CN103387894B - Beautifying gynostemma pentaphylla composite perfumed soap - Google Patents

Beautifying gynostemma pentaphylla composite perfumed soap Download PDF

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CN103387894B
CN103387894B CN201310193044.6A CN201310193044A CN103387894B CN 103387894 B CN103387894 B CN 103387894B CN 201310193044 A CN201310193044 A CN 201310193044A CN 103387894 B CN103387894 B CN 103387894B
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gynostemma pentaphylla
soap
skin
hydroxyethyl
perfumed soap
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CN103387894A (en
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黄美蓉
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Anhui Jinguang Agricultural Service Co., Ltd.
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SHANGHAI BAFANG FINE CHEMICAL ENGINEERING Co Ltd
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Abstract

The invention discloses a beautifying gynostemma pentaphylla composite perfumed soap. The perfumed soap comprises the following raw materials by weight: 0.05 to 0.15 part of a gynostemma pentaphylla extract, 15 to 25 parts of sodium cocoate, 50 to 70 parts of sodium palmitate, 3 to 5 parts of di(hydroxyethyl) lauryl amine oxide, 3 to 5 parts of di(hydroxyethyl) tallow glycinate and 20 parts of water. The beautifying gynostemma pentaphylla composite perfumed soap provided by the invention has fine and stable foam, mild performance and small irritation to the skin; in particular, after addition of the gynostemma pentaphylla extract, the soap can whiten the skin and exerts antisepsis and anti-inflammation effects.

