CN103251524B - Foam facial mask composition and preparation method thereof - Google Patents
Foam facial mask composition and preparation method thereof Download PDFInfo
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- CN103251524B CN103251524B CN201310169171.2A CN201310169171A CN103251524B CN 103251524 B CN103251524 B CN 103251524B CN 201310169171 A CN201310169171 A CN 201310169171A CN 103251524 B CN103251524 B CN 103251524B
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Abstract
The invention discloses a foam facial mask composition and a preparation method thereof. The foam facial mask comprises surfactant, emulsifier, alkyl perfluor butyl ether, conditioning and nursing components (conditioning effect agents), polydimethylsiloxane, essence, preservative, pH conditioning agent, pigment, viscosity modifier (thickening agent), natural active component extract and functional components. The raw materials in the formula of the foam facial mask composition are moderate and natural, so that the foam facial mask is moderate and low in irritation when being applied to a face; the irritation of fiber to the skin is avoided when the facial mask is used; and meanwhile people have the wonderful experience that a thick layer of foam grows out from nothing when using the facial mask. The foam facial mask composition has the advantages that the foam facial mask composition is moderate and can moisten and comfort the skin when used.
Description
Technical field
The present invention relates to a kind of foam facial mask composition, belong to daily chemical product technical field, particularly relate to a kind of foam facial mask composition and preparation method thereof.
Background technology
Foam mask is that cosmetics progressively improve in technology, the diverse requirements that consumer is different, the new cosmetics new technique that the process that cosmetics segment market produces, it in use provides a kind of special sensation to consumer, make this face gentleer in the process using bubble facial mask, zest is lower.Avoid veneer film in use fiber to the zest of skin, the marvellous process simultaneously making formula in use experience a thick layer of bubble to grow out of nothing.
Add volatile material soluble in water in the product, when it is released in air, will volatilize fast, liquid state becomes gaseous volume and naturally can expand, so just there is the bubble of constantly outwards emerging.Product common in the market, adopts this type of technique mostly.Or add ferment in the product, namely enzyme, this is more common in some Japanese product.Be sealed in the ferment ingress of air in sack, reaction produces bubble with it.This series products is without the need to fill and special nozzle, easy to carry, and some ferment also has the effect of exfoliation simultaneously, can increase the cleaning effect of facial film.
But existing foam mask still has and allows the unsatisfied place of consumer in use, requires further improvement necessity of its formula.
Summary of the invention
The object of the present invention is to provide a kind of new foam facial mask composition, make its production and application simple and convenient, and anti-corrosive properties and having good stability, gentleer to skin in use procedure, zest is less.
The object of the invention to solve the technical problems realizes by the following technical solutions.According to a kind of foam facial mask composition that the present invention proposes, comprise each raw material components of following weight percentage ratio:
Alkyl perfluorobutyl ether 0.1-20%;
Polydimethylsiloxane 0.1 ~ 20%;
Emulsifying agent 0.1-1.0%;
Surfactant 1-10%;
Conditioning effect agent 2 ~ 3%;
Thickening agent 0.01 ~ 0.5%;
PH regulator 0.01 ~ 0.5%;
Essence 0.1-2.0%;
Pigment appropriate (be adjusted to suitable can color);
Antiseptic 0.01-1%;
Water surplus adds to 100%;
Described alkyl perfluorobutyl ether is the mixture of any one or two kinds in ethyl perfluorobutyl ether, methyl perfluorobutyl ether agent.
A kind of foam facial mask composition, it can comprise each raw material components of following weight percentage ratio:
Methyl perfluorobutyl ether 0.1-20%;
Ethyl perfluorobutyl ether 0.1-20%;
Emulsifying agent 0.1-1.0%;
Surfactant 1-10%;
Conditioning effect agent 2 ~ 3%;
Thickening agent 0.01 ~ 0.5%;
PH regulator 0.01 ~ 0.5%;
Essence 0.1-2.0%;
Pigment appropriate (be adjusted to suitable can color);
Antiseptic 0.01-1%;
Water surplus adds to 100%.
