CN103313771B - 采用离子液体脱水的方法 - Google Patents
采用离子液体脱水的方法 Download PDFInfo
- Publication number
- CN103313771B CN103313771B CN201180063325.9A CN201180063325A CN103313771B CN 103313771 B CN103313771 B CN 103313771B CN 201180063325 A CN201180063325 A CN 201180063325A CN 103313771 B CN103313771 B CN 103313771B
- Authority
- CN
- China
- Prior art keywords
- ionic liquid
- medium
- aqueous medium
- dry
- aqueous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000002608 ionic liquid Substances 0.000 title claims abstract description 85
- 238000000034 method Methods 0.000 title claims abstract description 49
- 230000018044 dehydration Effects 0.000 title claims description 5
- 238000006297 dehydration reaction Methods 0.000 title claims description 5
- 239000012736 aqueous medium Substances 0.000 claims abstract description 40
- 239000002609 medium Substances 0.000 claims abstract description 27
- 239000004381 Choline salt Substances 0.000 claims abstract description 26
- 235000019417 choline salt Nutrition 0.000 claims abstract description 26
- 150000003248 quinolines Chemical class 0.000 claims abstract description 25
- 239000007788 liquid Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 42
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 25
- 238000001035 drying Methods 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 15
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 239000012530 fluid Substances 0.000 claims description 7
- 239000001569 carbon dioxide Substances 0.000 claims description 5
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 4
- 238000004064 recycling Methods 0.000 claims description 4
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 claims description 3
- 229960001231 choline Drugs 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 235000013361 beverage Nutrition 0.000 abstract description 2
- 235000013305 food Nutrition 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000002417 nutraceutical Substances 0.000 abstract description 2
- 235000021436 nutraceutical agent Nutrition 0.000 abstract description 2
- 239000008194 pharmaceutical composition Substances 0.000 abstract description 2
- MIFGTXFTLQVWJW-UHFFFAOYSA-M 2-hydroxyethyl(trimethyl)azanium;2-hydroxypropanoate Chemical group CC(O)C([O-])=O.C[N+](C)(C)CCO MIFGTXFTLQVWJW-UHFFFAOYSA-M 0.000 description 19
- 239000002274 desiccant Substances 0.000 description 11
- 239000007789 gas Substances 0.000 description 11
- 230000000694 effects Effects 0.000 description 10
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 9
- 240000003768 Solanum lycopersicum Species 0.000 description 9
- 239000004215 Carbon black (E152) Substances 0.000 description 4
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 4
- 229910021536 Zeolite Inorganic materials 0.000 description 4
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000010457 zeolite Substances 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- AEMRFAOFKBGASW-UHFFFAOYSA-M Glycolate Chemical compound OCC([O-])=O AEMRFAOFKBGASW-UHFFFAOYSA-M 0.000 description 2
- -1 N,N,N-trimethylethanolammonium cation Chemical class 0.000 description 2
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000002538 fungal effect Effects 0.000 description 2
- 230000036571 hydration Effects 0.000 description 2
- 238000006703 hydration reaction Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- AFENDNXGAFYKQO-UHFFFAOYSA-N 2-hydroxybutyric acid Chemical compound CCC(O)C(O)=O AFENDNXGAFYKQO-UHFFFAOYSA-N 0.000 description 1
- LVZWSLJZHVFIQJ-UHFFFAOYSA-N Cyclopropane Chemical compound C1CC1 LVZWSLJZHVFIQJ-UHFFFAOYSA-N 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- MDOAAHGPXOGVQG-UHFFFAOYSA-N ethene;propane Chemical compound C=C.CCC MDOAAHGPXOGVQG-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000000887 hydrating effect Effects 0.000 description 1