Description

Gynostemma pentaphylla beauty treatment composite soap
Technical field:
The present invention relates to a kind of perfumed soap, particularly a kind of gynostemma pentaphylla beauty treatment composite soap.
Background technology:
Perfumed soap (soap) is one of skin, hair washing and nursing article, is a kind of daily necessities.Perfumed soap is taking sodium soap and other tensio-active agents as main raw material, adds quality improver and outward appearance modifying agent, the product of making after machine-shaping.
Perfumed soap is requisite washing and nursing article in daily life, taking sodium soap and other tensio-active agents as main raw material, adds quality improver and outward appearance modifying agent, the product of making after machine-shaping.The function of perfumed soap is clean washing, be used in above skin that yes removes earth dirt, skin secretion, movement, chemical substance or bacterium etc., in today of stressing cosmetic result, makeup, skin care products or the medicine of removing skin surface are also one of its main purposes.
In the prior art, the many insights of perfumed soap are that fatty acid sodium salt is the Cake-shape soap of soap base, although there is good cleaning force, whipability and easy washability, but not resistance to hard water, when washing, can produce incrustation scale, form calcium magnesium soap, degreasing power is strong, the soap of human body life-time service meta-alkalescence can make skin feel dry and astringent, has excitement.
Gynostemma pentaphylla, claims again paradise grass, Chao Rencan, Herb Gynostemmae Pentaphylli, Herba Gynostemmatis, Rhizome or herb of Fiveleaf Gynostemma and gynostemma pentaphyllum makino etc.Mainly be distributed in China Hunan, Hubei, the provinces such as Yunnan, are known as " southern ginseng ", are grown in the medicinal content of southern gynostemma pentaphylla higher, and gynostemma pentaphylla is liked the weather of dark and damp gentleness, how wild in concealments place such as sylvan life, brook banks.Among the peoplely be called magical " elixir grass ", in Spark Program, classified as position first of " rare traditional Chinese medicine ".There is enterprise to be processed into gynostemma pentaphylla tea.
In gynostemma pentaphylla cauline leaf, contain the compositions such as protein, fat, food fibre, carbohydrate, calcium, phosphorus, iron, carotene, VITMAIN B1, Lin Suanna Vitamin B2 Sodium Phosphate, nicotinic acid, vitamins C and various trace elements.
Find through modern medicine study, the main effective constituent of gynostemma pentaphylla is polyose, flavonoid, saponins and microelement kind, its effect is mainly to promote body fat class substance metabolism, nutrition human body cell, there is good detoxicating, relieving inflammation effect simultaneously, be widely used in treatment and the health care of hyperlipidemia, fatty liver, obesity, constipation, insomnia, hepatitis B, chronic respiratory inflammation (pharyngolaryngitis, gastroenteritis etc.).
Gynostemma pentaphylla glucoside TN-1 and TN-2; Totally 79 of gynostemma pentaphylla glucoside I → LXXIX, wherein III, IV, VIII, VII level structure and ginsenoside-Rb1, Rb3, Rd, F2's is identical; 6 " malonyl ginsenoside-Rb1 and Rd, 6 " malonyl gynostemma pentaphylla glucoside V etc.The glucoside unit of these saponins has: panoxadiol, 2 Alpha-hydroxy panoxadiols, (20R, 25S)-12 β, 25-epoxy-20,26-encircles dammarane-2 α, 3 beta-diols, gynostemma pentaphylla glucoside unit II is (20R)-21, and 24-encircles-3 β, 25-dihydroxyl-23 (24)-Da Ma alkene-21-ketone.
" going back to nature, " (Back to nature) is the total slogan of current international cosmetic industry, and each advanced country all very payes attention to development natural type makeup.In this case, herbal medicine enjoys favor, and exhibition does not go out its unique charm, is bringing into play impayable advantage in cosmetic industry.And gynostemma pentaphylla acts on widely, significantly with it, be day by day subject to gazing at of makeup producer.
The active function of gynostemma pentaphylla to human body skin, is mainly reflected in the following aspects:
1, anti-aging effects.Conventionally,, in the time that senile plaque (also claiming lipofuscin) and brown macules and freckle form, can find that lipid peroxide accumulates in a large number and increase in skin.To drain the ability of lipid peroxide strong decomposing at an early age for people, weakens gradually with this effect of age growth, causes skin cells day by day aging.Total gypenosides can significantly reduce and suppress the generation of lipid peroxide, and protection skin cells film is avoided damage, and then prevents cell aging.Experiment confirmation, total gypenosides, to fetus diploid fibrocyte and human body Wei Erna syndromes skin cells, has the effect of significant prolongation cell survival; With human skin cell's vitro culture, add the nutrient solution of gypenoside 0.2%, can make cell reach for 27 generations by 22 generations, extend 22.7% of cell survival, therefore gypenoside has and composes the effect of living skin cells, can accelerate the renewal of skin surface cell, delay skin aging.Gynostemma pentaphylla is to body anti-aging effects, is vigor, the elimination of strengthening active oxidation free radical that can increase in human body and epiderm skin cell the Antioxidant Enzymes such as self Superoxide Dismutase (SOD) due to it, the metabolism that improves body.
2, improve skin microcirculation effect.Experiment showed, that Herb Gynostemmae Pentaphylli total glycosides is remarkable to the microcirculation improvement effect of skin, cutaneous circulation is plentiful, moisten and support moist and rich gloss.
