CN103361209A - Fructus cnidii inflammation diminishing compound perfumed soap - Google Patents
Fructus cnidii inflammation diminishing compound perfumed soap Download PDFInfo
- Publication number
- CN103361209A CN103361209A CN2013101930431A CN201310193043A CN103361209A CN 103361209 A CN103361209 A CN 103361209A CN 2013101930431 A CN2013101930431 A CN 2013101930431A CN 201310193043 A CN201310193043 A CN 201310193043A CN 103361209 A CN103361209 A CN 103361209A
- Authority
- CN
- China
- Prior art keywords
- fructus cnidii
- parts
- soap
- sodium
- perfumed soap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- 206010061218 Inflammation Diseases 0.000 title abstract description 5
- 230000003467 diminishing effect Effects 0.000 title abstract 4
- 230000004054 inflammatory process Effects 0.000 title abstract 4
- 150000001875 compounds Chemical class 0.000 title abstract 3
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- -1 amino betaine Chemical compound 0.000 claims abstract description 8
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- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 description 1
- WHNXAQZPEBNFBC-UHFFFAOYSA-K trisodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(2-hydroxyethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].OCCN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O WHNXAQZPEBNFBC-UHFFFAOYSA-K 0.000 description 1
- FHGJYTNPLCNRLG-UHFFFAOYSA-K trisodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(2-hydroxyethyl)amino]acetate;hydrate Chemical compound O.[Na+].[Na+].[Na+].OCCN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O FHGJYTNPLCNRLG-UHFFFAOYSA-K 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
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Abstract
The invention discloses a fructus cnidii inflammation diminishing compound perfumed soap which is prepared from the following raw materials in parts by weight: 0.05-0.15 parts of a fructus cnidii extract, 15-25 parts of sodium cocoate, 50-70 parts of sodium palmitate, 3-5 parts of amino betaine cocoamphopropinate, 3-5 parts of disodium cocoamphodiacetate and 20 parts of water. The fructus cnidii inflammation diminishing compound perfumed soap disclosed by the invention is fine and stable in foam, mild in performance and low in irritation to skin, and can be used for diminishing inflammation and sterilizing after being especially added with the fructus cnidii extract.
Description
Technical field:
The present invention relates to a kind of perfumed soap, particularly a kind of Fructus Cnidii anti-inflammatory composite soap.
Background technology:
Perfumed soap (soap) is one of skin, hair washing and nursing article, is a kind of daily necessities.Perfumed soap is take sodium soap and other tensio-active agents as main raw material, adds quality improver and outward appearance modifying agent, through the product of making after the machine-shaping.
Perfumed soap is requisite washing and nursing article in the daily life, take sodium soap and other tensio-active agents as main raw material, adds quality improver and outward appearance modifying agent, through the product of making after the machine-shaping.The function of perfumed soap is the cleaning washing, be used in that yes above the skin and remove earth dirt, skin secretion, movement, chemical substance or bacterium etc., in today of stressing cosmetic result, makeup, skin care products or the medicine of removing skin surface also are one of its main purposes.
In the prior art, the many insights of perfumed soap are that fatty acid sodium salt is the Cake-shape soap of soap base, although have preferably cleaning force, whipability and easy washability, but not anti-hard water, can produce incrustation scale during washing, form the calcium magnesium soap, degreasing power is strong, the soap of human body life-time service meta-alkalescence can make skin feel dry and astringent, and excitement is arranged.
Fructus Cnidii, another name Daucus carota L. is samphire cnidium monnieri Cnidium monnieri(L.) dry mature fruit of Cuss..Summer, two season of autumn gather during fruit maturation, remove impurity, dry.Nature and flavor: warm in nature, flavor is hot, bitter.Function cures mainly: warming the kidney to invigorate YANG, eliminating dampness is dispeled the wind, desinsection.Be used for that impotence, palace are cold, under the cold-dampness band, the arthritis with fixed pain caused by dampness pain in the back; Control vulval eczema, married woman's pruritus vulvae, trichomonal vaginitis outward.
Chemical composition of Chinese materia medica: fruit contains volatile oil 1.3%, and main component is firpene (l-Pine-ne), amphene (l-Camphene), different one-tenth acid borneol acetate (Bornyl isovale-rate), isocamphol (Isoborneol).Contain again Osthole (Ostho-le), cnidimine (Cnidimine, be Edultin), different saxifrage case (IsoPiBrpinelline), bergapton, columbianetin (Dihydroo-roselol, Columbianetin) and angelate thereof (ColuInbianadin), acetic ester (o-Acetyl columbianetin); The mouth isopentanoate, cnidiadin (Cnidiadiu), isobutyl acyloxy o-acetylcolumbianetin.Root contains the cloudy element of cnidium monnieri, Isopimpinellin, alloimperatorin (Alloimperatorine), xanthotoxol (Xanthotoxol), ammidin (Imperatorine).Fruit contains volatile oil approximately 1.3%, and wherein principal constituent is 1 firpene (l-pinene), 1-amphene (l-camphene), isovaleric acid borneol acetate (bornylisovalerare) and 7-Osthole (osthole) etc.From the fruit alcohol extract, except obtaining the 7-Osthole, still obtain palmitinic acid (palmitic acid)), β-sitosterol, bergapten (bergapten), Isopimpinellin (isopimpinellin) and xanthotoxol (xanthotoxol) etc.It is reported, Chinese commodity Fructus Cnidii fruit contains columbianadin (columbianadin) 0.20%, circle root of Dahurain angelica element (archangelicin), cnidimine (edultin), bergapten, Isopimpinellin, O-acetyl Columbianedin (O-acetyl-columbianetin), Columbianedin (columbianetin), O-isovaleryl Columbianedin (O-islvaleryl-columbianetin), 3'-isobutyl acyl-oxygen-O-acetyl Columbianedin (3'-isobutyloxy-O-acetylcolumbianetin) and O-isobutyryl Columbianedin (O-isobutylcolumbianetin, cnidiadin).Seed contains bergapten, Europe orecselon (orosclol) and cnidimine.