A kind of foam facial mask composition, it can also comprise each raw material components of following weight percentage ratio:
Polydimethylsiloxane 10 ~ 30%;
Emulsifying agent 0.1-1.0%;
Surfactant 1-10%;
Conditioning effect agent 2 ~ 3%;
Thickening agent 0.01 ~ 0.5%;
PH regulator 0.01 ~ 0.5%;
Essence 0.1-2.0%;
Pigment appropriate (be adjusted to suitable can color);
Antiseptic 0.01-1%;
Water surplus adds to 100%;
Described polydimethylsiloxane is the mixture that volatility to be greater than in the volatile polydimethylsiloxaneand of more than 0.65 any one or more than two kinds.
Described surfactant is any one or two or more mixture in alkyl polyglucoside, lauryl both sexes sodium acetate, cocos nucifera oil both sexes sodium acetate, cocamidopropyl betaine, lauryl alcohol disodium sulfosuccinate (potassium), lauryl alcohol disodium sulfosuccinate (potassium), sodium lauroyl glutamate, lauroyl glutamate potassium, sodium lauroyl sarcosine, potassium lauroyl sarcosine, myristoyl-N-methylaminoacetic acid sodium, myristoyl-N-methylaminoacetic acid potassium, sodium cocoyl glycinate, cocos nucifera oil acyl glycine potassium.
Described emulsifying agent is PEG-100 stearate; Any one or two or more mixture in glyceryl stearate, 10-polyglyceryl laurate, 10-polyglyceryl myristate 10-polyglycereol Palmic acid, Surfhope SE Cosme C 1216, Sucrose myristate, sucrose palmitate, sucrose stearate.
The agent of described conditioning effect is any one or two or more mixture in the both effectiveness compositions such as vitamin E, polyglyceryl ether-26, D-panthenol, glycerol, aminoacid, polysaccharide, polypeptide, whitening agent, antidotal agent.
Described thickening agent is any one or two or more mixture in polyacrylic acid, card ripple alkane.
Described PH regulator is triethanolamine, hydrogen-oxygen flower sodium, hydrogen-oxygen flower potassium, lactic acid, any one or both in citric acid.
Described essence is any one in the flavor essence liked of consumer and essential oil fragrances;
Described pigment is a kind of or both above mixing of all pigments of cosmetics-stage and food grade;
A preparation method for foam facial mask composition, it comprises the following steps:
1) accurately taking ormal weight distilled water in formula adds in A beaker, after opening heating by electric cooker to 70 ~ 75 DEG C, turn on agitator, mixing speed controls at 500 ~ 600 revs/min, add conditioning effect agent that the surfactant of ormal weight in formula, emulsifying agent and needs dissolve, be incubated at 70 DEG C of-75 DEG C of 10min; Cool to room temperature for subsequent use;
2) take part water abundant swollen thickener in B beaker, add in appropriate soda acid (PH) regulator and become reconciled, for subsequent use;
3) A, B mixing is fully stirred, rotating speed 500 ~ 600, stir 5min, be uniformly dispersed completely; Add the both effectiveness composition of conditioning (the conditioning effect agent without the need to dissolving), antiseptic, pigment and essence fully mixes, and regulates viscosity, for subsequent use;
4) take formula and specify that alkyl perfluorobutyl ether or polydimethylsiloxane join in the beaker of mixing, stir 5min, mix homogeneously, be transferred to rapidly in airtight container preserve and canned.
By technique scheme, the advantage that the present invention has is:
Adopt the surfactant of gentle alkyl polyglucoside, aminoacid, imidazolines as primary foaming agent in composition of raw materials of the present invention, make face gentleer in the process using bubble facial mask, zest is lower.Avoid veneer film in use fiber to the zest of skin, the marvellous process simultaneously making formula in use experience a thick layer of bubble to grow out of nothing.
