CN103304137A - Method for producing lead-free frosted glass wine bottle - Google Patents
Method for producing lead-free frosted glass wine bottle Download PDFInfo
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- CN103304137A CN103304137A CN 201310230626 CN201310230626A CN103304137A CN 103304137 A CN103304137 A CN 103304137A CN 201310230626 CN201310230626 CN 201310230626 CN 201310230626 A CN201310230626 A CN 201310230626A CN 103304137 A CN103304137 A CN 103304137A
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Abstract
The invention discloses a method for producing a lead-free frosted glass wine bottle. The product belongs to the field of glass manufacturing. The method comprises the steps of: by taking lead-free white cullet, white quartz sand, sodium carbonate, soda feldspar, calcite, anhydrous sodium sulphate and cobalt powder as materials and taking a washing machine, a mixing machine, a boiler, a kiln, a molding machine, an annealing box and a frosted glass box as equipments, preparing the lead-free frosted glass wine bottle after washing the lead-free white cullet, mixing, fusing, molding, annealing and frosting all materials. The product has the advantages that main materials are recovered waste lead-free glass products, and are low in price; the quartz sand is abundant in real estate resource source; the product does not contain toxic elements such as lead, arsenic and chromium, and is free of harm to a human body; the product is various in sculpt, and beautiful in appearance; the product is mainly used as fast-moving consumer goods wrappers, such as white spirit, yellow wine and red wine.
Description
Technical field
The invention belongs to glass manufacturing area, relate in particular to a kind of production method of unleaded mat glass bottle.
Background technology
Glass is a kind of transparent or semitransparent solid matter, when fusion, form the contiguous network structure, the process of cooling medium viscosity increases and sclerosis and non crystallized silicates non-metallic material gradually, principal item is silicate glass, wherein silicate glass refers to that basal component is the glass of silicon-dioxide, wherein the content of silicon-dioxide is between 55%-65%, also contain 15% sodium oxide, 15% calcium oxide and a certain amount of plumbous oxide, because it contains a certain amount of lead, if directly be used for making tea set, drinking utensils, bottle, the people is plumbous in the process of drink tea or wine just might to enter human body, there is part can pass through ight soil although enter the lead of human body, sweat is drained, but still have the lead of part will dissolve in blood, hinder the synthetic of blood, cause the human body anaemia, headache occurs, dizzy, weak, sleepy, constipation and limb aching pain etc., and then cause arteriosclerosis, symptom such as digestive tract ulcer and retinal hemorrhage is plumbous bigger to children and pregnant woman's toxicity.Along with the enhancing of people to environmental consciousness, use the crown glass vessel to become people's common recognition.Crown glass has its following advantage than flint glass: it is more melodized that crown glass knocks the metallic ring that sends than flint glass; Crown glass than flint glass vessel more flexible be the impact resistance performance; It is nontoxic that crown glass is used for making tea set, drinking utensils, kitchen vessel than flint glass.Product of the present invention is a kind of unleaded mat glass bottle, namely the crown glass bottle of producing is made through frosting technology again, colourless transparent glass presents the oyster white sensation after frosted, its distinguishing feature is that the surface is fine and smooth, printing opacity is opaque, dim sense is arranged, and the mat glass bottle is compared except transparency with the original hase glass wine bottle on capability and performance, and other are constant substantially.Two big advantages are arranged after the unleaded mat glass bottle of product uses: the one and general transparent glass wine bottle compare attractive in appearance; The 2nd, printing opacity is opaque, avoid the light direct projection in the bottle wine so that cause the volatilization of wine and rotten.The frosting technology of bottle has two classes, the one, pickling process, the 2nd, with the frosted of frosted machinery, the frosted of frosted machinery is compared with pickling process, have cost low, pollution-free, to series of advantages such as operator ' s health are harmless.Product of the present invention is a kind of production method of unleaded mat glass bottle, it is that not have lead white glass cullet, white quartz sand (iron-holder 0.15≤‰), soda ash, albite (iron-holder 0.25≤‰), calcite (iron-holder 0.15≤‰), Sodium sulfate anhydrous.min(99), cobalt powder be raw material, be equipment with rinsing machine, blending machine, boiler, kiln, shaper, annealing box, frosted case, by the washing of no lead white glass cullet, all make unleaded mat glass bottle after the mixing, fusion, moulding, annealing, frosted of raw materials.The advantage of product is: the waste and old crown glass goods of main raw material for reclaiming, and cheap; Quartz sand is that the real estate resources source is abundant; Poisonous elements such as not leaded in the product, arsenic, chromium, harmless; Product-forming is various, good looking appearance; Product is mainly as the packing material of fast-moving consumer goods such as liquor, yellow rice wine, red wine, and the product recyclable utilization in back of finishing using is environment friendly and pollution-free.
