CN103351253B - Microcapsule Chinese medicine organic fertilizer and preparation method thereof - Google Patents

Abstract

The invention discloses a microcapsule Chinese medicine organic fertilizer and a preparation method thereof. The compound organic fertilizer comprises the following ingredients by weight: 15 to 20 parts of potassium sulphate, 10 to 25 parts of ammonium sulfate, 5 to 10 parts of high-calcium clay, 10 to 15 parts of diammonium phosphate, 2 to 5 parts of fulvic acid, 1 to 4 parts of soluble chitosan and the like. The compound fertilizer reasonably composite various fertilizers, pearlstone and vermiculite; the recipe is scientific and reasonable; the adaptive range is wide; the fertilizing value is strong and lasting; the in-season utilization rate is high; the pearlstone and the vermiculite in the recipe have an obvious improvement effect on soil texture; various plants are enabled to achieve high quality and stable yield.

Description

A kind of Microcapsule Chinese medicine organic fertilizer and preparation method thereof

Technical field

What the present invention relates to is microcapsule organic fertilizer and preparation method thereof.

Background technology

Existing complex fertilizer product formula is unreasonable, and solely pursue high nitrogen or Gao Jia class composite fertilizer, blindness is large, and utilization ratio is low, and what have even causes quality of agricultural product low, harm consumer health; Physical behavior is bad, and dust is many, not resistance to compression, caking, is not easy to store, transport and fertilising.The utilising efficiency of general inorganic fertilizer is lower, its major cause be inorganic fertilizer be manured into soil or in water after, easily fixed by metal ions such as calcium, magnesium, iron, aluminium, easily adsorb by clay mineral particle, thus reduce fertilizer efficiency to environment.In composite fertilizer conventional at present, phosphorus potassium is easily fixed by metal ions such as the calcium in waste water, magnesium, iron, aluminium, and reduce the utilization ratio of fertilizer, the phosphorus content that excessive interpolation not only increases in reagent cost but also water outlet easily exceeds standard.Therefore the compoiste fertilizer developing high utilization rate has realistic meaning.

Summary of the invention

The present invention is directed to existing deficiency and provide a kind of organic composite Traditional Chinese medicine fertilizer and preparation method thereof.

The present invention realizes above-mentioned purpose by the following method.

A kind of Microcapsule Chinese medicine organic fertilizer, be made up of the composition of following weight ratio: potassium sulfate 15-20 part, ammonium sulfate 10-25 part, high calcium clay 5-10 part, diammonium phosphate 10-15 part, xanthohumic acid 2-5 part, soluble chitosan 1-4 part, organic waste 50-60 part, trace element 4-7 part, perlite 5-10 part, vermiculite 3-6 part, fenaminosulf 1-3 part, kongpo monkshood root 45-55 part, Semen Momordicae 40-50 part, Stellera chamaejasme L. 1-15 part, hops 5-10 part, matrine 5-10 part, Golden Larch Bark 10-15 part, Chinese prickly ash 20-30 part, ginkgo seed coat 20-30 part, Fructus Cnidii 20-30 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, Seed of Chinese Soapberry exosper 55-60 part, fructus ulmi 10-15 part, camphor 5-15 part, organic solvent 10 ~ 20 parts, cyst material 10 ~ 15 parts, 1 ~ 3 part, colloid,

Described organic waste is: one or several mixtures of branch, dry branches and fallen leaves, wood chip, peat, municipal sludge;

Described trace element is Cu, Fe, Mn, B, Mo mixture of equivalent.

Compound organic fertilizer is preferably made up of the composition of following weight ratio: potassium sulfate 17 parts, 18 parts, ammonium sulfate, high calcium clay 8 parts, diammonium phosphate 13 parts, xanthohumic acid 4 parts, soluble chitosan 2 parts, organic waste 55 parts, trace element 6 parts, perlite 6 parts, vermiculite 5 parts, fenaminosulf 2 parts, m-tetrachlorophthalodinitrile 3 parts.