Detailed description of the invention
Below by way of concrete preferred embodiment and effect experimental examples, the present invention is expressed in further detail, but the present invention is not limited in following embodiment.
embodiment 1
The object of the invention to solve the technical problems realizes by the following technical solutions.According to a kind of foam facial mask composition that the present invention proposes, comprise each raw material components of following percentage by weight, as shown in table 1:
The component formula of table 1 foam facial mask composition and content thereof
Sequence number | Composition | Percentage composition |
1 | Ethyl perfluorobutyl ether | 0.1-20% |
2 | Polydimethylsiloxane | 0.00~10% |
3 | 10-polyglyceryl laurate | 0.1-1.0% |
4 | Alkyl polyglucoside | 1-10% |
5 | Polyglyceryl ether-26 | 2~3% |
6 | Polyacrylic acid | 0.01~0.5% |
7 | Triethanolamine | 0.01~0.5% |
8 | Essence | 0.1-2.0% |
9 | Pigment | In right amount (be adjusted to suitable can color) |
10 | Antiseptic | 0.01-1% |
11 | Water | Add to 100% |
1) accurately taking ormal weight distilled water in formula adds in beaker A, after opening heating by electric cooker to 70 ~ 75 DEG C, turn on agitator, mixing speed controls at 500 ~ 600 revs/min, add conditioning effect agent that the surfactant of ormal weight in formula, emulsifying agent and needs dissolve, be incubated at 70 DEG C of-75 DEG C of 10min; Cool to room temperature for subsequent use;
2) take part water abundant swollen thickener in B beaker, add in appropriate acid-base modifier and become reconciled, for subsequent use.
3) A, B mixing is fully stirred, rotating speed 500 ~ 600, stir 5min, be uniformly dispersed completely; Add the both effectiveness composition of conditioning (the conditioning effect agent without the need to dissolving), antiseptic, pigment and essence fully mixes, and regulates viscosity, for subsequent use;
4) take formula and specify that alkyl perfluorobutyl ether or polydimethylsiloxane join in the beaker of mixing, stir 5min, mix homogeneously, be transferred to rapidly in airtight container preserve and canned.
embodiment 2
The object of the invention to solve the technical problems realizes by the following technical solutions.According to a kind of foam facial mask composition that the present invention proposes, comprise each raw material components of following weight percentage ratio, as shown in table 2:
The component formula of table 2 foam facial mask composition and content thereof
Sequence number | Composition | Percentage composition |
1 | Methyl perfluorobutyl ether | 0.1-20% |
2 | Ethyl perfluorobutyl ether | 0.1-20% |
3 | 10-polyglyceryl laurate | 0.1-1.0% |
4 | Alkyl polyglucoside | 1-10% |
5 | Polyglyceryl ether-26 | 2~3% |
6 | Polyacrylic acid | 0.01~0.5% |
7 | Triethanolamine | 0.01~0.5% |
8 | Essence | 0.1-2.0% |
9 | Pigment | In right amount (be adjusted to suitable can color) |
10 | Antiseptic | 0.01-1% |
11 | Water | Add to 100% |
1) accurately taking ormal weight distilled water in formula adds in beaker A, after opening heating by electric cooker to 70 ~ 75 DEG C, turn on agitator, mixing speed controls at 500 ~ 600 revs/min, add conditioning effect agent that the surfactant of ormal weight in formula, emulsifying agent and needs dissolve, be incubated at 70 DEG C of-75 DEG C of 10min; Cool to room temperature for subsequent use;
2) take part water abundant swollen thickener in B beaker, add in appropriate acid-base modifier and become reconciled, for subsequent use.
3) A, B mixing is fully stirred, rotating speed 500 ~ 600, stir 5min, be uniformly dispersed completely; Add the both effectiveness composition of conditioning (the conditioning effect agent without the need to dissolving), antiseptic, pigment and essence fully mixes, and regulates viscosity, for subsequent use;
4) take formula and specify that alkyl perfluorobutyl ether or polydimethylsiloxane join in the beaker of mixing, stir 5min, mix homogeneously, be transferred to rapidly in airtight container preserve and canned.
embodiment 3
The object of the invention to solve the technical problems realizes by the following technical solutions.According to a kind of foam facial mask composition that the present invention proposes, comprise each raw material components of following weight percentage ratio, as shown in table 3:
The component formula of table 3 foam facial mask composition and content thereof
Sequence number | Composition | Percentage composition |
1 | Polydimethylsiloxane | 10~30% |
2 | 10-polyglyceryl laurate | 0.1-1.0% |
3 | Alkyl polyglucoside | 1-10% |
4 | Polyglyceryl ether-26 | 2~3% |
5 | Polyacrylic acid | 0.01~0.5% |
6 | Triethanolamine | 0.01~0.5% |
7 | Essence | 0.1-2.0% |
8 | Pigment | In right amount (be adjusted to suitable can color) |
9 | Antiseptic | 0.01-1% |
10 | Water | Add to 100% |
1) accurately taking ormal weight distilled water in formula adds in beaker A, after opening heating by electric cooker to 70 ~ 75 DEG C, turn on agitator, mixing speed controls at 500 ~ 600 revs/min, add conditioning effect agent that the surfactant of ormal weight in formula, emulsifying agent and needs dissolve, be incubated at 70 DEG C of-75 DEG C of 10min; Cool to room temperature for subsequent use;
2) take part water abundant swollen thickener in B beaker, add in appropriate acid-base modifier and become reconciled, for subsequent use.