Summary of the invention:
It is the method that main raw material is produced unleaded mat glass bottle in batches with the no lead white glass cullet of purchase, white quartz sand that the problem that the present invention mainly solves provides a kind of, the unleaded mat glass bottle that this method is produced is exquisite in workmanship, specious, printing opacity is opaque, stable chemical performance, not leaded, and product is mainly as the packing material of fast-moving consumer goods such as liquor, yellow rice wine, red wine.The raw material weight proportioning that the present invention uses is: no lead white glass cullet 44%-46%, real estate quartz sand 28%-30%, soda ash 9%, albite 12%, calcite 4.6%, Sodium sulfate anhydrous.min(99) 0.2%, cobalt powder 0.2%.
The present invention can be achieved through the following technical solutions:
A kind of method of producing unleaded mat glass bottle in batches is characterized in that being made of following steps:
(1) the no lead white glass cullet that will purchase are sent into rinsing machine and are washed repeatedly with high pressure water, and dry naturally the flushing back.
(2) no lead white glass cullet, real estate quartz sand, soda ash, albite, calcite, Sodium sulfate anhydrous.min(99), the cobalt powder cleaned of formula ratio are sent into blending machine even blend and obtain compound, by transfer roller compound is sent into kiln.
(3) coal is sent into boiler combustion, 540 ℃-560 ℃ the coal gas that burning obtains is sent into kiln sealing combustion in kiln by the coal gas gas pipe line, make the temperature of compound reach 1550 ℃-1560 ℃, kept this temperature 26-28 hour, make compound reach molten state, obtain the crown glass molten mass.
(4) the crown glass molten mass is sent into shaper, control moulding built-in temperature is 1020 ℃-1080 ℃, makes the crown glass bottle of certain specification.
Send into annealing box with transfer roller when (5) the crown glass bottle of moulding being cooled to 700 ℃ naturally, annealing the temperature inside the box is 680-700 ℃, 2.5-3.0 hour time of process cools the temperature to about 150 ℃ then, this moment, annealing finished, the crown glass bottle is sent in the air, in air, naturally cooled to normal temperature.
(6) the crown glass bottle is sent into skin grinder, spray to the crown glass bottle of rotation at a high speed less than 40 purpose quartz sands with granularity, finish through frosting technology after 3-4 minute the sandblast, frosted crown glass bottle is sent into the unleaded mat glass bottle that gets product after rinsing machine is washed.
(7) using method of this unleaded mat glass bottle is: as the packing material of low and middle-grade liquor, yellow rice wine, red wine.
The temperature of fusion of compound is 1555 ℃ in the kiln described in the above-mentioned steps (3).
Annealing time in the annealing box described in the above-mentioned steps (5) is 2.75 hours.
The invention has the beneficial effects as follows: provide a kind of method of producing unleaded mat glass bottle in batches, the characteristics that this method has that technology is simple, starting material convenient sources, production cost are low, pollution-free, be fit to suitability for industrialized production; The unleaded mat glass bottle of product can be used as the packing material of low and middle-grade liquor, yellow rice wine, and product is not leaded, the recyclable utilization in back of finishing using.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1
The no lead white glass cullet of purchase are sent into rinsing machine wash repeatedly with high pressure water, dry naturally the flushing back.