The preparation method of compound organic fertilizer,

(1) to become thoroughly decomposed program: macerating inserting corruption in pond after organic waste fragmentation, slowly rising to 60 DEG C from normal temperature, the hold-time is 1 day, 70 DEG C are raised to from 60 DEG C, hold-time is 2 days, then cools the temperature to less than 40 DEG C, keeps 10 days, make organic waste slaking, after slaking, dry, pulverize, cross 60 mesh sieves, obtain the organic powder of slaking;

(2) kongpo monkshood root, Semen Momordicae, Stellera chamaejasme L., hops, matrine, Golden Larch Bark, Chinese prickly ash, ginkgo seed coat, Fructus Cnidii, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, Seed of Chinese Soapberry exosper, fructus ulmi, camphor is got according to described parts by weight, soak in water after 2.5 hours, be warmed to 50 DEG C to keep 30 minutes, then the cellulase adding (unit of activity of 10 parts is 100U) carries out enzymolysis, enzyme digestion reaction temperature is 30-50 DEG C, the enzyme digestion reaction time is 1.5 hours, filters and obtains Chinese herbal medicine fluid; Described obtained herbal liquid medicine 300 parts is added 75% alcohol immersion 80min of 10 times of weight, be heated to 70 DEG C times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 DEG C times and heats up in a steamer 45min, filter, collect extracting solution, be dried to powder; Mix with the organic powder of slaking in step (2)

; Add the cyst material of described weight part, then the colloid adding described weight part stirs with per minute 2500 rotating speed, forms oil-in-water emulsion; Reduce revolution to 1500 turns, stir and within 25 minutes, then add dilute hydrochloric acid adjustment pH value to 3.0, then after stirring 1 hour, rotating speed is dropped to 100 revs/min, be warmed up to 50 ~ 55 DEG C, continue to stir, add sodium hydroxide after 2 hours and regulate pH value to 7.0.

Beneficial effect

The present invention has the following advantages:

(1) use and can reduce soil salinity and alkalinity, in a large number, keep soil from packing together, containing the impurity that heavy metal etc. is harmful to plants and soil, be conducive to protection of the environment; Use conveniently, can topdress, to yield positive results the demand of phase to N, P, K as plant growth early stage, tuber expansion period and fruit tree, also can make base manure; Applied widely, be both applicable to the cash crop such as apple, vegetables, tobacco, large cherry, watermelon, be applicable to again the grain and oil crops such as wheat, corn, paddy rice, peanut, Be very effective; Not containing any objectionable constituent, be the green fertilizer developed eco-agriculture, can reduce costs to greatest extent, improve fertilizer efficiency, highly efficient and productive, high-quality;

(2) new approach is opened for the industrialization of organic waste is agricultural.Using the increase soil organism of this product, improving soil physico-chemical property will get positive effect;

(3) fertilizer of the present invention has set up fenaminosulf and m-tetrachlorophthalodinitrile, under the prerequisite increasing the soil organism, reduces the probability of plant infection disease and pest;

(4) various fertilizer and perlite, vermiculite are carried out reasonable formula by composite fertilizer of the present invention, and scientific formulation is reasonable, wide accommodation, fertilizer efficiency is lastingly powerful, this season utilization ratio is high, and perlite, the vermiculite in formula has obvious improved effect to the soil texture, makes each kind of plant reach high quality and stable yield.

(5) to have herbicidal effect good, environmentally safe for distinctive formula of the present invention, and weeds such as not easily to develop immunity to drugs at the feature, have a extensive future.To people and animals, relatively safety is to eyes, no skin irritation, and be low toxicity through day skin test checking its acute toxicity bright, easily decompose in air and soil, non-poisonous material remains; On farmland natural enemy impact little (natural enemy kill rate is less than 1%), contribute to keeping ecotope, more friendly to environment, meet the production requirement of crop.Fertilizer efficiency time lengthening more than 3 months, utilization rate of fertilizer improves 15%, improves the benefit of the producer.

Embodiment

Below in conjunction with embodiment, the present invention is further illustrated, and following each embodiment, only for illustration of the present invention, does not limit the present invention.

