CN103315928A - Red date pectin mask and preparation method thereof - Google Patents
Red date pectin mask and preparation method thereof Download PDFInfo
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- CN103315928A CN103315928A CN2013102079174A CN201310207917A CN103315928A CN 103315928 A CN103315928 A CN 103315928A CN 2013102079174 A CN2013102079174 A CN 2013102079174A CN 201310207917 A CN201310207917 A CN 201310207917A CN 103315928 A CN103315928 A CN 103315928A
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- pectin
- fructus jujubae
- red date
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Abstract
The invention relates to the field of cosmetics and discloses a red date pectin mask and a preparation method thereof. The red date pectin mask solves the problem that a film forming agent in the existing peel-off mask can produce adverse influence on the skin. The red date pectin mask comprises 5 to 10% of red date pectin, 1 to 5% of glycerol, 5 to 10% of NaCl, 0.5 to 2% of Tween-80, 5 to 15% of stearic acid, 5 to 10% of 1, 3-butanediol, 0.1 to 0.5% of methylparaben, 0.5 to 1.5% of essence, 0.2 to 0.5% of polyethylene glycol distearate and the balance distilled water. The preparation method comprises the following steps of 1, uniformly dividing red date pectin powder into two parts, orderly mixing one of the two parts, polyethylene glycol distearate, glycerol and stearic acid, adding water into the mixture, and carrying out stirring heating until precipitates are dissolved fully, 2, carrying out ultrasonic crushing of the liquid obtained by the step 1 so that red date pectin is crushed and simultaneously, the crushed red date pectin and other materials in the solution are fully emulsified, and 3, adding the rest of the raw materials into the emulsion obtained by the step 2, and carrying out uniform mixing to obtain the red date pectin mask.
Description
Technical field
The present invention relates to cosmetic field, specifically is a kind of pectin mask product and preparation method thereof.
Background technology
Along with the raising of people's living standard, the maintenance of skin more becomes a kind of trend, and facial film is as a kind of cosmetics, being subjected to youngster pays close attention to greatly, facial film nutritious and the cleaning skin function, can provide the most sufficient nutrient to skin at short notice, skin is rejuvenated.Mask product is used more and more widely, and just nourishing nursing product by original deep layer becomes the operational maintenance product.Though mask product has the characteristics that can supplement the nutrients immediately, improve skin condition, for skin easily the responsive people always or worry arranged.At present, comparatively traditional peel off pack contains the film former polyvinyl alcohol more, easily causes cutis laxa, corse sweat pore, and to the people Yi Zaocheng allergy of responsive skin matter, the facial film safety upgrade also becomes the facial film fashion trend.The safety of face pack prescription also is need not or to lack with the chemical compound that makes people's allergy except composition uses natural plant extraction composition, active ingredient, natural minerals composition etc. as far as possible as far as possible.
Pectin is a kind of acidic polysaccharose material in the plant, and it is generally white to pale yellow powder, is with tart flavour slightly, has water solublity, and is industrial namely separable, its molecular weight about 50,000 one 30 ten thousand.Make gellant at food, thickening agent, stabilizing agent, suspending agent, emulsifying agent, the flavouring synergist, and can be used for cosmetics, and to protection skin, preventing ultraviolet radiation, looks improving and the skin nourishing is all deposited certain effect.Find no at present and use the report of pectin on cosmetics that Fructus Jujubae extracts.
Summary of the invention
The present invention overcomes in the prior art that the film former polyvinyl alcohol causes dysgenic deficiency to skin in the peel off pack, a kind of Fructus Jujubae pectin facial film and preparation method thereof is provided, the purpose of this invention is to provide a kind of novel pectin facial film that contains the high-activity natural material.This facial film is the gel-type facial film, and the gel-type facial film need cooperate the oils and fats with glossy degree and lock water, the visual effect that reaching skin has " having enough " by the composition of some high suctions usually.The macromole pectin that the present invention is difficult to absorb with the skin composition of preserving moisture, the micromolecule that replaces easily the absorbing composition of preserving moisture is to reach more obvious visual effect.Have elastic force preserve moisture, compact lift, effect such as skin-moisturizing, skin, wrinkle resistant defying age, anti-ultraviolet radiation.