Summary of the invention:
For the prior art above shortcomings, technical problem to be solved by this invention provides a kind of Fructus Cnidii anti-inflammatory composite soap.
Technical problem of the present invention is achieved by following technical proposals:
A kind of Fructus Cnidii anti-inflammatory composite soap comprises the raw material of following weight part: Fructus cnidii extract 0.05-0.15 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, coco betaine amide group both sexes base propionic salt 3-5 part, cocounut oil acyl both sexes base oxalic acid disodium 3-5 part, 20 parts in water.
Preferably, a kind of Fructus Cnidii anti-inflammatory composite soap, the raw material that comprises following weight part: Fructus cnidii extract 0.05-0.15 part, sequestrant 0.5-1.5 part, coco betaine amide group both sexes base propionic salt 3-5 part, cocounut oil acyl both sexes base oxalic acid disodium 3-5 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, 20 parts in water.
Described sequestrant is disodium EDTA, tetrasodium salt of EDTA, ethylenediamine tetramethylene phosphonic acid, the hydroxymethyl phosphonic acid diethyl ester, diethylenetriamine pentamethylene Alendronate, hexanediamine tetramethyl fork phosphonic acids, two hexene triamines, five methylenephosphonic acids, diethylenetriamine pentamethylenophosphonic acid(DTPP) seven sodium salts, EDTMP six sodium salts, sodium ethylenediamine tetramethylenephosphonate, a kind of or its mixture in MDGA trisodium salt and the hydroxyethyl diamine tetraacethyl trisodium salt.
Optimally, described sequestrant is made of by weight following component: MDGA trisodium salt 40-60 part and hydroxyethyl diamine tetraacethyl trisodium salt 40-60 part.
Below, part material involved in the present invention is made simple declaration:
Fructus Cnidii English name: Fructus Cnidii (drawing); Common cnidium fruit definition: the dry mature fruit of samphire cnidium monnieri Cnidium monnieri (L.) Cuss..Fructus cnidii extract of the present invention can pass through commercially available getting, such as the Fructus cnidii extract of Shenzhen BoDun spice Co., Ltd's production.This Fructus cnidii extract also can adopt following method preparation and get: after Fructus Cnidii is pulverized, the deionized water that adds the 6-10 times of weight, soaked 1-3 hour, ultrasonic extraction 10-15 minute, filter, centrifugal, discard precipitation with supernatant concentration, make Fructus cnidii extract, control Fructus cnidii extract density is at 1.05g/cm
3About.
Coco betaine amide group both sexes base propionic salt, CAS accession number: 100085-64-1.
Cocounut oil acyl both sexes base oxalic acid disodium, CAS accession number: 68650-39-5.
Described MDGA trisodium salt, CAS accession number: 170492-24-7, its English name: L-Alanine, N, N-bis (carboxymethyl)-, sodium salt (1:3).It has better biological degradability than sequestrant EDTA, NTA commonly used, and is more stable under wider PH scope and high temperature, has higher calcium sequestration capacity, and inorganic sediment is had higher solubility property, and heavy metal is had preferably sequestering power.Select in the present invention BASF AG to produce
Described hydroxyethyl diamine tetraacethyl trisodium salt, CAS accession number: 207386-87-6, its English name: Glycine, N-[2-[bis (carboxymethyl) amino] ethyl]-N-(2-hydroxyethyl)-, trisodium salt, hydrate (9CI).
In addition, in the present invention, can also add other functional ingredient commonly used in the common perfumed soap, such as: antiseptic-germicide, pigment, essence, oxidation inhibitor, titanium dioxide etc., to realize respectively corresponding function.As add the antiseptic-germicide of 0.2-0.8 weight part, the antioxidant of 0.05-0.20 weight part, the sanitas of 0.02-0.2 weight part, the white dyes of the titanium dioxide of 0.02-2 weight part, 0.001-0.05 weight part or the essence of 0.2-1.2 weight part on prescription of the present invention basis.
Fructus Cnidii anti-inflammatory composite soap of the present invention can adopt the general soapmaking step of the common perfumed soap of the industry to be prepared, as:
(a) spice of kneading: the various raw materials of said components are taken by weighing in proportion join in the kneading machine that conventional soapmaking uses, kneading mixes.
