CN103301219B - Traditional Chinese medicine snow pear lozenge and preparation method thereof - Google Patents
Traditional Chinese medicine snow pear lozenge and preparation method thereof Download PDFInfo
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- CN103301219B CN103301219B CN201310251744.6A CN201310251744A CN103301219B CN 103301219 B CN103301219 B CN 103301219B CN 201310251744 A CN201310251744 A CN 201310251744A CN 103301219 B CN103301219 B CN 103301219B
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- 241000287420 Pyrus x nivalis Species 0.000 title claims abstract description 41
- 239000003814 drug Substances 0.000 title claims abstract description 24
- 239000007937 lozenge Substances 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 241000220324 Pyrus Species 0.000 claims abstract description 55
- 239000007788 liquid Substances 0.000 claims abstract description 38
- 235000000346 sugar Nutrition 0.000 claims abstract description 26
- 239000011248 coating agent Substances 0.000 claims abstract description 22
- 238000000576 coating method Methods 0.000 claims abstract description 22
- 235000014443 Pyrus communis Nutrition 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 238000009501 film coating Methods 0.000 claims abstract description 3
- 235000021017 pears Nutrition 0.000 claims description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 31
- 239000008187 granular material Substances 0.000 claims description 30
- 239000000843 powder Substances 0.000 claims description 25
- 238000000034 method Methods 0.000 claims description 23
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 241000209051 Saccharum Species 0.000 claims description 11
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 7
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical group C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 claims description 6
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 5
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 5
- 235000019359 magnesium stearate Nutrition 0.000 claims description 5
- 238000000643 oven drying Methods 0.000 claims description 5
- 239000008213 purified water Substances 0.000 claims description 5
- 238000005496 tempering Methods 0.000 claims description 5
- 239000007888 film coating Substances 0.000 claims description 2
- 239000006071 cream Substances 0.000 abstract description 5
- 239000010409 thin film Substances 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 238000004806 packaging method and process Methods 0.000 abstract description 2
- 238000007670 refining Methods 0.000 abstract description 2
- 230000007547 defect Effects 0.000 abstract 1
- 229940079593 drug Drugs 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 235000021552 granulated sugar Nutrition 0.000 abstract 1
- 239000000047 product Substances 0.000 description 11
- 230000000694 effects Effects 0.000 description 4
- 238000007664 blowing Methods 0.000 description 3
- 238000010348 incorporation Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000003826 tablet Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 2
- 238000012913 prioritisation Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940046011 buccal tablet Drugs 0.000 description 1
- 239000006189 buccal tablet Substances 0.000 description 1
- 229940126678 chinese medicines Drugs 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
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Abstract
The invention relates to a traditional Chinese medicine snow pear lozenge and a preparation method thereof, belonging to the technical field of a traditional Chinese medicine. The traditional Chinese medicine snow pear lozenge disclosed by the invention is characterized by comprising the following raw materials in parts by weight: 25-30 parts of snow pears, 50-60 parts of granulated sugar and 2-4 parts of thin film coating liquid. The preparation method comprises nine steps of: cleaning pear cream, refining sugar, drying, crushing, granulating, totally mixing, tabletting, coating and packaging. According to the traditional Chinese medicine snow pear lozenge disclosed by the invention, the defects of snow pear cream that the quality stability is poor and the snow pear cream is not easy to store are overcome; the quality of the prepared snow pear lozenge is stable and the content of medicines is accurate; the traditional Chinese medicine snow pear lozenge can be taken by being contained in a mouth, is good in mouth feel, is convenient to use, and is convenient to store and transport.
Description
Technical field
The invention discloses a kind of Traditional Chinese medicine snow pear lozenge and preparation method thereof, belong to technical field of Chinese medicines.