Be 44% no lead white glass cullet of cleaning with accounting for total amount, to account for total amount be 30% real estate quartz sand, account for total amount is 9% soda ash, account for total amount is 12% albite, account for total amount is 4.6% calcite, account for total amount is 0.2% Sodium sulfate anhydrous.min(99), account for total amount is that 0.2% cobalt powder is sent into blending machine even blend and obtained compound, by transfer roller compound sent into kiln.Coal is sent into boiler combustion, 540 ℃-560 ℃ the coal gas that burning obtains is sent into kiln sealing combustion in kiln by the coal gas gas pipe line, makes the temperature of compound reach 1550 ℃, keeps this temperature 28 hours, make compound reach molten state, obtain the crown glass molten mass.The crown glass molten mass is sent into shaper, and control moulding built-in temperature is 1020 ℃-1080 ℃, makes the crown glass bottle of certain specification.When being cooled to 700 ℃ naturally, the crown glass bottle of moulding sends into annealing box with transfer roller, annealing the temperature inside the box is 680 ℃, cools the temperature to about 150 ℃ through time of 2.5 hours then, and this moment, annealing finished, the crown glass bottle is sent in the air, in air, naturally cooled to normal temperature.The crown glass bottle is sent into skin grinder, spray to the crown glass bottle of rotation at a high speed less than 40 purpose quartz sands with granularity, finish through frosting technology after 3-4 minute the sandblast, frosted crown glass bottle is sent into the unleaded mat glass bottle that gets product after rinsing machine is washed.The using method of this unleaded mat glass bottle is: as the packing material of low and middle-grade liquor, yellow rice wine, red wine.
Embodiment 2
The no lead white glass cullet of purchase are sent into rinsing machine wash repeatedly with high pressure water, dry naturally the flushing back.
Be 45% no lead white glass cullet of cleaning with accounting for total amount, to account for total amount be 29% real estate quartz sand, account for total amount is 9% soda ash, account for total amount is 12% albite, account for total amount is 4.6% calcite, account for total amount is 0.2% Sodium sulfate anhydrous.min(99), account for total amount is that 0.2% cobalt powder is sent into blending machine even blend and obtained compound, by transfer roller compound sent into kiln.Coal is sent into boiler combustion, 540 ℃-560 ℃ the coal gas that burning obtains is sent into kiln sealing combustion in kiln by the coal gas gas pipe line, makes the temperature of compound reach 1555 ℃, keeps this temperature 27 hours, make compound reach molten state, obtain the crown glass molten mass.The crown glass molten mass is sent into shaper, and control moulding built-in temperature is 1020 ℃-1080 ℃, makes the crown glass bottle of certain specification.When being cooled to 700 ℃ naturally, the crown glass bottle of moulding sends into annealing box with transfer roller, annealing the temperature inside the box is 690 ℃, cool the temperature to about 150 ℃ through time of 2.75 hours then, this moment, annealing finished, the crown glass bottle is sent in the air, in air, naturally cooled to normal temperature.The crown glass bottle is sent into skin grinder, spray to the crown glass bottle of rotation at a high speed less than 40 purpose quartz sands with granularity, finish through frosting technology after 3-4 minute the sandblast, frosted crown glass bottle is sent into the unleaded mat glass bottle that gets product after rinsing machine is washed.The using method of this unleaded mat glass bottle is: as the packing material of low and middle-grade liquor, yellow rice wine, red wine.
Embodiment 3
The no lead white glass cullet of purchase are sent into rinsing machine wash repeatedly with high pressure water, dry naturally the flushing back.
Be 46% no lead white glass cullet of cleaning with accounting for total amount, to account for total amount be 28% real estate quartz sand, account for total amount is 9% soda ash, account for total amount is 12% albite, account for total amount is 4.6% calcite, account for total amount is 0.2% Sodium sulfate anhydrous.min(99), account for total amount is that 0.2% cobalt powder is sent into blending machine even blend and obtained compound, by transfer roller compound sent into kiln.Coal is sent into boiler combustion, 540 ℃-560 ℃ the coal gas that burning obtains is sent into kiln sealing combustion in kiln by the coal gas gas pipe line, the temperature of compound is reached-1560 ℃, keeps this temperature 26 hours, make compound reach molten state, obtain the crown glass molten mass.The crown glass molten mass is sent into shaper, and control moulding built-in temperature is 1020 ℃-1080 ℃, makes the crown glass bottle of certain specification.When being cooled to 700 ℃ naturally, the crown glass bottle of moulding sends into annealing box with transfer roller, annealing the temperature inside the box is 700 ℃, cools the temperature to about 150 ℃ through time of 3.0 hours then, and this moment, annealing finished, the crown glass bottle is sent in the air, in air, naturally cooled to normal temperature.The crown glass bottle is sent into skin grinder, spray to the crown glass bottle of rotation at a high speed less than 40 purpose quartz sands with granularity, finish through frosting technology after 3-4 minute the sandblast, frosted crown glass bottle is sent into the unleaded mat glass bottle that gets product after rinsing machine is washed.The using method of this unleaded mat glass bottle is: as the packing material of low and middle-grade liquor, yellow rice wine, red wine.