(b) grind: the material after mixing will kneaded, enter in the shredder, carry out soap body and grind.
(c) vacuum press strip: the soap body after will grinding, enter vacuum plodder, carry out the vacuum press strip.
(d) print: the rectangular soap body that plodder extrudes directly enters printer and prints, and obtains the soap body of moulding.
Fructus Cnidii anti-inflammatory composite soap of the present invention, foam is fine and smooth stable, performance is gentle, and is low to the pungency of skin, add Fructus cnidii extract especially after, more can anti-inflammation and sterilization.Especially, trichomonas vaginitis there is stronger killing action.
Embodiment:
Following embodiment further specifies of the present invention, rather than limits the scope of the invention.In the present invention, if no special instructions, each raw material is all take working substance content as 100%.
Embodiment 1
Embodiment 1 data by table 1 correspondence take by weighing each raw material.
(a) spice of kneading: various raw materials are joined soap with in the kneading machine, and kneading mixes.
(b) grind: the material after mixing will kneaded, enter in the shredder, carry out soap body and grind.
(c) vacuum press strip: the soap body after will grinding, enter vacuum plodder, carry out the vacuum press strip.
(d) print: the rectangular soap body that plodder extrudes directly enters printer and prints, and obtains the soap body of moulding.
Embodiment 2
Embodiment 2 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Embodiment 3
Embodiment 3 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Embodiment 4
Embodiment 4 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Comparative Examples 1
Comparative Examples 1 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Table 1: fancy soap formula list position: kilogram
Test case 1:
Experiment is 5wt% with soap lye concentration, and when consumption was 0.3ml, by HET VAM measurements determination skin reaction classification (relatively values classification), intense stimulus＞2.0 stimulated 1.2-2.0, medium stimulation 0.8-1.2, minimal irritation 0.0-0.8.
Use the Luo Shi Latherometer to carry out the foaming properties test, soap lye concentration is 2.5wt%, tests respectively the foam height of 0 minute and 5 minutes.
Table 2: test data table
The test data of experiment of associative list 2, the present invention selects coco betaine amide group both sexes base propionic salt and cocounut oil acyl both sexes base oxalic acid disodium built-up soap fundamental mode anion surfactant coconut oil sodium and Sodium pentadecanecarboxylate initiatively, can effectively reduce the pungency of perfumed soap; Select the composite interpolation of sequestrant MDGA trisodium salt and hydroxyethyl diamine tetraacethyl trisodium salt initiatively, further can promote foaming power and the foam stability of perfumed soap.Above-mentioned difference technical characterictic did not have open in the prior art, was not common practise yet.
Claims (3)
1. Fructus Cnidii anti-inflammatory composite soap, it is characterized in that, the raw material that comprises following weight part: Fructus cnidii extract 0.05-0.15 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, coco betaine amide group both sexes base propionic salt 3-5 part, cocounut oil acyl both sexes base oxalic acid disodium 3-5 part, 20 parts in water.
2. Fructus Cnidii perfumed soap as claimed in claim 1, it is characterized in that, the raw material that comprises following weight part: Fructus cnidii extract 0.05-0.15 part, sequestrant 0.5-1.5 part, coco betaine amide group both sexes base propionic salt 3-5 part, cocounut oil acyl both sexes base oxalic acid disodium 3-5 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, 20 parts in water.
3. Fructus Cnidii anti-inflammatory composite soap as claimed in claim 2, it is characterized in that: described sequestrant is made of by weight following component: MDGA trisodium salt 40-60 part and hydroxyethyl diamine tetraacethyl trisodium salt 40-60 part.
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| CN104263569A (en) * | 2014-10-14 | 2015-01-07 | 李正梅 | Anti-inflammatory homalocladium platycladium soap and preparation method thereof |
| CN105462727A (en) * | 2015-12-11 | 2016-04-06 | 梁文成 | Wormwood mixed soap |
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| CN1908144A (en) * | 2006-08-22 | 2007-02-07 | 乔爱娴 | Soap and its preparing process |
| CN102363740A (en) * | 2010-12-10 | 2012-02-29 | 江南大学 | Low-irritation and high-foaminess fancy soap formula |
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| US4743395A (en) * | 1986-09-12 | 1988-05-10 | The Drackett Company | Thickened acid cleaner compositions containing quaternary ammonium germicides and having improved thermal stability |
| CN1113264A (en) * | 1995-05-18 | 1995-12-13 | 高秀云 | Functional perfumed soap made from traditional Chinese herbal medicines |
| CN1908144A (en) * | 2006-08-22 | 2007-02-07 | 乔爱娴 | Soap and its preparing process |
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| CN104263569A (en) * | 2014-10-14 | 2015-01-07 | 李正梅 | Anti-inflammatory homalocladium platycladium soap and preparation method thereof |
| CN104263569B (en) * | 2014-10-14 | 2017-10-20 | 淄博职业学院 | A kind of centipedaplant herb anti-inflammatory perfumed soap and preparation method thereof |
| CN105462727A (en) * | 2015-12-11 | 2016-04-06 | 梁文成 | Wormwood mixed soap |
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