Background technology
At present, existing Traditional Chinese medicine snow pear product is soft extract, and the method step of employing comprises Fructus Pyri thin paste process, sugar refinery, receipts cream, fill, packaging five steps.(1) Fructus Pyri thin paste process: get pears and decoct with water secondary, amount of water is 18% of pears quality for the first time, decocts 3 hours; Second time amount of water is 65% of pears quality, decocts 2 hours.Merged by decocting liquid, cryoconcentration becomes clear paste, and clear paste 80 DEG C of Baume degrees recorded are 33 ~ 37 ° of B é; The Fructus Pyri thin paste concentrated is added appropriate water, is about the solution of 14 ° of B about é to Baume degrees, protect and boil 2 hours, staticly settle 24 hours, get supernatant and filter; (2) sugar refinery: get Saccharum Sinensis Roxb., be incorporated as the water of sugar amount 50%, heating is dissolved, and boils, and tempers to sugar liquid in golden yellow, with the Cheng Zhuwei degree that drips, and then adds appropriate water dilution, boils, leave standstill after 24 hours, filter, for subsequent use; (3) receive cream: add in Fructus Pyri thin paste filtrate by the sugared filtrate after refining, mixing, heating, is constantly stirred to and boils, concentrated, until record Baume degrees at 80 DEG C to be about 36 ° of B é; (4) fill: with the fill of cleaning glass bottle, shimming, screws bottle cap; (5) pack.The snow pear paste quality stability that prior art obtains is poor, and medicament contg is not accurate enough, in use, can not control taking dose accurately, and uses inconvenient, not easily stores.
Summary of the invention
The object of the invention is must be not enough in prior art in order to solve, and provide a kind of Traditional Chinese medicine snow pear lozenge and preparation method thereof, the Traditional Chinese medicine snow pear lozenge steady quality that the inventive method is obtained, medicament contg is accurate, in use, can control taking dose accurately.
To achieve these goals, the present invention is by the following technical solutions:
A kind of Traditional Chinese medicine snow pear lozenge, is characterized in that comprising the following raw material according to weight parts: 25-30 part pear, 50-60 part Saccharum Sinensis Roxb., 2-4 part film-coat liquid.
Further, its prioritization scheme is the following raw material that described film-coat liquid comprises according to weight parts: 10-20 part HPMC, 5-10 part PEG400,10-20 part propylene glycol, 2-20 part magnesium stearate, 500-800 part purified water.
The present invention also provides a kind of preparation method of Traditional Chinese medicine snow pear lozenge, it is characterized in that comprising the following steps:
(1) Fructus Pyri thin paste process: get pear and decoct with water secondary, amount of water is the 20-30% of pear quality for the first time, decocts 2-3 hour, obtains decocting liquid A; Second time amount of water is the 50-60% of pear quality, decocts 1-2 hour, obtains decocting liquid B; Collecting decoction A and decocting liquid B, cryoconcentration becomes Fructus Pyri thin paste, and Fructus Pyri thin paste 80 DEG C of Baume degrees recorded are 33 ~ 37 ° of B é;
(2) sugar refinery: get Saccharum Sinensis Roxb., be incorporated as the water of saccharic amount 50-60%, heating is dissolved, and boils, and it is golden yellow for spending for tempering to sugar liquid, obtains sugar refinery;
(3) dry: Fructus Pyri thin paste step (1) obtained becomes pears dry extract and sugared dry extract with step (2) sugar refinery oven drying;
(4) pulverize: the pears dry extract obtain step (3) and sugared dry extract high speed disintegrator are ground into fine powder, obtain pears fine powder and sugared fine powder;
(5) granulate: the pears fine powder obtain step (4) and sugared fine powder one-step-granulating method are directly made can the granule of tabletting, obtains pears granule and sugared granule;
(6) always mix: the pears granule obtain step (5) and sugared granule three-dimensional mixer mix homogeneously, obtain hybrid particles;
(7) tabletting: hybrid particles tabletting step (6) obtained, obtains snow pear slice element sheet;
(8) coating: step (7) is obtained snow pear slice element sheet, be placed in high-efficiency coating pot, obtain snow pear slice element sheet with film-coat liquid to step (7) and carry out film coating, coating temperature is 50 ~ 60 DEG C;
(9) pack.
Further, its prioritization scheme is that in step (5), one-step-granulating method inlet temperature is 180 ~ 210 DEG C, and transfusion frequency values is 30 ~ 45HZ.
Snow pear lozenge is buccal tablet because of it, and therefore its steady quality, medicament contg is accurate.Patient in use, can control taking dose accurately; Snow pear lozenge because of its can buccal, therefore compared with snow pear paste, what can continue for a long time acts on affected part, not only increases the effectiveness time, also enhances therapeutic effect.
Compared with prior art, its beneficial effect is in the present invention: (1) snow pear lozenge steady quality of the present invention, and medicament contg is accurate, makes patient in use, can control taking dose accurately; (2) this product can be taken containing change, and mouthfeel is good, and compared with snow pear paste, its effectiveness time is longer, and effect is better; (3) snow pear lozenge that the inventive method is obtained is easy to use, is convenient to storage, transport.