3) A, B mixing is fully stirred, rotating speed 500 ~ 600, stir 5min, be uniformly dispersed completely; Add the both effectiveness composition of conditioning (the conditioning effect agent without the need to dissolving), antiseptic, pigment and essence fully mixes, and regulates viscosity, for subsequent use;
4) take formula and specify that alkyl perfluorobutyl ether or polydimethylsiloxane join in the beaker of mixing, stir 5min, mix homogeneously, be transferred to rapidly in airtight container preserve and canned.
embodiment 4
The object of the invention to solve the technical problems realizes by the following technical solutions.According to a kind of foam facial mask composition that the present invention proposes, comprise each raw material components of following weight percentage ratio, as shown in table 4:
The component formula of table 4 foam facial mask composition and content thereof
Sequence number | Composition | Percentage composition |
1 | Ethyl perfluorobutyl ether | 0.1-20% |
2 | Polydimethylsiloxane | 0.00~10% |
3 | Lauric acid polyglycerin ester-10 | 0.1-1.0% |
4 | Sodium lauroyl sarcosine | 1-10% |
5 | Polyglyceryl ether-26 | 2~3% |
6 | Polyacrylic acid | 0.01~0.5% |
7 | Triethanolamine | 0.01~0.5% |
8 | Essence | 0.1-2.0% |
9 | Pigment | In right amount (be adjusted to suitable can color) |
10 | Antiseptic | 0.01-1% |
11 | Water | Add to 100% |
1) accurately taking ormal weight distilled water in formula adds in beaker A, after opening heating by electric cooker to 70 ~ 75 DEG C, turn on agitator, mixing speed controls at 500 ~ 600 revs/min, add conditioning effect agent that the surfactant of ormal weight in formula, emulsifying agent and needs dissolve, be incubated at 70 DEG C of-75 DEG C of 10min; Cool to room temperature for subsequent use;
2) take part water abundant swollen thickener in B beaker, add in appropriate acid-base modifier and become reconciled, for subsequent use.
3) A, B mixing is fully stirred, rotating speed 500 ~ 600, stir 5min, be uniformly dispersed completely; Add the both effectiveness composition of conditioning (the conditioning effect agent without the need to dissolving), antiseptic, pigment and essence fully mixes, and regulates viscosity, for subsequent use;
4) take formula and specify that alkyl perfluorobutyl ether or polydimethylsiloxane join in the beaker of mixing, stir 5min, mix homogeneously, be transferred to rapidly in airtight container preserve and canned.
embodiment 5
The object of the invention to solve the technical problems realizes by the following technical solutions.According to a kind of foam facial mask composition that the present invention proposes, comprise each raw material components of following weight percentage ratio, as shown in table 5:
The component formula of table 5 foam facial mask composition and content thereof
Sequence number | Composition | Percentage composition |
1 | Ethyl perfluorobutyl ether | 0.1-20% |
2 | Polydimethylsiloxane | 0.00~10% |
3 | 10-polyglyceryl myristate | 0.1-1.0% |
4 | Sodium lauroyl sarcosine | 1-10% |
5 | Polyglyceryl ether-26 | 2~3% |
6 | Polyacrylic acid | 0.01~0.5% |
7 | Triethanolamine | 0.01~0.5% |
8 | Essence | 0.1-2.0% |
9 | Pigment | In right amount (be adjusted to suitable can color) |
10 | Antiseptic | 0.01-1% |
11 | Water | Add to 100% |
1) accurately taking ormal weight distilled water in formula adds in beaker A, after opening heating by electric cooker to 70 ~ 75 DEG C, turn on agitator, mixing speed controls at 500 ~ 600 revs/min, add conditioning effect agent that the surfactant of ormal weight in formula, emulsifying agent and needs dissolve, be incubated at 70 DEG C of-75 DEG C of 10min; Cool to room temperature for subsequent use;
2) take part water abundant swollen thickener in B beaker, add in appropriate acid-base modifier and become reconciled, for subsequent use.
