CN103351958A - Eider down caring agent and preparation method thereof - Google Patents
Eider down caring agent and preparation method thereof Download PDFInfo
- Publication number
- CN103351958A CN103351958A CN201310270961XA CN201310270961A CN103351958A CN 103351958 A CN103351958 A CN 103351958A CN 201310270961X A CN201310270961X A CN 201310270961XA CN 201310270961 A CN201310270961 A CN 201310270961A CN 103351958 A CN103351958 A CN 103351958A
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- CN
- China
- Prior art keywords
- parts
- agent
- eider down
- minute
- vinyltriethoxysilane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002360 preparation method Methods 0.000 title claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims abstract description 10
- -1 polyoxyethylene octylphenol Polymers 0.000 claims abstract description 10
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 8
- ZFOZVQLOBQUTQQ-UHFFFAOYSA-N Tributyl citrate Chemical compound CCCCOC(=O)CC(O)(C(=O)OCCCC)CC(=O)OCCCC ZFOZVQLOBQUTQQ-UHFFFAOYSA-N 0.000 claims abstract description 8
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims abstract description 4
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims abstract description 4
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims abstract description 4
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000005642 Oleic acid Substances 0.000 claims abstract description 4
- REZZEXDLIUJMMS-UHFFFAOYSA-M dimethyldioctadecylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC REZZEXDLIUJMMS-UHFFFAOYSA-M 0.000 claims abstract description 4
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims abstract description 4
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 claims abstract description 4
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims abstract description 4
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims abstract description 4
- WEAPVABOECTMGR-UHFFFAOYSA-N triethyl 2-acetyloxypropane-1,2,3-tricarboxylate Chemical compound CCOC(=O)CC(C(=O)OCC)(OC(C)=O)CC(=O)OCC WEAPVABOECTMGR-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000009637 wintergreen oil Substances 0.000 claims abstract description 4
- 230000000474 nursing effect Effects 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 10
- 239000004902 Softening Agent Substances 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 6
- LCPVQAHEFVXVKT-UHFFFAOYSA-N 2-(2,4-difluorophenoxy)pyridin-3-amine Chemical compound NC1=CC=CN=C1OC1=CC=C(F)C=C1F LCPVQAHEFVXVKT-UHFFFAOYSA-N 0.000 claims description 6
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Substances [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims description 3
- 241000628997 Flos Species 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 3
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 3
- UMGDCJDMYOKAJW-UHFFFAOYSA-N aminothiocarboxamide Natural products NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 claims description 3
- 239000007822 coupling agent Substances 0.000 claims description 3
- 239000004664 distearyldimethylammonium chloride (DHTDMAC) Substances 0.000 claims description 3
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 3
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 3
- 229940049964 oleate Drugs 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 239000000344 soap Substances 0.000 claims description 3
- 230000003750 conditioning effect Effects 0.000 abstract description 3
- RYYXDZDBXNUPOG-UHFFFAOYSA-N 4,5,6,7-tetrahydro-1,3-benzothiazole-2,6-diamine;dihydrochloride Chemical compound Cl.Cl.C1C(N)CCC2=C1SC(N)=N2 RYYXDZDBXNUPOG-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 241000220317 Rosa Species 0.000 abstract 1
- 230000007935 neutral effect Effects 0.000 abstract 1
- 239000000341 volatile oil Substances 0.000 abstract 1
- 238000005406 washing Methods 0.000 description 4
- 230000001954 sterilising effect Effects 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
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- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Detergent Compositions (AREA)
Abstract
An eider down caring agent is characterized by being composed of following components in parts by weight: 2 to 3 parts of dioctadecyl dimethyl ammonium chloride, 0.1 to 0.2 part of oil of wintergreen, 0.03 to 0.05 part of rose essential oil, 2 to 3 parts of isomeric alcohol ethoxylates, 1 to 2 parts of neopentylene glycol, 2 to 3 parts of triethyl O-acetylcitrate, 1 to 2 parts of tributyl citrate, 1 to 2 parts of polyoxyethylene octylphenol ether, 2 to 3 parts of vinyltriethoxysilane, 1 to 2 parts of thiourea dioxide, 1 to 2 parts of oleic acid, 3 to 4 parts of softener, and 150 parts of water. The eider down caring agent can effectively remove stains on eider downs, has a strong anti-bacterium performance and relatively good conditioning and caring functions on eider downs, is capable of restoring original elasticity and fluffy state of eider downs and maintaining original heat-insulating performance, integrates the functions of anti-bacterium, odor-eliminating, and conditioning together, and has the advantages of strong detergency and good stability. The caring agent can be used with hot or cold water; furthermore, the caring agent is neutral and is harmless to human hands.