Embodiment one

A kind of Microcapsule Chinese medicine organic fertilizer, be made up of the composition of following weight ratio: potassium sulfate 15 parts, 10 parts, ammonium sulfate, high calcium clay 5 parts, diammonium phosphate 10 parts, xanthohumic acid 2 parts, soluble chitosan 1 part, dry branches and fallen leaves 50 parts, trace element 4 parts, perlite 5 parts, vermiculite 3 parts, fenaminosulf 1 part, kongpo monkshood root 45 parts, Semen Momordicae 40 parts, Stellera chamaejasme L. 1 part, hops 5 parts, matrine 5 parts, Golden Larch Bark 10 parts, 20 parts, Chinese prickly ash, ginkgo seed coat 20 parts, Fructus Cnidii 20 parts, Cortex Meliae 10 parts, Rangooncreeper Fruit 15 parts, 1 part, Turkey-galls, Root of Pubescent Holly 5 parts, Seed of Chinese Soapberry exosper 55 parts, fructus ulmi 10 parts, camphor 5 parts, organic solvent 10 ~ 20 parts, cyst material 10 ~ 15 parts, 1 ~ 3 part, colloid,

Described trace element is Cu, Fe, Mn, B, Mo mixture of equivalent.

The preparation method of compound organic fertilizer,

(1) to become thoroughly decomposed program: macerating inserting corruption in pond after organic waste fragmentation, slowly rising to 60 DEG C from normal temperature, the hold-time is 1 day, 70 DEG C are raised to from 60 DEG C, hold-time is 2 days, then cools the temperature to less than 40 DEG C, keeps 10 days, make organic waste slaking, after slaking, dry, pulverize, cross 60 mesh sieves, obtain the organic powder of slaking;

(2) kongpo monkshood root, Semen Momordicae, Stellera chamaejasme L., hops, matrine, Golden Larch Bark, Chinese prickly ash, ginkgo seed coat, Fructus Cnidii, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, Seed of Chinese Soapberry exosper, fructus ulmi, camphor is got according to described parts by weight, soak in water after 2.5 hours, be warmed to 50 DEG C to keep 30 minutes, then the cellulase adding (unit of activity of 10 parts is 100U) carries out enzymolysis, enzyme digestion reaction temperature is 30-50 DEG C, the enzyme digestion reaction time is 1.5 hours, filters and obtains Chinese herbal medicine fluid; Described obtained herbal liquid medicine 300 parts is added 75% alcohol immersion 80min of 10 times of weight, be heated to 70 DEG C times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 DEG C times and heats up in a steamer 45min, filter, collect extracting solution, be dried to powder; After mixing with the organic powder of slaking in step (2)

; Add the cyst material of described weight part, then the colloid adding described weight part stirs with per minute 2500 rotating speed, forms oil-in-water emulsion; Reduce revolution to 1500 turns, stir and within 25 minutes, then add dilute hydrochloric acid adjustment pH value to 3.0, then after stirring 1 hour, rotating speed is dropped to 100 revs/min, be warmed up to 50 ~ 55 DEG C, continue to stir, add sodium hydroxide after 2 hours and regulate pH value to 7.0.

Embodiment two

A kind of Microcapsule Chinese medicine organic fertilizer, be made up of the composition of following weight ratio: potassium sulfate 20 parts, 25 parts, ammonium sulfate, high calcium clay 10 parts, diammonium phosphate 15 parts, xanthohumic acid 5 parts, soluble chitosan 4 parts, peat and municipal sludge 60 parts, trace element 7 parts, perlite 10 parts, vermiculite 6 parts, fenaminosulf 3 parts, kongpo monkshood root 55 parts, Semen Momordicae 50 parts, Stellera chamaejasme L. 15 parts, hops 10 parts, matrine 10 parts, Golden Larch Bark 15 parts, 30 parts, Chinese prickly ash, ginkgo seed coat 30 parts, Fructus Cnidii 30 parts, Cortex Meliae 30 parts, Rangooncreeper Fruit 25 parts, 15 parts, Turkey-galls, Root of Pubescent Holly 15 parts, Seed of Chinese Soapberry exosper 60 parts, fructus ulmi 15 parts, camphor 15 parts, organic solvent 10 ~ 20 parts, cyst material 10 ~ 15 parts, 1 ~ 3 part, colloid,

Described trace element is Cu, Fe, Mn, B, Mo mixture of equivalent.