3) A, B mixing is fully stirred, rotating speed 500 ~ 600, stir 5min, be uniformly dispersed completely; Add the both effectiveness composition of conditioning (the conditioning effect agent without the need to dissolving), antiseptic, pigment and essence fully mixes, and regulates viscosity, for subsequent use;
4) take formula and specify that alkyl perfluorobutyl ether or polydimethylsiloxane join in the beaker of mixing, stir 5min, mix homogeneously, be transferred to rapidly in airtight container preserve and canned.
effect experimental examples 1(stability test)
In order to detect a kind of stability of foam facial mask composition, under a kind of foam facial mask composition water being placed on respectively room temperature, low temperature-15 DEG C, high temperature 40 DEG C of environment, observe the cosmetic variation situation of sample; The sample being regularly opposite to room temperature carries out viscosity, pH value measures, and observes the change of two indices.
Result shows: be placed in the sample under varying environment, appearance color significant change does not occur, without floccule or precipitation, without lamination, has good stability.
effect experimental examples 2(anti-corrosive properties are tested)
A kind of foam facial mask composition is carried out to preservation challenge tests in 28 days of CTFA recommendation.
Result shows: in sample, the quantity of antibacterial and fungus is all lower than 10, and its antiseptic power is excellent.
The above, it is only preferred embodiment of the present invention, not any pro forma restriction is done to the present invention, therefore everyly do not depart from technical solution of the present invention content, the any simple modification done above embodiment according to technical spirit of the present invention, equivalent variations and modification, all still belong in the scope of technical solution of the present invention.
Claims (7)
1. a foam facial mask composition, is characterized in that, comprises each raw material components of following weight percentage ratio:
Alkyl perfluorobutyl ether 0.1-20%;
Polydimethylsiloxane 0.1 ~ 20%;
Emulsifying agent 0.1-1.0%;
Surfactant 1-10%, described surfactant is alkyl polyglucoside, lauryl both sexes sodium acetate, cocos nucifera oil both sexes sodium acetate, cocamidopropyl betaine, lauryl alcohol disodium sulfosuccinate, lauryl alcohol 2-Sulfosuccinic acid dipotassium, lauryl alcohol disodium sulfosuccinate, lauryl alcohol 2-Sulfosuccinic acid dipotassium, sodium lauroyl glutamate, lauroyl glutamate potassium, sodium lauroyl sarcosine, potassium lauroyl sarcosine, myristoyl-N-methylaminoacetic acid sodium, myristoyl-N-methylaminoacetic acid potassium, sodium cocoyl glycinate, any one or two or more mixture in cocos nucifera oil acyl glycine potassium,
Described alkyl perfluorobutyl ether is the mixture of any one or two kinds in ethyl perfluorobutyl ether, methyl perfluorobutyl ether agent.