Specific embodiment
Below in conjunction with detailed description of the invention, the invention will be further described.
Embodiment 1
A kind of Traditional Chinese medicine snow pear lozenge, comprises the following raw material according to weight parts: 30 portions of pears, 60 parts of Saccharum Sinensis Roxb., 4 parts of film-coat liquid.
Take with 10 of weight parts parts of HPMC, 5 parts of PEG400,10 parts of propylene glycol, 2 parts of magnesium stearate, then add 500 parts of purified water, stir, obtain film-coat liquid, be placed in high-efficiency coating pot for subsequent use.
Its preparation method, comprises the following steps:
(1) Fructus Pyri thin paste process: get pear and decoct with water secondary, amount of water is 20% of pear quality for the first time, decocts 2 hours, obtains decocting liquid A; Second time amount of water is 50% of pear quality, decocts 1 hour, obtains decocting liquid B; Collecting decoction A and decocting liquid B, cryoconcentration becomes Fructus Pyri thin paste, and Fructus Pyri thin paste 80 DEG C of Baume degrees recorded are 33 ° of B é;
(2) sugar refinery: get Saccharum Sinensis Roxb., be incorporated as the water of saccharic amount 50%, heating is dissolved, and boils, and it is golden yellow for tempering to sugar liquid, with the Cheng Zhuwei degree that drips, obtains sugar refinery;
(3) dry: Fructus Pyri thin paste step (1) obtained becomes pears dry extract and sugared dry extract with step (2) sugar refinery oven drying;
(4) pulverize: the pears dry extract obtain step (3) and sugared dry extract high speed disintegrator are ground into fine powder, obtain pears fine powder and sugared fine powder;
(5) granulate: the pears fine powder obtain step (4) and sugared fine powder one-step-granulating method are directly made can the granule of tabletting, and obtain pears granule and sugared granule, wherein one-step-granulating method inlet temperature is 180 DEG C, and transfusion frequency values is 30HZ;
(6) always mix: the pears granule obtain step (5) and sugared granule three-dimensional mixer mix homogeneously, incorporation time is 90 minutes, obtains hybrid particles;
(7) tabletting: the hybrid particles tabletting that step (6) is obtained, punch die
scrobicula, checks every 15 minutes in tableting processes that average sheet is heavy and once checks hardness, outward appearance simultaneously, obtains qualified snow pear slice element sheet;
(8) coating: the qualified snow pear slice element sheet that pickup step (7) obtains, set high in effect coating pan, start seed-coating machine, exhaust blower and hot-air blower, first blowing hot-air pre-phlogiston sheet to 40 DEG C, then spraying system is started, film-coat liquid is sprayed onto coat tablets equably, and coating temperature is 50 DEG C, till spray full thin film dress material;
(9) pack, obtain the present embodiment product.
The present embodiment product hardness is label 5.01kg/cm
3.
Embodiment 2
A kind of Traditional Chinese medicine snow pear lozenge, comprises the following raw material according to weight parts: 25 portions of pears, 50 parts of Saccharum Sinensis Roxb., 2 parts of film-coat liquid.
Take with 20 of weight parts parts of HPMC, 10 parts of PEG400,20 parts of propylene glycol, 20 parts of magnesium stearate, then add 800 parts of purified water, stir, obtain film-coat liquid, be placed in high-efficiency coating pot for subsequent use.