- 239000011244 liquid electrolyte Substances 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- XLOUGJKOJPVZMT-UHFFFAOYSA-N n-ethyl-n-methylethanamine;sulfuric acid Chemical compound OS([O-])(=O)=O.CC[NH+](C)CC XLOUGJKOJPVZMT-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- 239000001272 nitrous oxide Substances 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- TVBIVRGNYNBFCD-UHFFFAOYSA-N triethylazanium;trifluoromethanesulfonate Chemical compound CC[NH+](CC)CC.[O-]S(=O)(=O)C(F)(F)F TVBIVRGNYNBFCD-UHFFFAOYSA-N 0.000 description 1
- 230000004584 weight gain Effects 0.000 description 1
- 235000019786 weight gain Nutrition 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B7/00—Preservation of fruit or vegetables; Chemical ripening of fruit or vegetables
- A23B7/02—Dehydrating; Subsequent reconstitution
- A23B7/022—Dehydrating; Subsequent reconstitution with addition of chemicals before or during drying, e.g. semi-moist products
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/10—Preservation of foods or foodstuffs, in general by treatment with pressure variation, shock, acceleration or shear stress
- A23B2/103—Preservation of foods or foodstuffs, in general by treatment with pressure variation, shock, acceleration or shear stress using sub- or super-atmospheric pressures, or pressure variations transmitted by a liquid or gas
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/70—Preservation of foods or foodstuffs, in general by treatment with chemicals
- A23B2/725—Preservation of foods or foodstuffs, in general by treatment with chemicals in the form of liquids or solids
- A23B2/729—Organic compounds; Microorganisms; Enzymes
- A23B2/762—Organic compounds containing nitrogen
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/90—Preservation of foods or foodstuffs, in general by drying or kilning; Subsequent reconstitution
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B2/00—Preservation of foods or foodstuffs, in general
- A23B2/90—Preservation of foods or foodstuffs, in general by drying or kilning; Subsequent reconstitution
- A23B2/91—Preservation of foods or foodstuffs, in general by drying or kilning; Subsequent reconstitution with addition of chemicals before or during drying
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B7/00—Preservation of fruit or vegetables; Chemical ripening of fruit or vegetables
- A23B7/02—Dehydrating; Subsequent reconstitution
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B7/00—Preservation of fruit or vegetables; Chemical ripening of fruit or vegetables
- A23B7/02—Dehydrating; Subsequent reconstitution
- A23B7/0205—Dehydrating; Subsequent reconstitution by contact of the material with fluids, e.g. drying gas or extracting liquids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
- B01D53/263—Drying gases or vapours by absorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
- B01D53/28—Selection of materials for use as drying agents
Landscapes
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Analytical Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Drying Of Gases (AREA)
- Extraction Or Liquid Replacement (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10197431 | 2010-12-30 | ||
| EP10197431.9 | 2010-12-30 | ||
| PCT/NL2011/050909 WO2012091572A1 (en) | 2010-12-30 | 2011-12-28 | Dehydration process that employs an ionic liquid choline salt |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103313771A CN103313771A (zh) | 2013-09-18 |
| CN103313771B true CN103313771B (zh) | 2015-07-15 |
Family
ID=43981119
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201180063325.9A Expired - Fee Related CN103313771B (zh) | 2010-12-30 | 2011-12-28 | 采用离子液体脱水的方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20130326903A1 (enExample) |
| EP (1) | EP2658634B1 (enExample) |
| JP (1) | JP2014505586A (enExample) |
| CN (1) | CN103313771B (enExample) |
| AU (1) | AU2011353205A1 (enExample) |
| BR (1) | BR112013016778A2 (enExample) |
| CA (1) | CA2819579A1 (enExample) |
| WO (1) | WO2012091572A1 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103467245B (zh) * | 2013-09-23 | 2015-07-01 | 河北科技大学 | 一种利用低共熔溶剂络合脱除乙醇水混合溶液中水分的方法 |