The preparation method of compound organic fertilizer,

(1) to become thoroughly decomposed program: macerating inserting corruption in pond after organic waste fragmentation, slowly rising to 60 DEG C from normal temperature, the hold-time is 1 day, 70 DEG C are raised to from 60 DEG C, hold-time is 2 days, then cools the temperature to less than 40 DEG C, keeps 10 days, make organic waste slaking, after slaking, dry, pulverize, cross 60 mesh sieves, obtain the organic powder of slaking;

(2) kongpo monkshood root, Semen Momordicae, Stellera chamaejasme L., hops, matrine, Golden Larch Bark, Chinese prickly ash, ginkgo seed coat, Fructus Cnidii, Cortex Meliae, Rangooncreeper Fruit, Turkey-galls, Root of Pubescent Holly, Seed of Chinese Soapberry exosper, fructus ulmi, camphor is got according to described parts by weight, soak in water after 2.5 hours, be warmed to 50 DEG C to keep 30 minutes, then the cellulase adding (unit of activity of 10 parts is 100U) carries out enzymolysis, enzyme digestion reaction temperature is 30-50 DEG C, the enzyme digestion reaction time is 1.5 hours, filters and obtains Chinese herbal medicine fluid; Described obtained herbal liquid medicine 300 parts is added 75% alcohol immersion 80min of 10 times of weight, be heated to 70 DEG C times and heat up in a steamer 45min, filter, collect extracting solution; Filter residue adds 70% ethanol of 5 times of weight again, is heated to 80 DEG C times and heats up in a steamer 45min, filter, collect extracting solution, be dried to powder; After mixing with the organic powder of slaking in step (2); Add the cyst material of described weight part, then the colloid adding described weight part stirs with per minute 2500 rotating speed, forms oil-in-water emulsion; Reduce revolution to 1500 turns, stir and within 25 minutes, then add dilute hydrochloric acid adjustment pH value to 3.0, then after stirring 1 hour, rotating speed is dropped to 100 revs/min, be warmed up to 50 ~ 55 DEG C, continue to stir, add sodium hydroxide after 2 hours and regulate pH value to 7.0.

Composite microbiological fertilizer prepared by table 1 the present invention and common fertilizer compare

	Oidium decrement (%)	Anthrax decrement (%)	Spot disease decrement (%)	Output increases (%)
					Embodiment 1	74	48	58	39
Embodiment 2	79	53	47	46

Fertilizer efficiency time lengthening more than 3 months, utilization rate of fertilizer improves 15%, improves the benefit of the producer.

The preferred embodiment that the above-mentioned contriver of being provides, the invention is not restricted to these embodiments.Formula of the present invention can carry out adjustment of formula according to location soil status, all can reach promising result.

Claims (1)

1. a Microcapsule Chinese medicine organic fertilizer, it is characterized in that, be made up of the composition of following weight ratio: potassium sulfate 15-20 part, ammonium sulfate 10-25 part, high calcium clay 5-10 part, diammonium phosphate 10-15 part, xanthohumic acid 2-5 part, soluble chitosan 1-4 part, organic waste 50-60 part, trace element 4-7 part, perlite 5-10 part, vermiculite 3-6 part, fenaminosulf 1-3 part, m-tetrachlorophthalodinitrile 2-4 part, kongpo monkshood root 45-55 part, Semen Momordicae 40-50 part, Stellera chamaejasme L. 1-15 part, hops 5-10 part, matrine 5-10 part, Golden Larch Bark 10-15 part, Chinese prickly ash 20-30 part, ginkgo seed coat 20-30 part, Fructus Cnidii 20-30 part, Cortex Meliae 10-30 part, Rangooncreeper Fruit 15-25 part, Turkey-galls 1-15 part, Root of Pubescent Holly 5-15 part, Seed of Chinese Soapberry exosper 55-60 part, fructus ulmi 10-15 part, camphor 5-15 part, organic solvent 10 ~ 20 parts, cyst material 10 ~ 15 parts, 1 ~ 3 part, colloid,

Described organic waste is: one or several mixtures of branch, dry branches and fallen leaves, wood chip, peat, municipal sludge;

Described trace element is Cu, Fe, Mn, B, Mo mixture of equivalent.