3, the resistibility that improves skin, prevents skin cells canceration.Experiment showed, that Herb Gynostemmae Pentaphylli total glycosides can improve immunity of organisms, the infection of opposing skin.Prove through cell culture method, Herb Gynostemmae Pentaphylli total glycosides canceration capable of inhibiting cell, to the killing rate of tumour cell up to 91%.Thereby can protect skin, prevent that skin carcinoma from occurring.
4, Herb Gynostemmae Pentaphylli total glycosides contains multiple ginsenoside, and it is the same with ginseng has the degraded of the skin keratin of promotion; Stratum germinativum epidermidis hyperplasia metabolism; Collagen fibers of skin upgrades, arranges the effects such as parallel, can make skin tenderize and high resilience.Gynostemma pentaphylla, except containing ginsenoside, also contains multiple amino acids, VITAMIN and trace element, and this many kinds of substance is collaborative has profit to moisten effect to skin, can eliminate blackspot, prevents pachylosis.
5, ultraviolet injury resistant, anti-coarse and crowfoot cracks effect.Daylight, ultraviolet ray, ozone and oxynitride and most industrial pollutants all bring out active oxygen radical and generate, and cause dermal melanin cell sulfhydryl oxidase or directly increase tyrosinase activity; Thermal radiation also can increase tyrosine---tyrosine oxidase reaction, thus dermal melanin is increased, skin is blackening thus; Local melanochrome increases can form freckle or brown macules.The makeup that to experiment showed, with Herb Gynostemmae Pentaphylli total glycosides be effective ingredient, can resist the effect to skin such as ultraviolet ray and daylight, prevent skin tanning, dark brown spot is alleviated even and disappear.In addition Herb Gynostemmae Pentaphylli total glycosides has anti-coarsely and crease-resistantly split effect, and then plays beauty treatment and the dual function that keeps healthy.
6, stable spirit, prevents wan and sallow effect.Psychataxia, too excited, have a rest not good, in addition tiredly, can cause organism metabolic disorder, make wan and sallowly,, easily there is wrinkle in the skin elasticity that tarnishes, presents a weathered appearance.Herb Gynostemmae Pentaphylli total glycosides has stable spirit, keeping tensions down and fatigue-resisting function, can make people in high spirits, and face is ruddy, is difficult for producing wrinkle, seems young and dynamic.
7, gynostemma pentaphylla wetting ability composition can significantly suppress adipocyte generation free fatty acids and synthetic neutral fat, and stoping conversion of glucose is fat, therefore can be by lipometabolic adjusting is played to antiobesity action.Body fat is not that adipocyte number increases, but because adipocyte volume increases, the thickness of subcutaneous lipids increases.Experiment is common cultivation after half an hour at 37 DEG C with adipocyte and tracer compound C14-glucose, and the per minute umber of pulse of measuring adipocyte enters as glucose the index that cell synthesizes neutral fat.Nutrient solution adds gynostemma pentaphylla hydrophilic composition, and the CPm number that every gram of adipocyte records is not only for adding 50% left and right of group.Illustrate, the hydrophilic composition of gynostemma pentaphylla can suppress the synthetic neutral fat of adipocyte, makes adipocyte volume-diminished, thereby has antiobesity action.Oral gynostemma pentaphylla fitness tablet (tablet made from hydrophilic composition) is to reduce lipogenesis from overall angle, and topical application can make medicine directly act on subcutaneous fat thickness, thereby plays effect of fat-reducing, fitness.
Summary of the invention:
For prior art above shortcomings, technical problem to be solved by this invention is to provide a kind of gynostemma pentaphylla beauty treatment composite soap.
Technical problem of the present invention, is achieved by following technical proposals:
A kind of gynostemma pentaphylla beauty treatment composite soap, comprises the raw material of following weight part: Herb Gynostemmae Pentaphylli extract 0.05-0.15 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, two (hydroxyethyl) lauryl amine oxide compound 3-5 part, two (hydroxyethyl) tallow base glycinate 3-5 part, 20 parts, water.
Preferably, a kind of gynostemma pentaphylla beauty treatment composite soap, comprise the raw material of following weight part: Herb Gynostemmae Pentaphylli extract 0.05-0.15 part, sequestrant 0.5-1.5 part, two (hydroxyethyl) lauryl amine oxide compound 3-5 part, two (hydroxyethyl) tallow base glycinate 3-5 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, 20 parts, water.
Described sequestrant is disodium EDTA, tetrasodium salt of EDTA, ethylenediamine tetramethylene phosphonic acid, hydroxymethyl phosphonic acid diethyl ester, diethylenetriamine pentamethylene Alendronate, hexanediamine four methylenephosphonic acids, two hexene triamine five methylenephosphonic acids, diethylenetriamine pentamethylenophosphonic acid(DTPP) seven sodium salts, EDTMP six sodium salts, sodium ethylenediamine tetramethylenephosphonate, a kind of or its mixture in MDGA trisodium salt and hydroxyethyl diamine tetraacethyl trisodium salt.
Optimally, described sequestrant, is made up of by weight following component: MDGA trisodium salt 40-60 part and hydroxyethyl diamine tetraacethyl trisodium salt 40-60 part.
Part material involved in the present invention is made to simple declaration below:
Herb Gynostemmae Pentaphylli extract of the present invention can pass through commercially available obtaining, as the Herb Gynostemmae Pentaphylli extract of Shenzhen BoDun spice Co., Ltd's production.This Herb Gynostemmae Pentaphylli extract also can adopt following method preparation and obtain: after gynostemma pentaphylla is pulverized, add the deionized water of 6-10 times of weight, soak 1-3 hour, ultrasonic extraction 10-15 minute, filter, centrifugal, discard precipitation by supernatant concentration, make Herb Gynostemmae Pentaphylli extract, control Herb Gynostemmae Pentaphylli extract density at 1.05g/cm 3left and right.