The technical solution used in the present invention is as follows:
A kind of Fructus Jujubae pectin facial film, its prescription following (by mass percentage):
Fructus Jujubae pectin powder 5%-10%, effect is: bring into play natural polymer thickening agent, emulsifying agent, function of stabilizer, substituted the material of promotion film forming emulsifyings such as polyvinyl alcohol, triethanolamine;
Glycerol 1%-5%, effect is to lubricate, preserve moisture;
NaCl5%-10%, effect is antibiotic, thickening agent, stabilizing agent;
Tween 80 0.5%-2%, effect is dispersant, solubilizing agent, emulsifying agent;
Stearic acid 5%-15%, effect is excipient, stabilizing agent, emulsifying agent;
1,3 butanediol 5%-10%, act on the same with glycerol, moisture-keeping function;
Methyl hydroxybenzoate 0.1%-0.5% is as antibacterial;
Essence 0.5%-1.5%, effect is to tart up, different essence are in harmonious proportion out the mask product of diverse fragrant flavour;
Polyethylene glycol stearate diester 0.2%-0.5%, effect is thickening agent, emulsifying agent;
More than other addition agents except pectin all are with Fructus Jujubae pectin in the prescription, play synergism, to make the more superior effect of Fructus Jujubae pectin performance;
Surplus is distilled water.
When using Fructus Jujubae pectin of the present invention to carry out the daily facial-care of facial film, guarantee a face according to the personal considerations of each user and evenly smear fully and get final product.
The preparation method of above-mentioned Fructus Jujubae pectin facial film, step is as follows:
(1) with two parts of Fructus Jujubae pectin powder div in par aeq, a copy of it pectin is mixed successively with polyethylene glycol stearate diester, glycerol and stearic acid, add the low amounts of water agitating heating, to there not being deposit;
(2) the liquid ultrasonic grinding that obtains of step (1), make pectin pulverize simultaneously with liquid in other materials fully emulsified;
(3) add other a pectin again in the emulsion of step (2), and NaCl, tween 80, methyl hydroxybenzoate, 1,3 butanediol, essence and water, stir repeatedly, up to all substances mix homogeneously all, both Fructus Jujubae pectin mask product.
As preferably, the described thermal control temperature that adds of step (1) is 60 ℃-70 ℃.
As preferably, the described Ultrasonic Pulverization condition of step (2) is 20-25KHz, 400-2000W, Ultrasonic Pulverization 5min-10min.
As preferably, the described pectin of step (2) is pulverized to the pectin molecule amount is crushed to below 1000 dalton.
The present invention has following advantage: (1) is the pectin for preparing from Fructus Jujubae because of it, contains the distinctive active substances of Fructus Jujubae such as flavone, to replenishing skin-nourishing fabulous effect is arranged.
(2) Ultrasonic Pulverization part pectin, molecular weight diminishes and is conducive to skin absorbs, another part pectin that the back adds, performance natural polymer thickening agent, emulsifying agent, function of stabilizer, substitute the material of promotion film forming emulsifyings such as polyvinyl alcohol, triethanolamine, made facial film have no adverse effects to skin.
(3) except the effect with common facial film cleaning, skin care, also at nutrition, anti-ultraviolet radiation, whiten, preserve moisture and to repair aspect the skin effect obvious.
(4) cheaper than common facial film cost, and can take full advantage of resource, expand the Fructus Jujubae value.
Be rich in flavone compound in the Fructus Jujubae, it is a kind of very strong antioxidant, can effectively remove the oxygen-derived free radicals in the body, and it is more than ten times of vitamin E that this material stops the ability of oxidation, and it is 100% to the biological effectiveness of human body.The pectin that extracts from Fructus Jujubae is a lot of because of carboxyl on its strand, unique antioxidant in the easy bonding Fructus Jujubae, thus make Fructus Jujubae pectin have the not available special performance of other pectin.
The specific embodiment
Embodiment 1
Prescription is: Fructus Jujubae pectin powder (available from the U.S. pure bio tech ltd GZ type jelly powder in Nanjing) 10%, glycerol 5%, NaCl10%, tween 80 2%, stearic acid 15%, Metagin 0.5%, essence 1.5%, 1,3 butanediols 10%, polyethylene glycol stearate diester 0.5%, surplus is distilled water.