Description
Technical field
The invention belongs to washing and nursing article, specifically a kind of eider down nursing agent and preparation method thereof.
Background technology
Eider down is widely used in the making down jackets, but because eider down comes from animal, usually with more bacterium, fishy smell is arranged.With general articles for washing, can the flush away foul, but there is not sterilizing function, and easily damage eider down, cause and harden, no longer have original elasticity and loftiness, thermal property reduces, therefore, be badly in need of nursing and the washing composition that research has the washing of having concurrently, nursing, taste removal, sterilizing function to take into account to eider down.
Summary of the invention
The purpose of this invention is to provide a kind of eider down nursing agent and preparation method thereof.
Technical scheme of the present invention is as follows:
A kind of eider down nursing agent is characterized in that being made by the raw material of following weight part: distearyl dimethyl ammonium chloride 2-3, wintergreen oil 0.1-0.2, Flos Rosae Rugosae quintessence oil 0.03-0.05, different tridecanol polyoxyethylene ether 2-3, neopentyl glycol 1-2, acetyl triethyl citrate 2-3, tributyl citrate 1-2, polyoxyethylene octylphenol ether 1-2, vinyltriethoxysilane 2-3, thiourea peroxide 1-2, oleic acid 1-2, softening agent 3-4, water 150;
Described softener is made by the feed composition of following weight part: tea-polyphenol 0.2-0.3, Sodium Persulfate 0.3-0.4, glyceryl monostearate 2.3-2.5, morpholine 1-1.2, trihydroxy ethylamine oleate soap 0.8-0.9, amido silicon oil 3.4-3.8, Soxylat A 25-7 1.2-1.5, titanate coupling agent TMC-TTS 1.2-1.5, citric acid 2.0-2.4, di-n-octyl-4-isothiazoline-3-ketone 0.3-0.5, water 15-18; The preparation method adds suitable quantity of water dissolving with Sodium Persulfate, drops in the mixture of other remaining component, stirs 40-50 minute, then is warming up to 70-80 ℃, stirring reaction 1-2 hour and get final product.
The preparation method of described eider down nursing agent, it is characterized in that other composition except vinyltriethoxysilane, softening agent is mixed, be heated to 75-80 ℃, stirring reaction 50-60 minute, then add vinyltriethoxysilane, stirred 30-40 minute, be warming up to again 90-95 ℃, add softening agent, continue stirring reaction 30-40 minute and get final product.
The present invention can effectively remove the dirt on the eider down, germicidal action is strong, eider down there are preferably conditioning, nursing role, eider down recovers original elasticity and bulk shape, keeps original thermal property, integrates sterilization, de-tastes, nurses one's health, strong detergency, good stability, cold and hot water all can, neutrality is not hindered hand.
Embodiment
A kind of eider down nursing agent is made by the raw material of following weight part (kilogram): distearyl dimethyl ammonium chloride 2, wintergreen oil 0.1, Flos Rosae Rugosae quintessence oil 0.05, different tridecanol polyoxyethylene ether 2, neopentyl glycol 1, acetyl triethyl citrate 2, tributyl citrate 2, polyoxyethylene octylphenol ether 1, vinyltriethoxysilane 3, thiourea peroxide 1, oleic acid 1, softening agent 4, water 150;
Described softener is made by the feed composition of following weight part (kilogram): tea-polyphenol 0.2, Sodium Persulfate 0.3, glyceryl monostearate 2.3, morpholine 1, trihydroxy ethylamine oleate soap 0.9, amido silicon oil 3.4, Soxylat A 25-7 1.2, titanate coupling agent TMC-TTS 1.2, citric acid 2.0, di-n-octyl-4-isothiazoline-3-ketone 0.3, water 15; The preparation method adds suitable quantity of water dissolving with Sodium Persulfate, drops in the mixture of other remaining component, stirs 40-50 minute, then is warming up to 70-80 ℃, stirring reaction 1-2 hour and get final product.
The preparation method of eider down nursing agent: be that other composition except vinyltriethoxysilane, softening agent is mixed, be heated to 75-80 ℃, stirring reaction 50-60 minute, then add vinyltriethoxysilane, stirred 30-40 minute, be warming up to again 90-95 ℃, add softening agent, continue stirring reaction 30-40 minute and get final product.