| KR101799871B1 (ko) | 2016-02-19 | 2017-11-22 | 한남대학교 산학협력단 | 이온성 액체를 이용한 슬러지 함수율 저감방법 |
| CN106076078A (zh) * | 2016-08-22 | 2016-11-09 | 苏州迈沃环保工程有限公司 | 用以调控气体湿度的离子液除湿方法与系统 |
| JP7371861B2 (ja) * | 2019-11-11 | 2023-10-31 | 中部電力株式会社 | 吸湿材 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1310543A1 (en) * | 2001-11-07 | 2003-05-14 | Haldor Topsoe A/S | Process for the drying of a hydrocarbon stream |
| WO2008147181A1 (en) * | 2007-05-18 | 2008-12-04 | Technische Universiteit Delft | A method for the removal of a gas from a process gas stream by means of liquid crystals |
| EP2093278A1 (de) * | 2008-02-05 | 2009-08-26 | Evonik Goldschmidt GmbH | Performance-Additive zur Verbesserung der Benetzungseigenschaften von ionischen Flüssigkeiten auf festen Oberflächen |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4887335U (enExample) * | 1972-01-26 | 1973-10-22 | ||
| JPS61221299A (ja) * | 1985-03-28 | 1986-10-01 | 昭和炭酸株式会社 | 動植物材料から有機質成分を抽出・分離する方法 |
| US6534075B1 (en) * | 1999-03-26 | 2003-03-18 | Ecolab Inc. | Antimicrobial and antiviral compositions and treatments for food surfaces |
| US6797291B2 (en) * | 2002-01-09 | 2004-09-28 | Balchem Corporation | Stable hygroscopic compositions and methods for stabilizing hygroscopic ingredients |
| US20030180249A1 (en) * | 2002-03-18 | 2003-09-25 | Khanna Satish Chandra | Dosage forms for hygroscopic active ingredients |
| ATE297368T1 (de) | 2002-04-18 | 2005-06-15 | Haldor Topsoe As | Kontinuierliches verfahren zur trennung von wasser von einer kohlenwasserstoffbeschickung |
| US20060150892A1 (en) * | 2003-04-29 | 2006-07-13 | Akzo Nobel N.V. | Processes Involving the Use of Antisolvent Crystallisation |
| KR100466637B1 (ko) * | 2003-06-26 | 2005-01-13 | 주식회사 펩트론 | 서방성 미립구의 혼합 제형을 연속한 단일 공정으로제조하는 방법 |
| FR2866345B1 (fr) * | 2004-02-13 | 2006-04-14 | Inst Francais Du Petrole | Procede de traitement d'un gaz naturel avec extraction du solvant contenu dans le gaz naturel purifie |
| ES2333605T3 (es) * | 2004-06-16 | 2010-02-24 | FEYECON DEVELOPMENT & IMPLEMENTATION B.V. | Metodo de deshidratacion. |
| JP2006142121A (ja) * | 2004-11-16 | 2006-06-08 | Daikin Ind Ltd | 空気処理装置 |
| US20070128243A1 (en) * | 2005-12-02 | 2007-06-07 | Xylos Corporation | Implantable microbial cellulose materials for various medical applications |
| JP2008162899A (ja) * | 2006-12-27 | 2008-07-17 | Tokyo Univ Of Agriculture & Technology | 生体関連化合物からなるイオン液体 |
-
2011
- 2011-12-28 CN CN201180063325.9A patent/CN103313771B/zh not_active Expired - Fee Related
- 2011-12-28 CA CA2819579A patent/CA2819579A1/en not_active Abandoned
- 2011-12-28 BR BR112013016778A patent/BR112013016778A2/pt not_active IP Right Cessation
- 2011-12-28 JP JP2013547381A patent/JP2014505586A/ja active Pending
- 2011-12-28 AU AU2011353205A patent/AU2011353205A1/en not_active Abandoned
- 2011-12-28 EP EP11817430.9A patent/EP2658634B1/en not_active Not-in-force
- 2011-12-28 US US13/976,297 patent/US20130326903A1/en not_active Abandoned
- 2011-12-28 WO PCT/NL2011/050909 patent/WO2012091572A1/en not_active Ceased
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1310543A1 (en) * | 2001-11-07 | 2003-05-14 | Haldor Topsoe A/S | Process for the drying of a hydrocarbon stream |
| WO2008147181A1 (en) * | 2007-05-18 | 2008-12-04 | Technische Universiteit Delft | A method for the removal of a gas from a process gas stream by means of liquid crystals |
| EP2093278A1 (de) * | 2008-02-05 | 2009-08-26 | Evonik Goldschmidt GmbH | Performance-Additive zur Verbesserung der Benetzungseigenschaften von ionischen Flüssigkeiten auf festen Oberflächen |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2658634A1 (en) | 2013-11-06 |
| BR112013016778A2 (pt) | 2017-06-20 |
| JP2014505586A (ja) | 2014-03-06 |
| US20130326903A1 (en) | 2013-12-12 |
| AU2011353205A2 (en) | 2013-07-11 |
| CA2819579A1 (en) | 2012-07-05 |
| EP2658634B1 (en) | 2016-03-23 |
| CN103313771A (zh) | 2013-09-18 |
| AU2011353205A1 (en) | 2013-07-11 |
| WO2012091572A1 (en) | 2012-07-05 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150715 Termination date: 20161228 |