Its preparation method is:
(1) get two parts of pectin powder div in par aeq, a copy of it pectin and polyethylene glycol stearate diester, glycerol and stearic acid are put into container successively, add the water of 1 times of quality of mixture, agitating heating, 60 ℃ of temperature controls dissolve fully to all substances.
(2) step (1) liquid ultrasonic grinding instrument, ultrasonic 5min under 25KHz, 400W condition makes the pectin molecule amount be crushed to below 1000 dalton, and is simultaneously fully emulsified with other materials.
(3) add other a pectin again in the emulsion of step (2), and NaCl, tween 80, methyl hydroxybenzoate, 1,3 butanediol, essence, water, stir repeatedly, up to all substances mix homogeneously all, both Fructus Jujubae pectin mask product.
Embodiment 2
Fructus Jujubae pectin powder ((available from the U.S. pure bio tech ltd GZ type jelly powder in Nanjing) 5%, glycerol 1%, NaCl5%, tween 80 50%, stearic acid 5%, Metagin 0.1%, essence 0.5%, 1,3 butanediols 5%, polyethylene glycol stearate diester 0.2%, surplus is distilled water.
Its preparation method is:
(1) get two parts of a certain amount of pectin powder div in par aeq, a copy of it pectin and polyethylene glycol stearate diester, glycerol and stearic acid are put into container successively, add the water of 3 times of quality of mixture, agitating heating, 70 ℃ of temperature controls dissolve fully to all substances.
(2) step 1 liquid ultrasonic grinding instrument, ultrasonic 10min under 20KHz, 2000W condition makes the pectin molecule amount be crushed to 1000 dalton once, and is simultaneously fully emulsified with other materials.
(3) add other a pectin again in the emulsion of step 2, and NaCl, tween 80, methyl hydroxybenzoate, 1,3 butanediol, essence, water, stir repeatedly, up to all substances mix homogeneously all, both Fructus Jujubae pectin mask product.
Embodiment 3
Fructus Jujubae pectin powder (available from the U.S. pure bio tech ltd GZ type jelly powder in Nanjing) 7%, glycerol 3%, NaCl7%, tween 80 1%, stearic acid 10%, Metagin 0.3%, essence 1%, 1,3 butanediols 7%, polyethylene glycol stearate diester 0.4%, surplus is distilled water.
Its preparation method is:
(1) get two parts of a certain amount of pectin powder div in par aeq, a copy of it pectin and polyethylene glycol stearate diester, glycerol and stearic acid are put into container successively, add the water of 2 times of quality of mixture, agitating heating, 65 ℃ of temperature controls dissolve fully to all substances.
(2) step 1 liquid ultrasonic grinding instrument, ultrasonic 8min under 24KHz, 1200W condition makes the pectin molecule amount be crushed to 1000 dalton once, and is simultaneously fully emulsified with other materials.
(3) add other a pectin again in the emulsion of step 2, and NaCl, tween 80, methyl hydroxybenzoate, 1,3 butanediol, essence, water, stir repeatedly, up to all substances mix homogeneously all, both Fructus Jujubae pectin mask product.
Claims (5)
1. Fructus Jujubae pectin facial film is characterized in that: fill a prescription following (by mass percentage):
Fructus Jujubae pectin powder 5%-10%,
Glycerol 1%-5%,
NaCl?5%-10%，
Tween 80 0.5%-2%,
Stearic acid 5%-15%,
1,3 butanediol 5%-10%,
Methyl hydroxybenzoate 0.1%-0.5%,
Essence 0.5%-1.5%,
Polyethylene glycol stearate diester 0.2%-0.5%,
Surplus is distilled water.