Its preparation method, comprises the following steps:
(1) Fructus Pyri thin paste process: get pear and decoct with water secondary, amount of water is 30% of pear quality for the first time, decocts 3 hours, obtains decocting liquid A; Second time amount of water is 60% of pear quality, decocts 2 hours, obtains decocting liquid B; Collecting decoction A and decocting liquid B, cryoconcentration becomes Fructus Pyri thin paste, and Fructus Pyri thin paste 80 DEG C of Baume degrees recorded are 37 ° of B é;
(2) sugar refinery: get Saccharum Sinensis Roxb., be incorporated as the water of saccharic amount 60%, heating is dissolved, and boils, and tempering to sugar liquid in golden yellow (dripping into pearl) is degree, obtains sugar refinery;
(3) dry: Fructus Pyri thin paste step (1) obtained becomes pears dry extract and sugared dry extract with step (2) sugar refinery oven drying;
(4) pulverize: the pears dry extract obtain step (3) and sugared dry extract high speed disintegrator are ground into fine powder, obtain pears fine powder and sugared fine powder;
(5) granulate: the pears fine powder obtain step (4) and sugared fine powder one-step-granulating method are directly made can the granule of tabletting, and obtain pears granule and sugared granule, wherein one-step-granulating method inlet temperature is 210 DEG C, and transfusion frequency values is 45HZ;
(6) always mix: the pears granule obtain step (5) and sugared granule three-dimensional mixer mix homogeneously, incorporation time is 90 minutes, obtains hybrid particles;
(7) tabletting: the hybrid particles tabletting that step (6) is obtained, punch die
scrobicula, checks every 15 minutes in tableting processes that average sheet is heavy and once checks hardness, outward appearance simultaneously, obtains qualified snow pear slice element sheet;
(8) coating: the qualified snow pear slice element sheet that pickup step (7) obtains, set high in effect coating pan, start seed-coating machine, exhaust blower and hot-air blower, first blowing hot-air pre-phlogiston sheet to 40 DEG C, then spraying system is started, film-coat liquid is sprayed onto coat tablets equably, and coating temperature is 60 DEG C, till spray full thin film dress material;
(9) pack, obtain the present embodiment product.
The present embodiment product hardness is label 4.99kg/cm
3.
Embodiment 3
A kind of Traditional Chinese medicine snow pear lozenge, comprises the following raw material according to weight parts: 28 portions of pears, 56 parts of Saccharum Sinensis Roxb., 3 parts of film-coat liquid.
Take with 15 of weight parts parts of HPMC, 7.6 parts of PEG400,15 parts of propylene glycol, 8 parts of magnesium stearate, then add 700 parts of purified water, stir, obtain film-coat liquid, be placed in high-efficiency coating pot for subsequent use.
Its preparation method, comprises the following steps:
(1) Fructus Pyri thin paste process: get pear and decoct with water secondary, amount of water is 25% of pear quality for the first time, decocts 2.5 hours, obtains decocting liquid A; Second time amount of water is 55% of pear quality, decocts 1.5 hours, obtains decocting liquid B; Collecting decoction A and decocting liquid B, cryoconcentration becomes Fructus Pyri thin paste, and Fructus Pyri thin paste 80 DEG C of Baume degrees recorded are 35 ° of B é;
(2) sugar refinery: get Saccharum Sinensis Roxb. (the double amount of the quality of quality and the pears of sugar), be incorporated as the water of saccharic amount 55%, heating is dissolved, and boils, tempering to sugar liquid in golden yellow (dripping into pearl) as spending, obtaining sugar refinery;
(3) dry: Fructus Pyri thin paste step (1) obtained becomes pears dry extract and sugared dry extract with step (2) sugar refinery oven drying;
(4) pulverize: the pears dry extract obtain step (3) and sugared dry extract high speed disintegrator are ground into fine powder, obtain pears fine powder and sugared fine powder;
(5) granulate: the pears fine powder obtain step (4) and sugared fine powder one-step-granulating method are directly made can the granule of tabletting, and obtain pears granule and sugared granule, wherein one-step-granulating method inlet temperature is 195 DEG C, and transfusion frequency values is 38HZ;
(6) always mix: the pears granule obtain step (5) and sugared granule three-dimensional mixer mix homogeneously, incorporation time is 90 minutes, obtains hybrid particles;
(7) tabletting: the hybrid particles tabletting that step (6) is obtained, punch die
scrobicula, checks every 15 minutes in tableting processes that average sheet is heavy and once checks hardness, outward appearance simultaneously, obtains qualified snow pear slice element sheet;
(8) coating: the qualified snow pear slice element sheet that pickup step (7) obtains, set high in effect coating pan, start seed-coating machine, exhaust blower and hot-air blower, first blowing hot-air pre-phlogiston sheet to 40 DEG C, then spraying system is started, film-coat liquid is sprayed onto coat tablets equably, and coating temperature is 55 DEG C, till spray full thin film dress material;
(9) pack, obtain the present embodiment product.
The present embodiment product hardness is label 5.00kg/cm
3.
Meanwhile, carry out stability test to this example 1 ~ 3, its result is as shown in table 1 ~ 3.