Two (hydroxyethyl) lauryl amine oxide compound, claims again: 2, and 2 '-imino-di-methylcarbinol-N-tallow alkyl derivative-N-oxide, CAS accession number: 2530-44-1.
Two (hydroxyethyl) tallow base glycinate, CAS accession number: 61791-45-5.
Described MDGA trisodium salt, CAS accession number: 170492-24-7, its English name: L-Alanine, N, N-bis (carboxymethyl)-, sodium salt (1:3).It has better biological degradability than conventional sequestrant EDTA, NTA, under wider PH scope and high temperature, more stable, has higher calcium sequestration capacity, and inorganic sediment is had to higher solubility property, and heavy metal is had to good sequestering power.Select in the present invention BASF AG to produce m liquid.
Described hydroxyethyl diamine tetraacethyl trisodium salt, CAS accession number: 207386-87-6, its English name: Glycine, N-[2-[bis (carboxymethyl) amino] ethyl]-N-(2-hydroxyethyl)-, trisodium salt, hydrate (9CI).
In addition, in the present invention, can also add other functional ingredient conventional in common perfumed soap, for example: antiseptic-germicide, pigment, essence, oxidation inhibitor, titanium dioxide etc., to realize respectively corresponding function.As added the antiseptic-germicide of 0.2-0.8 weight part, the antioxidant of 0.05-0.20 weight part, the sanitas of 0.02-0.2 weight part, the essence of the titanium dioxide of 0.02-2 weight part, the white dyes of 0.001-0.05 weight part or 0.2-1.2 weight part on formula of the present invention basis.
Gynostemma pentaphylla beauty treatment composite soap of the present invention can adopt the general soapmaking step of the common perfumed soap of the industry to be prepared, as:
(a) spice of kneading: the various raw materials of said components are taken in proportion and joined in the kneading machine that conventional soapmaking uses, knead and be uniformly mixed.
(b) grind: the material after being uniformly mixed kneading, enter in shredder, carry out soap body grinding.
(c) vacuum press strip: by the soap body after grinding, enter vacuum plodder, carry out vacuum press strip.
(d) print: the rectangular soap body that plodder extrudes directly enters printer and prints, obtain the soap body of moulding.
Gynostemma pentaphylla of the present invention beauty treatment composite soap, foam is fine and smooth stable, and performance gentleness is low to the pungency of skin, adds especially after Herb Gynostemmae Pentaphylli extract, more can skin whitening, antisepsis and anti-inflammation.
Embodiment:
Embodiment further illustrates of the present invention below, instead of limits the scope of the invention.In the present invention, if no special instructions, each raw material is all taking working substance content as 100%.
Embodiment 1
Take each raw material by the embodiment of table 1 correspondence 1 data.
(a) spice of kneading: various raw materials are joined to soap with in kneading machine, knead and be uniformly mixed.
(b) grind: the material after being uniformly mixed kneading, enter in shredder, carry out soap body grinding.
(c) vacuum press strip: by the soap body after grinding, enter vacuum plodder, carry out vacuum press strip.
(d) print: the rectangular soap body that plodder extrudes directly enters printer and prints, obtain the soap body of moulding.
Embodiment 2
Take each raw material by the embodiment of table 1 correspondence 2 data.Prepare perfumed soap by the method for embodiment 1.
Embodiment 3
Take each raw material by the embodiment of table 1 correspondence 3 data.Prepare perfumed soap by the method for embodiment 1.
Embodiment 4
Take each raw material by the embodiment of table 1 correspondence 4 data.Prepare perfumed soap by the method for embodiment 1.
Comparative example 1
Take each raw material by the comparative example of table 1 correspondence 1 data.Prepare perfumed soap by the method for embodiment 1.
Table 1: fancy soap formula list position: kilogram
? Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Comparative example 1
Herb Gynostemmae Pentaphylli extract 0.1 0.1 0.1 0.1 0.1
Coconut oil sodium 20 20 20 20 20
Sodium pentadecanecarboxylate 60 60 60 60 60
Two (hydroxyethyl) lauryl amine oxide compound 4 4 4 4 /
Two (hydroxyethyl) tallow base glycinate 4 4 4 4 /
α-lauryl alkyl betaine / / / / 8
MDGA trisodium salt / 1 / 0.5 /
Hydroxyethyl diamine tetraacethyl trisodium salt / / 1 0.5 /
Water 20 20 20 20 20
Test case 1:
Experiment is 5wt% by soap lye concentration, and when consumption is 0.3ml, by HET VAM measurements determination skin reaction classification (values classification relatively), intense stimulus > 2.0, stimulates 1.2-2.0, medium stimulation 0.8-1.2, minimal irritation 0.0-0.8.
Use Roche Latherometer to carry out foaming properties test, soap lye concentration is 2.5wt%, tests respectively the foam height of 0 minute and 5 minutes.
Table 2: test data table
The test data of experiment of associative list 2, the present invention selects two (hydroxyethyl) lauryl amine oxide compound and two (hydroxyethyl) tallow base glycinate built-up soap fundamental mode anion surfactant coconut oil sodium and Sodium pentadecanecarboxylate initiatively, can effectively reduce the pungency of perfumed soap; Select the composite interpolation of sequestrant MDGA trisodium salt and hydroxyethyl diamine tetraacethyl trisodium salt initiatively, further can promote foaming power and the foam stability of perfumed soap.Above-mentioned difference technical characterictic did not have open in the prior art, was not common practise yet.