2. the preparation method of Fructus Jujubae pectin facial film according to claim 1, it is characterized in that: step is as follows:
(1) with two parts of Fructus Jujubae pectin powder div in par aeq, a copy of it pectin mixed successively obtaining mixture with polyethylene glycol stearate diester, glycerol and stearic acid, add water, agitating heating is to there not being deposit;
(2) the liquid ultrasonic grinding that obtains of step (1), make pectin pulverize simultaneously with liquid in other materials fully emulsified;
(3) add other a pectin again in the emulsion of step (2), and NaCl, tween 80, methyl hydroxybenzoate, 1,3 butanediol, essence and water, stir repeatedly, up to all substances mix homogeneously all, both Fructus Jujubae pectin mask product.
3. the preparation method of Fructus Jujubae pectin facial film according to claim 2 is characterized in that: the water of the described adding of step (1) be mixture quality 1-3 doubly; The described thermal control temperature that adds is 60 ℃-70 ℃.
4. the preparation method of Fructus Jujubae pectin facial film according to claim 2, it is characterized in that: the described Ultrasonic Pulverization condition of step (2) is 20-25KHz, 400-2000W, Ultrasonic Pulverization 5min-10min.
5. the preparation method of Fructus Jujubae pectin facial film according to claim 2 is characterized in that: the described pectin of step 2 is pulverized to the pectin molecule amount is crushed to below 1000 dalton.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310207917.4A CN103315928B (en) | 2013-05-28 | 2013-05-28 | Red date pectin mask and preparation method thereof |
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| CN201310207917.4A CN103315928B (en) | 2013-05-28 | 2013-05-28 | Red date pectin mask and preparation method thereof |
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| CN103315928B CN103315928B (en) | 2014-08-27 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104739684A (en) * | 2013-12-25 | 2015-07-01 | 廖展昌 | Preparation method and application of jelly fig pectin composition |
| CN104840407A (en) * | 2015-05-18 | 2015-08-19 | 安徽宇宁生物科技有限公司 | Pectin mask and preparation method thereof |
| CN105193654A (en) * | 2015-09-24 | 2015-12-30 | 吴莹 | Aloe pectin |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1065427C (en) * | 1996-11-26 | 2001-05-09 | 李建民 | Mask type nutrient face-pack and preparing process thereof |
| KR20090111719A (en) * | 2008-04-22 | 2009-10-27 | (주)더페이스샵코리아 | Cosmetic Compositions for whitening Skin containing jujube culture |
| KR20110100452A (en) * | 2010-03-04 | 2011-09-14 | 배화여자대학 산학협력단 | Solid type beauty pack and method for manufacturing the solid type beauty pack thereof |
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2013
- 2013-05-28 CN CN201310207917.4A patent/CN103315928B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1065427C (en) * | 1996-11-26 | 2001-05-09 | 李建民 | Mask type nutrient face-pack and preparing process thereof |
| KR20090111719A (en) * | 2008-04-22 | 2009-10-27 | (주)더페이스샵코리아 | Cosmetic Compositions for whitening Skin containing jujube culture |
| KR20110100452A (en) * | 2010-03-04 | 2011-09-14 | 배화여자대학 산학협력단 | Solid type beauty pack and method for manufacturing the solid type beauty pack thereof |
Non-Patent Citations (1)
| Title |
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| 曾晓君 等: "中药免洗面膜的研制", 《广东化工》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104739684A (en) * | 2013-12-25 | 2015-07-01 | 廖展昌 | Preparation method and application of jelly fig pectin composition |
| CN104840407A (en) * | 2015-05-18 | 2015-08-19 | 安徽宇宁生物科技有限公司 | Pectin mask and preparation method thereof |
| CN105193654A (en) * | 2015-09-24 | 2015-12-30 | 吴莹 | Aloe pectin |
| CN105193654B (en) * | 2015-09-24 | 2018-08-24 | 吴莹 | Aloe pectin |
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| CN103315928B (en) | 2014-08-27 |
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Effective date of registration: 20211222 Address after: Room 407-2-6, building C, Tian'an Digital City, 588 Changwu South Road, Wujin high tech Industrial Development Zone, Changzhou City, Jiangsu Province 213100 Patentee after: CHANGZHOU XIAOGUO INFORMATION SERVICES Co.,Ltd. Address before: Gehu Lake Road Wujin District 213164 Jiangsu city of Changzhou province No. 1 Patentee before: CHANGZHOU University |
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