Claims (2)
1. an eider down nursing agent is characterized in that being made by the raw material of following weight part: distearyl dimethyl ammonium chloride 2-3, wintergreen oil 0.1-0.2, Flos Rosae Rugosae quintessence oil 0.03-0.05, different tridecanol polyoxyethylene ether 2-3, neopentyl glycol 1-2, acetyl triethyl citrate 2-3, tributyl citrate 1-2, polyoxyethylene octylphenol ether 1-2, vinyltriethoxysilane 2-3, thiourea peroxide 1-2, oleic acid 1-2, softening agent 3-4, water 150;
Described softener is made by the feed composition of following weight part: tea-polyphenol 0.2-0.3, Sodium Persulfate 0.3-0.4, glyceryl monostearate 2.3-2.5, morpholine 1-1.2, trihydroxy ethylamine oleate soap 0.8-0.9, amido silicon oil 3.4-3.8, Soxylat A 25-7 1.2-1.5, titanate coupling agent TMC-TTS 1.2-1.5, citric acid 2.0-2.4, di-n-octyl-4-isothiazoline-3-ketone 0.3-0.5, water 15-18; The preparation method adds suitable quantity of water dissolving with Sodium Persulfate, drops in the mixture of other remaining component, stirs 40-50 minute, then is warming up to 70-80 ℃, stirring reaction 1-2 hour and get final product.
2. the preparation method of eider down nursing agent according to claim 1, it is characterized in that other composition except vinyltriethoxysilane, softening agent is mixed, be heated to 75-80 ℃, stirring reaction 50-60 minute, then add vinyltriethoxysilane, stirred 30-40 minute, be warming up to again 90-95 ℃, add softening agent, continue stirring reaction 30-40 minute and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310270961.XA CN103351958B (en) | 2013-07-01 | 2013-07-01 | Eider down caring agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310270961.XA CN103351958B (en) | 2013-07-01 | 2013-07-01 | Eider down caring agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103351958A true CN103351958A (en) | 2013-10-16 |
| CN103351958B CN103351958B (en) | 2015-03-25 |
Family
ID=49308372
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310270961.XA Expired - Fee Related CN103351958B (en) | 2013-07-01 | 2013-07-01 | Eider down caring agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103351958B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104450283A (en) * | 2014-10-20 | 2015-03-25 | 常熟市奥琪特服饰有限公司 | Novel down coat cleaning agent |
| CN105506970A (en) * | 2015-12-25 | 2016-04-20 | 常熟市明达腈纺有限公司 | Crude-fine fiber blended yarn |
| CN106281744A (en) * | 2016-08-16 | 2017-01-04 | 薛常莲 | A kind of infantile clothes concentrated cleaning and preparation method thereof |
| CN108103791A (en) * | 2017-12-26 | 2018-06-01 | 安徽羽洁家纺有限公司 | A kind of sterilizing and mould-proofing down feather nursing agent and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100500985C (en) * | 2006-11-27 | 2009-06-17 | 常熟市亚德实业有限公司 | Feather-down clothing care agent |
-
2013
- 2013-07-01 CN CN201310270961.XA patent/CN103351958B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100500985C (en) * | 2006-11-27 | 2009-06-17 | 常熟市亚德实业有限公司 | Feather-down clothing care agent |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104450283A (en) * | 2014-10-20 | 2015-03-25 | 常熟市奥琪特服饰有限公司 | Novel down coat cleaning agent |
| CN105506970A (en) * | 2015-12-25 | 2016-04-20 | 常熟市明达腈纺有限公司 | Crude-fine fiber blended yarn |
| CN106281744A (en) * | 2016-08-16 | 2017-01-04 | 薛常莲 | A kind of infantile clothes concentrated cleaning and preparation method thereof |
| CN106281744B (en) * | 2016-08-16 | 2019-02-26 | 苏雨江 | A kind of infantile clothes concentrated cleaning and preparation method thereof |
| CN108103791A (en) * | 2017-12-26 | 2018-06-01 | 安徽羽洁家纺有限公司 | A kind of sterilizing and mould-proofing down feather nursing agent and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103351958B (en) | 2015-03-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190923 Address after: 236 800 Haijing Building, Baocheng District, Bozhou City, Anhui Province, 3 buildings 207 Patentee after: BOZHOU WOYE INTELLECTUAL PROPERTY SERVICE Co.,Ltd. Address before: 231300, Anhui, Lu'an province Shucheng County town of plum river east road, Seven Star Industrial Park, Anhui Huaqiang down Co., Ltd. Patentee before: Chen Houqian |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20191120 Address after: Cao Dian Zhen Hao she Cun, Baoying County, Yangzhou City, Jiangsu Province Patentee after: Yangzhou Ruixin down products Co.,Ltd. Address before: 236 800 Haijing Building, Baocheng District, Bozhou City, Anhui Province, 3 buildings 207 Patentee before: BOZHOU WOYE INTELLECTUAL PROPERTY SERVICE Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150325 |