Claims (1)

1. a gynostemma pentaphylla beauty treatment composite soap, it is characterized in that, comprise the raw material of following weight part: Herb Gynostemmae Pentaphylli extract 0.05-0.15 part, sequestrant 0.5-1.5 part, two (hydroxyethyl) lauryl amine oxide compound 3-5 part, two (hydroxyethyl) tallow base glycinate 3-5 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, 20 parts, water, described sequestrant, is made up of by weight following component: MDGA trisodium salt 40-60 part and hydroxyethyl diamine tetraacethyl trisodium salt 40-60 part.
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KR102501943B1 (en) 2014-07-31 2023-03-15 킴벌리-클라크 월드와이드, 인크. Anti-adherent composition
KR102441223B1 (en) 2014-07-31 2022-09-08 킴벌리-클라크 월드와이드, 인크. Anti-adherent alcohol-based composition
US9969885B2 (en) 2014-07-31 2018-05-15 Kimberly-Clark Worldwide, Inc. Anti-adherent composition
MX2017004281A (en) * 2014-10-31 2017-06-15 Kimberly Clark Co Anti-adherent botanical compositions.
MX2017011771A (en) 2015-04-01 2017-12-04 Kimberly Clark Co Fibrous substrate for capture of gram negative bacteria.
KR102627187B1 (en) 2016-05-26 2024-01-22 킴벌리-클라크 월드와이드, 인크. Anti-adhesion compositions and methods for inhibiting adhesion of microorganisms to surfaces
CN106434048A (en) * 2016-08-19 2017-02-22 跨越生物科技(滁州)有限公司 Anti-ageing handmade soap

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US4743395A (en) * 1986-09-12 1988-05-10 The Drackett Company Thickened acid cleaner compositions containing quaternary ammonium germicides and having improved thermal stability
CN1088976A (en) * 1993-01-01 1994-07-06 刘武青 Gynostemma pentaphyllum toilet soap

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4743395A (en) * 1986-09-12 1988-05-10 The Drackett Company Thickened acid cleaner compositions containing quaternary ammonium germicides and having improved thermal stability
CN1088976A (en) * 1993-01-01 1994-07-06 刘武青 Gynostemma pentaphyllum toilet soap

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Patentee before: Shanghai Bafang Fine Chemical Engineering Co., Ltd.