CN103295664B - 一种多元纳米材料的制备方法和含有该多元纳米材料的太阳能电池电子银浆料 - Google Patents
一种多元纳米材料的制备方法和含有该多元纳米材料的太阳能电池电子银浆料 Download PDFInfo
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- CN103295664B CN103295664B CN201310144709.4A CN201310144709A CN103295664B CN 103295664 B CN103295664 B CN 103295664B CN 201310144709 A CN201310144709 A CN 201310144709A CN 103295664 B CN103295664 B CN 103295664B
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- metal oxide
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- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims abstract description 41
- 229910052709 silver Inorganic materials 0.000 title claims abstract description 32
- 239000004332 silver Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000002086 nanomaterial Substances 0.000 title abstract description 27
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract description 30
- 239000002105 nanoparticle Substances 0.000 claims abstract description 24
- 239000003960 organic solvent Substances 0.000 claims abstract description 19
- 239000000463 material Substances 0.000 claims description 43
- 150000004706 metal oxides Chemical class 0.000 claims description 28
- 239000002002 slurry Substances 0.000 claims description 18
- 239000002245 particle Substances 0.000 claims description 16
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 9
- 239000004094 surface-active agent Substances 0.000 claims description 9
- 239000000654 additive Substances 0.000 claims description 8
- 230000000996 additive effect Effects 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 5
- 239000012459 cleaning agent Substances 0.000 claims description 4
- 239000013008 thixotropic agent Substances 0.000 claims description 4
- 238000000354 decomposition reaction Methods 0.000 claims description 3
- 239000004014 plasticizer Substances 0.000 claims description 3
- 239000002562 thickening agent Substances 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 abstract description 8
- 238000005245 sintering Methods 0.000 abstract description 8
- 229910052751 metal Inorganic materials 0.000 abstract description 3
- 239000002184 metal Substances 0.000 abstract description 3
- 239000000843 powder Substances 0.000 abstract 1
- 239000011521 glass Substances 0.000 description 11
- 239000000428 dust Substances 0.000 description 9
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 4
- 239000012043 crude product Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 229910052710 silicon Inorganic materials 0.000 description 4
- 239000010703 silicon Substances 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- DRGYXGZFRXFMHF-UHFFFAOYSA-N diazanium;tellurate Chemical compound [NH4+].[NH4+].[O-][Te]([O-])(=O)=O DRGYXGZFRXFMHF-UHFFFAOYSA-N 0.000 description 3
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 3
- 150000003378 silver Chemical class 0.000 description 3
- KILURZWTCGSYRE-LNTINUHCSA-K (z)-4-bis[[(z)-4-oxopent-2-en-2-yl]oxy]alumanyloxypent-3-en-2-one Chemical compound CC(=O)\C=C(\C)O[Al](O\C(C)=C/C(C)=O)O\C(C)=C/C(C)=O KILURZWTCGSYRE-LNTINUHCSA-K 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- XNRNVYYTHRPBDD-UHFFFAOYSA-N [Si][Ag] Chemical compound [Si][Ag] XNRNVYYTHRPBDD-UHFFFAOYSA-N 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- RZJRJXONCZWCBN-UHFFFAOYSA-N alpha-octadecene Natural products CCCCCCCCCCCCCCCCCC RZJRJXONCZWCBN-UHFFFAOYSA-N 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 229940046892 lead acetate Drugs 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 2
- 239000005052 trichlorosilane Substances 0.000 description 2
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- QGLWBTPVKHMVHM-KTKRTIGZSA-N (z)-octadec-9-en-1-amine Chemical compound CCCCCCCC\C=C/CCCCCCCCN QGLWBTPVKHMVHM-KTKRTIGZSA-N 0.000 description 1
- NKJOXAZJBOMXID-UHFFFAOYSA-N 1,1'-Oxybisoctane Chemical compound CCCCCCCCOCCCCCCCC NKJOXAZJBOMXID-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- XCJXQCUJXDUNDN-UHFFFAOYSA-N chlordene Chemical compound C12C=CCC2C2(Cl)C(Cl)=C(Cl)C1(Cl)C2(Cl)Cl XCJXQCUJXDUNDN-UHFFFAOYSA-N 0.000 description 1
- -1 content Substances 0.000 description 1
- WCOATMADISNSBV-UHFFFAOYSA-K diacetyloxyalumanyl acetate Chemical compound [Al+3].CC([O-])=O.CC([O-])=O.CC([O-])=O WCOATMADISNSBV-UHFFFAOYSA-K 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- FXADMRZICBQPQY-UHFFFAOYSA-N orthotelluric acid Chemical compound O[Te](O)(O)(O)(O)O FXADMRZICBQPQY-UHFFFAOYSA-N 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- DKFGYGJKRWRIPR-UHFFFAOYSA-N triethoxy(1-phenylethenyl)silane Chemical compound CCO[Si](OCC)(OCC)C(=C)C1=CC=CC=C1 DKFGYGJKRWRIPR-UHFFFAOYSA-N 0.000 description 1
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CN201310144709.4A CN103295664B (zh) | 2013-04-24 | 2013-04-24 | 一种多元纳米材料的制备方法和含有该多元纳米材料的太阳能电池电子银浆料 |
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CN103295664B true CN103295664B (zh) | 2015-06-24 |
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Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105694598A (zh) * | 2016-04-21 | 2016-06-22 | 华东理工大学 | 一种纳米银3d喷墨导电墨水及其制备方法 |
CN108321224A (zh) * | 2017-10-30 | 2018-07-24 | 无锡帝科电子材料科技有限公司 | 用于制备太阳能电池电极的多元纳米材料、包括其的糊剂组合物及太阳能电池电极和电池 |
CN112777935A (zh) * | 2019-11-11 | 2021-05-11 | 江西佳银科技有限公司 | 一种含纳米银玻璃粉及其制备方法 |
CN118486498A (zh) * | 2024-07-11 | 2024-08-13 | 深圳市深云基新材料科技有限公司 | 一种应用于陶瓷封装的灌孔导电银浆及其制备方法 |
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KR101193286B1 (ko) * | 2010-09-01 | 2012-10-19 | 삼성전기주식회사 | 전도성 페이스트, 그 제조방법 및 이를 이용한 전극 |
CN102708943B (zh) * | 2012-06-04 | 2014-04-16 | 惠州市富济电子材料有限公司 | 一种低温烧结型高导热高导电银浆、制备方法及烧结方法 |
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Address after: 214203 11 Jincheng Road, Yixing economic and Technological Development Zone, Wuxi, Jiangsu Patentee after: WUXI DIKE ELECTRONIC MAT Co.,Ltd. Address before: 214203 Wuxi Road, Yixing Economic Development Zone, Yongan Road, Pioneer Park two phase B2 building, Jiangsu Patentee before: DK ELECTRONIC MATERIALS Co.,Ltd. |
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Address after: No. 8 Yongsheng Road, Qiting Street, Yixing City, Wuxi City, Jiangsu Province, 214203 Patentee after: WUXI DIKE ELECTRONIC MAT Co.,Ltd. Country or region after: China Address before: 214203 11 Jincheng Road, Yixing economic and Technological Development Zone, Wuxi, Jiangsu Patentee before: WUXI DIKE ELECTRONIC MAT Co.,Ltd. Country or region before: China |