Table 1 embodiment 1 product stability result of the test
Table 2 embodiment 2 product stability result of the test
Table 3 embodiment 3 product stability result of the test
Claims (2)
1. a Traditional Chinese medicine snow pear lozenge, it is characterized in that being made up of the following raw material according to weight parts: 25-30 part pear, 50-60 part Saccharum Sinensis Roxb., 2-4 part film-coat liquid, wherein said film-coat liquid comprises the following raw material according to weight parts: 10-20 part HPMC, 5-10 part PEG400,10-20 part propylene glycol, 2-20 part magnesium stearate, 500-800 part purified water, and the preparation method of wherein said Traditional Chinese medicine snow pear lozenge is as follows:
(1) Fructus Pyri thin paste process: get pear and decoct with water secondary, amount of water is the 20-30% of pear quality for the first time, decocts 2-3 hour, obtains decocting liquid A; Second time amount of water is the 50-60% of pear quality, decocts 1-2 hour, obtains decocting liquid B; Collecting decoction A and decocting liquid B, cryoconcentration becomes Fructus Pyri thin paste, and Fructus Pyri thin paste 80 DEG C of Baume degrees recorded are 33 ~ 37 ° of B é;
(2) sugar refinery: get Saccharum Sinensis Roxb., be incorporated as the water of saccharic amount 50-60%, heating is dissolved, and boils, and it is golden yellow for spending for tempering to sugar liquid, obtains sugar refinery;
(3) dry: Fructus Pyri thin paste step (1) obtained becomes pears dry extract and sugared dry extract with step (2) sugar refinery oven drying;
(4) pulverize: the pears dry extract obtain step (3) and sugared dry extract high speed disintegrator are ground into fine powder, obtain pears fine powder and sugared fine powder;
(5) granulate: the pears fine powder obtain step (4) and sugared fine powder one-step-granulating method are directly made can the granule of tabletting, obtains pears granule and sugared granule;
(6) always mix: the pears granule obtain step (5) and sugared granule three-dimensional mixer mix homogeneously, obtain hybrid particles;
(7) tabletting: hybrid particles tabletting step (6) obtained, obtains snow pear slice element sheet;
(8) coating: step (7) is obtained snow pear slice element sheet, be placed in high-efficiency coating pot, obtain snow pear slice element sheet with film-coat liquid to step (7) and carry out film coating, coating temperature is 50 ~ 60 DEG C;
(9) pack.
2. Traditional Chinese medicine snow pear lozenge according to claim 1, it is characterized in that in step (5), one-step-granulating method inlet temperature is 180 ~ 210 DEG C, transfusion frequency values is 30 ~ 45HZ.
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| CN103301219B true CN103301219B (en) | 2015-04-08 |
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| CN101073433A (en) * | 2007-06-22 | 2007-11-21 | 上海新康制药厂 | Blackthorn pear fruit-juice solid product and its production |
| CN101181390A (en) * | 2007-11-27 | 2008-05-21 | 山东大学 | Roxburgh rose juice buccal tablets |
| CN101461518A (en) * | 2007-12-20 | 2009-06-24 | 徐建华 | Original Rosa roxburghii effervescence granule and lozenge |
| CN101991065A (en) * | 2009-08-28 | 2011-03-30 | 刘峰 | Method for producing pear buccal tablets |
-
2013
- 2013-06-21 CN CN201310251744.6A patent/CN103301219B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101073433A (en) * | 2007-06-22 | 2007-11-21 | 上海新康制药厂 | Blackthorn pear fruit-juice solid product and its production |
| CN101181390A (en) * | 2007-11-27 | 2008-05-21 | 山东大学 | Roxburgh rose juice buccal tablets |
| CN101461518A (en) * | 2007-12-20 | 2009-06-24 | 徐建华 | Original Rosa roxburghii effervescence granule and lozenge |
| CN101991065A (en) * | 2009-08-28 | 2011-03-30 | 刘峰 | Method for producing pear buccal tablets |
Non-Patent Citations (1)
| Title |
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| 无糖软儿梨含片生产工艺研究;杨生辉等;《食品科技》;20081231(第01期);第43-45页 * |
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Address after: No. 707 Changjiang Road, Runzhou District, Zhenjiang City, Jiangsu Province, 212000 Patentee after: JIANGSU 707 NATURAL PHARMACEUTICAL Co.,Ltd. Country or region after: China Address before: No. 707 Changjiang Road, Runzhou District, Zhenjiang City, Jiangsu Province, 212000 Patentee before: JIANGSU 707 NATURAL PHARMACEUTICAL Co.,Ltd. Country or region before: China |