75 parts.
The preparation method of described wheat embryo milk tea beverage comprises the following steps:
(1) preparation of wheat embryo Ultramicro-powder: a. stable state processing: at first selected wheat embryo is carried out under 104 ℃ of conditions the xeothermic enzyme 17 minutes of going out, then be cooled to room temperature;
B. ultramicro grinding: the wheat embryo that will be cooled to room temperature is positioned in micronizer and carries out ultramicro grinding, makes the wheat embryo Ultramicro-powder;
(2) allotment: by weight 7 parts of 18 parts of wheat embryo Ultramicro-powders, 9 parts of black tea powders, 10 parts of milk powder, white sugar are added in mixer, stirred 6 minutes, mix, obtain mixed powder;
(3) emulsification: first 75 parts of water are added in mixed powder by weight, and then add 0.5 part of honey, 0.6 part of citric acid, be heated to 80 ℃, constantly stir, until form uniform emulsion;
(4) homogeneous: emulsion by high pressure homogenizer under 20-25MPa, 60-70 ℃ condition, homogeneous 2-3 time;
(5) filter: the emulsion of step (4) gained is filtered, remove large granular impurity;
(6) sterilizing: as after the emulsion after filtering carries out pasteurization, namely to obtain the wheat embryo milk tea beverage.
The wheat embryo Ultramicro-powder that makes in described step (1) b is 850 orders.
In described step (2), the rotating speed of mixer is 16 rev/mins.
Filter in described step (5) and adopt the nylon drinking filter bag.
Claims (8)
1. a wheat embryo milk tea beverage, is characterized in that, comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 16～20 parts;
Black tea powder: 7～9 parts;
Milk powder: 9～11 parts;
White sugar: 6～8 parts;
Honey: 0.4～0.6 part;
Citric acid: 0.3～0.5 part;
Water: 60～80 parts.
2. wheat embryo milk tea beverage according to claim 1, is characterized in that, comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 17～19 parts;
Black tea powder: 7.5～8.5 parts;
Milk powder: 9.5～10.5 parts;
White sugar: 6.5～7.5 parts;
Honey: 0.5～0.6 part;
Citric acid: 0.4～0.5 part;
Water: 70～80 parts.
3. wheat embryo milk tea beverage according to claim 1, is characterized in that, comprises the raw material of following weight portion:
Wheat embryo Ultramicro-powder: 20 parts;
Black tea powder: 8 parts;
Milk powder: 10 parts;
White sugar: 7 parts;
Honey: 0.6 part;
Citric acid: 0.5 part;
Water: 80 parts.
4. the preparation method of the described wheat embryo milk tea beverage of claim 1 comprises the following steps:
(1) preparation of wheat embryo Ultramicro-powder: a. stable state processing: at first selected wheat embryo is carried out under 100～105 ℃ of conditions the xeothermic enzyme 15～20 minutes of going out, then be cooled to room temperature;
B. ultramicro grinding: the wheat embryo that will be cooled to room temperature is positioned in micronizer and carries out ultramicro grinding, makes the wheat embryo Ultramicro-powder;
(2) allotment: by weight ratio wheat embryo Ultramicro-powder, black tea powder, milk powder, white sugar are added in mixer, stirred 6～8 minutes, mix, obtain mixed powder;
(3) emulsification: first water is added in mixed powder by weight ratio, and then adds honey, citric acid, be heated to 60～85 ℃, constantly stir, until form uniform emulsion;
(4) homogeneous: emulsion by high pressure homogenizer under 20-25MPa, 60-70 ℃ condition, homogeneous 2-3 time;
(5) filter: the emulsion of step (4) gained is filtered, remove large granular impurity;
(6) sterilizing: as after the emulsion after filtering carries out pasteurization, namely to obtain the wheat embryo milk tea beverage.
5. the preparation method of wheat embryo milk tea beverage according to claim 4, is characterized in that, the wheat embryo Ultramicro-powder that makes in described step (1) b is 800～1000 orders.
6. the preparation method of wheat embryo milk tea beverage according to claim 4, is characterized in that, in described step (2), the rotating speed of mixer is 15～20 rev/mins.
7. the preparation method of wheat embryo milk tea beverage according to claim 4, is characterized in that, filters in described step (5) and adopt the nylon drinking filter bag.
8. the preparation method of wheat embryo milk tea beverage according to claim 4, is characterized in that, comprises the following steps:
(1) preparation of wheat embryo Ultramicro-powder: a. stable state processing: at first selected wheat embryo is carried out under 102 ℃ of conditions the xeothermic enzyme 16 minutes of going out, then be cooled to room temperature;
B. ultramicro grinding: the wheat embryo that will be cooled to room temperature is positioned in micronizer and carries out ultramicro grinding, makes the wheat embryo Ultramicro-powder;
(2) allotment: by weight ratio wheat embryo Ultramicro-powder, black tea powder, milk powder, white sugar are added in mixer, stirred 7 minutes, mix, obtain mixed powder;
(3) emulsification: first water is added in mixed powder by weight ratio, and then adds honey, citric acid, be heated to 70 ℃, constantly stir, until form uniform emulsion;
(4) homogeneous: emulsion by high pressure homogenizer under 20-25MPa, 60-70 ℃ condition, homogeneous 2-3 time;
(5) filter: the emulsion of step (4) gained is filtered, remove large granular impurity;
(6) sterilizing: as after the emulsion after filtering carries out pasteurization, namely to obtain the wheat embryo milk tea beverage.
?
?