Claims (4)
1. the production method of a unleaded mat glass bottle, its composition of raw materials is counted by weight percentage: comprise no lead white glass cullet 44%-46%, real estate quartz sand 28%-30%, soda ash 9%, albite 12%, calcite 4.6%, Sodium sulfate anhydrous.min(99) 0.2%, cobalt powder 0.2%; It is characterized in that:
The no lead white glass cullet that step (1) will be purchased are sent into rinsing machine and are washed repeatedly with high pressure water, and dry naturally the flushing back;
Step (2) is sent no lead white glass cullet, real estate quartz sand, soda ash, albite, calcite, Sodium sulfate anhydrous.min(99), the cobalt powder cleaned of formula ratio into blending machine even blend and is obtained compound, by transfer roller compound is sent into kiln;
Step (3) is sent coal into boiler combustion, 540 ℃-560 ℃ the coal gas that burning obtains is sent into kiln sealing combustion in kiln by the coal gas gas pipe line, make the temperature of compound reach 1550 ℃-1560 ℃, kept this temperature 26-28 hour, make compound reach molten state, obtain the crown glass molten mass;
Step (4) is sent the crown glass molten mass into shaper, and control moulding built-in temperature is 1020 ℃-1080 ℃, makes the crown glass bottle of certain specification;
When being cooled to 700 ℃ naturally with the crown glass bottle of moulding, step (5) sends into annealing box with transfer roller, annealing the temperature inside the box is 680-700 ℃, 2.5-3.0 hour time of process cools the temperature to about 150 ℃ then, this moment, annealing finished, the crown glass bottle is sent in the air, in air, naturally cooled to normal temperature;
Step (6) is sent the crown glass bottle into skin grinder, spray to the crown glass bottle of rotation at a high speed less than 40 purpose quartz sands with granularity, finish through frosting technology after 3-4 minute the sandblast, frosted crown glass bottle is sent into the unleaded mat glass bottle that gets product after rinsing machine is washed.
2. the production method of a kind of unleaded mat glass bottle according to claim 1, its step (3) feature is: the temperature of fusion of compound is 1555 ℃ in the described kiln.
3. the production method of a kind of unleaded mat glass bottle according to claim 1, its step (5) feature is: the annealing time in the described annealing box is 2.75 hours.
4. the production method of a kind of unleaded mat glass bottle according to claim 1, this unleaded mat glass bottle using method is: as the packing material of low and middle-grade liquor, yellow rice wine, red wine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201310230626 CN103304137A (en) | 2013-06-10 | 2013-06-10 | Method for producing lead-free frosted glass wine bottle |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 201310230626 CN103304137A (en) | 2013-06-10 | 2013-06-10 | Method for producing lead-free frosted glass wine bottle |
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| CN103304137A true CN103304137A (en) | 2013-09-18 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104445941A (en) * | 2014-12-08 | 2015-03-25 | 新沂市新奥特玻璃制品有限公司 | Production method and decoration firing process of lead-free glass bottle |
| CN110590159A (en) * | 2019-10-19 | 2019-12-20 | 徐州宏华玻璃科技有限公司 | Formula and manufacturing method of lead-free glass with better environmental protection |
-
2013
- 2013-06-10 CN CN 201310230626 patent/CN103304137A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104445941A (en) * | 2014-12-08 | 2015-03-25 | 新沂市新奥特玻璃制品有限公司 | Production method and decoration firing process of lead-free glass bottle |
| CN104445941B (en) * | 2014-12-08 | 2016-04-13 | 新沂市新奥特玻璃制品有限公司 | A kind of making method of crown glass bottle and enamel firing process |
| CN110590159A (en) * | 2019-10-19 | 2019-12-20 | 徐州宏华玻璃科技有限公司 | Formula and manufacturing method of lead-free glass with better environmental protection |
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Application publication date: 20130918 |