2. a foam facial mask composition, is characterized in that, comprises each raw material components of following weight percentage ratio:
Methyl perfluorobutyl ether 0.1-20%;
Ethyl perfluorobutyl ether 0.1-20%;
Emulsifying agent 0.1-1.0%;
Surfactant 1-10%, described surfactant is alkyl polyglucoside, lauryl both sexes sodium acetate, cocos nucifera oil both sexes sodium acetate, cocamidopropyl betaine, lauryl alcohol disodium sulfosuccinate, lauryl alcohol 2-Sulfosuccinic acid dipotassium, lauryl alcohol disodium sulfosuccinate, lauryl alcohol 2-Sulfosuccinic acid dipotassium, sodium lauroyl glutamate, lauroyl glutamate potassium, sodium lauroyl sarcosine, potassium lauroyl sarcosine, myristoyl-N-methylaminoacetic acid sodium, myristoyl-N-methylaminoacetic acid potassium, sodium cocoyl glycinate, any one or two or more mixture in cocos nucifera oil acyl glycine potassium,
3. a foam facial mask composition, is characterized in that, comprises each raw material components of following weight percentage ratio:
Polydimethylsiloxane 10 ~ 30%;
Emulsifying agent 0.1-1.0%;
Surfactant 1-10%, described surfactant is alkyl polyglucoside, lauryl both sexes sodium acetate, cocos nucifera oil both sexes sodium acetate, cocamidopropyl betaine, lauryl alcohol disodium sulfosuccinate, lauryl alcohol 2-Sulfosuccinic acid dipotassium, lauryl alcohol disodium sulfosuccinate, lauryl alcohol 2-Sulfosuccinic acid dipotassium, sodium lauroyl glutamate, lauroyl glutamate potassium, sodium lauroyl sarcosine, potassium lauroyl sarcosine, myristoyl-N-methylaminoacetic acid sodium, myristoyl-N-methylaminoacetic acid potassium, sodium cocoyl glycinate, any one or two or more mixture in cocos nucifera oil acyl glycine potassium,
Described polydimethylsiloxane is the mixture that volatility to be greater than in the volatile polydimethylsiloxaneand of 0.65 any one or more than two kinds.
4. a kind of foam facial mask composition according to claim 1 or 2 or 3, is characterized in that: described emulsifying agent is PEG-100 stearate; Any one or two or more mixture in glyceryl stearate, 10-polyglyceryl laurate, 10-polyglyceryl myristate, 10-polyglycereol Palmic acid, Surfhope SE Cosme C 1216, Sucrose myristate, sucrose palmitate, sucrose stearate.
5. a kind of foam facial mask composition according to claim 1 or 2 or 3, is characterized in that: described conditioner is any one or two or more mixture in vitamin E, D-panthenol, polyglyceryl ether-26, glycerol, aminoacid, polysaccharide, polypeptide.
6. a kind of foam facial mask composition according to claim 1 or 2 or 3, is characterized in that: described PH regulator is any one or both in triethanolamine, sodium hydroxide, potassium hydroxide, lactic acid, citric acid.
7. a kind of foam facial mask composition according to claim 1 or 2 or 3, is characterized in that: described essence be the flavor essence liked of consumer and quintessence oil fragrant any one; Described pigment is a kind of or both above mixing of all pigments of cosmetics-stage and food grade.
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Cited By (1)
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DE102016224029A1 (en) * | 2016-12-02 | 2018-06-07 | Beiersdorf Ag | Foaming emulsion-based cleaning preparation-1 |
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KR101614803B1 (en) * | 2014-03-18 | 2016-04-22 | 주식회사 한국화장품제조 | Mask sheet cosmetic composition with self foaming function and manufacturing method thereof |
CN106880527A (en) * | 2016-02-13 | 2017-06-23 | 顾银凤 | A kind of cosmetics with anti-aging, whitening, moisture-keeping efficacy |
CN106038392B (en) * | 2016-06-27 | 2019-04-16 | 上海乐宝日化股份有限公司 | Bubble facial mask |
CN109464292B (en) * | 2018-10-11 | 2021-11-09 | 珀莱雅化妆品股份有限公司 | Mild self-foaming facial mask |
CN108904430A (en) * | 2018-10-15 | 2018-11-30 | 广州骐源生物科技有限公司 | A kind of foam mask |
CN109157422B (en) * | 2018-10-26 | 2021-07-06 | 广州市白云区大荣精细化工有限公司 | Foaming cleaning skin care product and preparation method thereof |
CN110538106A (en) * | 2019-09-12 | 2019-12-06 | 广州品赫生物科技有限公司 | bubble mask and preparation method thereof |
CN117323258B (en) * | 2023-12-01 | 2024-01-26 | 广州百孚润化工有限公司 | Bubble mask and preparation method thereof |
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US6702792B2 (en) * | 2002-07-18 | 2004-03-09 | Kenji Nakamura | Face mask having excellent usability |
CN101744743A (en) * | 2008-11-28 | 2010-06-23 | 高宝化妆品(中国)有限公司 | Self-foaming skin cleaning mask and preparation method thereof |
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DE102016224029A1 (en) * | 2016-12-02 | 2018-06-07 | Beiersdorf Ag | Foaming emulsion-based cleaning preparation-1 |
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