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310258810.2A CN103385303B (en) | 2013-06-26 | 2013-06-26 | Wheat germ milk tea drink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310258810.2A CN103385303B (en) | 2013-06-26 | 2013-06-26 | Wheat germ milk tea drink and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103385303A true CN103385303A (en) | 2013-11-13 |
| CN103385303B CN103385303B (en) | 2015-07-15 |
Family
ID=49529864
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310258810.2A Active CN103385303B (en) | 2013-06-26 | 2013-06-26 | Wheat germ milk tea drink and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103385303B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104286318A (en) * | 2014-11-05 | 2015-01-21 | 合肥康龄养生科技有限公司 | Wheat germ acetic acid milk tea and preparation method thereof |
| CN105394293A (en) * | 2015-12-17 | 2016-03-16 | 阜南红洁食品有限公司 | Original-taste germ milk tea and preparation method thereof |
| CN105558053A (en) * | 2015-12-17 | 2016-05-11 | 阜南红洁食品有限公司 | Milk tea with germ and walnut kernels and preparation method thereof |
| CN105580940A (en) * | 2015-12-17 | 2016-05-18 | 阜南红洁食品有限公司 | Health-care germ milky tea and preparation method thereof |
| CN105594923A (en) * | 2015-12-17 | 2016-05-25 | 阜南红洁食品有限公司 | Germ sweetened bean paste milk tea and preparation method thereof |
| CN106720395A (en) * | 2017-01-06 | 2017-05-31 | 天津熹旺众创科技有限公司 | Water bar smears tea plumule cheese and preparation method thereof with without chemistry addition |
| CN107751502A (en) * | 2017-11-07 | 2018-03-06 | 蚌埠学院 | A kind of processing method of wheat germ tea |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101756337A (en) * | 2010-01-20 | 2010-06-30 | 贾巍 | Preparation method of corn germ drink |
| CN102132749A (en) * | 2011-03-24 | 2011-07-27 | 郑福 | Purple sweet potato milk tea and preparation method thereof |
-
2013
- 2013-06-26 CN CN201310258810.2A patent/CN103385303B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101756337A (en) * | 2010-01-20 | 2010-06-30 | 贾巍 | Preparation method of corn germ drink |
| CN102132749A (en) * | 2011-03-24 | 2011-07-27 | 郑福 | Purple sweet potato milk tea and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 席彦: "《小麦胚芽的开发利用》", 《江苏科技信息》, no. 9, 31 December 1997 (1997-12-31), pages 34 - 36 * |
| 陈存社: "《小麦胚芽深加工技术的研究》", 《食品工业科技》, vol. 25, no. 6, 31 December 2004 (2004-12-31), pages 139 - 141 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104286318A (en) * | 2014-11-05 | 2015-01-21 | 合肥康龄养生科技有限公司 | Wheat germ acetic acid milk tea and preparation method thereof |
| CN105394293A (en) * | 2015-12-17 | 2016-03-16 | 阜南红洁食品有限公司 | Original-taste germ milk tea and preparation method thereof |
| CN105558053A (en) * | 2015-12-17 | 2016-05-11 | 阜南红洁食品有限公司 | Milk tea with germ and walnut kernels and preparation method thereof |
| CN105580940A (en) * | 2015-12-17 | 2016-05-18 | 阜南红洁食品有限公司 | Health-care germ milky tea and preparation method thereof |
| CN105594923A (en) * | 2015-12-17 | 2016-05-25 | 阜南红洁食品有限公司 | Germ sweetened bean paste milk tea and preparation method thereof |
| CN106720395A (en) * | 2017-01-06 | 2017-05-31 | 天津熹旺众创科技有限公司 | Water bar smears tea plumule cheese and preparation method thereof with without chemistry addition |
| CN107751502A (en) * | 2017-11-07 | 2018-03-06 | 蚌埠学院 | A kind of processing method of wheat germ tea |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103385303B (en) | 2015-07-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103385303B (en) | Wheat germ milk tea drink and preparation method thereof | |
| CN102987490B (en) | Suaeda glauca wild vegetable juice and production method and application thereof | |
| KR101374424B1 (en) | Method for health food using rice bran and embryo and linseed | |
| CN103271160B (en) | Health preserving whole-cereal milk and preparation method thereof | |
| CN103750495B (en) | Production method of potato solid beverage | |
| CN102028034B (en) | Acid anti-oxidation liquid dairy product and preparation method thereof | |
| CN104855790B (en) | A kind of instant oats particles and preparation method thereof | |
| CN103271157B (en) | Health preserving cereal milk and preparation method thereof | |
| CN106234598A (en) | A kind of instant milk tea and preparation method thereof | |
| CN102771692A (en) | Probiotics-containing infant colorful nutritional rice flour and preparation technique thereof | |
| CN103271158B (en) | Health preserving cereal milk and preparation method thereof | |
| CN110178896A (en) | A kind of linseed fat reducing Yoghourt nutrition bar and its manufacturing method | |
| CN106070813A (en) | Green tea powder nourishing medicinal granule | |
| CN102342555A (en) | Wheat germ-sesame protein fermented beverage and preparation process thereof | |
| CN107397071A (en) | A kind of chicken feed addictive for improving meat | |
| KR101156002B1 (en) | Preparation method of rice-soybean milk typed sikhye | |
| CN106616152A (en) | Manufacturing method of tremella fermented solid beverage | |
| CN1559301A (en) | Rice beverage, and its prepn. method | |
| CN105875834A (en) | Ginkgo sour milk and preparation method | |
| CN103385300B (en) | Pite pear milk drink | |
| CN105341155A (en) | Pitaya and active lactic acid bacteria beverage and preparation method thereof | |
| CN104855525B (en) | A kind of production method of Moringa Walnut Milk | |
| KR100994196B1 (en) | Method of preparing fermented liquid of garlic and chonggugjang | |
| CN104982538B (en) | A kind of production method of maca Walnut Milk | |
| CN106107293A (en) | A kind of health-care food composition with weight losing function containing Armeniaca mume Sieb. |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |