CN103215111B - Novel high-brightness environment-friendly stainless steel wire drawing lubricant - Google Patents
Novel high-brightness environment-friendly stainless steel wire drawing lubricant Download PDFInfo
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- CN103215111B CN103215111B CN201310111046.6A CN201310111046A CN103215111B CN 103215111 B CN103215111 B CN 103215111B CN 201310111046 A CN201310111046 A CN 201310111046A CN 103215111 B CN103215111 B CN 103215111B
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- stainless steel
- steel wire
- percent
- wire drawing
- novel high
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- 229910001220 stainless steel Inorganic materials 0.000 title claims abstract description 43
- 238000005491 wire drawing Methods 0.000 title claims abstract description 35
- 239000000314 lubricant Substances 0.000 title abstract description 19
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 13
- 239000010439 graphite Substances 0.000 claims abstract description 13
- -1 polyoxyethylene lauryl ether sulfate sodium Polymers 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 229930182470 glycoside Natural products 0.000 claims abstract description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 6
- 239000011734 sodium Substances 0.000 claims abstract description 6
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 6
- 150000001875 compounds Chemical class 0.000 claims description 25
- 230000007613 environmental effect Effects 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 claims description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 5
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 5
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 5
- 150000004996 alkyl benzenes Chemical class 0.000 claims description 5
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 5
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 5
- 235000011152 sodium sulphate Nutrition 0.000 claims description 5
- 150000001408 amides Chemical class 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 4
- 239000004711 α-olefin Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims 1
- 238000005868 electrolysis reaction Methods 0.000 abstract description 6
- 239000003963 antioxidant agent Substances 0.000 abstract description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 2
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 abstract 1
- 229940077388 benzenesulfonate Drugs 0.000 abstract 1
- 238000003912 environmental pollution Methods 0.000 abstract 1
- 150000002191 fatty alcohols Chemical class 0.000 abstract 1
- 238000005461 lubrication Methods 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 239000000779 smoke Substances 0.000 abstract 1
- 230000001988 toxicity Effects 0.000 abstract 1
- 231100000419 toxicity Toxicity 0.000 abstract 1
- 238000009423 ventilation Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000006260 foam Substances 0.000 description 4
- 230000003245 working effect Effects 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000001737 promoting effect Effects 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 238000005238 degreasing Methods 0.000 description 2
- 229910003460 diamond Inorganic materials 0.000 description 2
- 239000010432 diamond Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002736 nonionic surfactant Substances 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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- Metal Extraction Processes (AREA)
- Lubricants (AREA)
Abstract
The invention discloses a novel high-brightness environment-friendly stainless steel wire drawing lubricant. The novel high-brightness environment-friendly stainless steel wire drawing lubricant comprises the following components calculated based on 100 percent of total mass fraction: 60 to 85 percent of water graphite and 15 to 40 percent of composition, the composition comprises the following components according to the total mass fraction of 100 percent: 24 to 30 percent of sodium n-alkyl benzene sulfonate, 15 to 20 percent of lauryl sodium sulfate, 12 to 13 percent of AOS, 15 to 17 percent of fatty alcohol polyoxyethylene lauryl ether sulfate sodium, 6 to 8 percent of alkyl alcohol amine and 12 to 18 percent of alkyl glycoside. The high-brightness environment-friendly stainless steel wire drawing lubricant is high-temperature-resisting, friction-resisting, antioxidant, self-lubricating, good in ventilation and free from smoke and toxicity and can improve the appetency and lubrication performance for the metal surface, the surface brightness of a drawn product is high, the fineness is good, no electrolysis is needed, the environmental pollution can be reduced, the hardness and strength of a stainless steel wire can be stable and uniform, and the stainless steel wire can be used as a bus blank for a subsequent top-grade deep processing product.
Description
Technical field
The present invention relates to a kind of lubricant, specifically relate to a kind of novel high brightness environmental protection stainless steel wire drawing compound.
Background technology
At present, the lubricant of stainless steel wire drawing is all single wire drawing powder and liquid wire drawing oil, mainly contain graphite, calcium soap lubricant, in oildag, taking mineral substance as medium, in the time of drawing, oil content exhausts, lubricant has lost lubricant effect, forms the phenomenon of foam and conglomeration, and stability is poor, the wire surface pulling out is brightless, and can cause damage in various degree to wire-drawing die, reduce work-ing life of mould, because temperature when the drawing is very high, lubricity is inadequate, affects significantly the mechanical property of wire rod.
Summary of the invention
The object of this invention is to provide a kind of high temperature resistant, wear-resisting wiping, anti-oxidant, self-lubricating, good permeability, smokeless nontoxic novel high brightness environmental protection stainless steel wire drawing compound.
Novel high brightness environmental protection stainless steel wire drawing compound of the present invention, it is characterized in that, by total mass mark 100%, comprise aqueous graphite 60～85%, composition 15～40%, described composition, by total mass mark 100%, comprises linear alkylbenzene sulphonic acid 24～30%, sodium lauryl sulphate 15～20%, alpha-olefin sodium sulfonate 12～13%, polyoxyethylenated alcohol sodium sulfate 15～17%, alkylol amide 6～8% and alkyl glycoside 12～18%.
Aqueous graphite of the present invention, can buy and obtain from the market.
Adopt linear alkylbenzene sulphonic acid, sodium lauryl sulphate, alkene sulfonic acid sodium, polyoxyethylenated alcohol sodium sulfate and alkyl glycoside can make novel high brightness environmental protection stainless steel wire drawing compound of the present invention there is superior oilness and stability.
Alkyl glycoside is synthetic by renewable resources natural fat alcohol and glucose, it is the more comprehensive new non-ionic surfactants of a kind of performance, have the characteristic of common nonionic and anion surfactant concurrently, there is high surface, good ecological security and intermiscibility, it is internationally recognized first-selection " green " functional surface promoting agent, its wetting power is strong, strong detergency, compatibleness are strong, nontoxic, harmless, non-stimulated to skin, biological degradation is thorough rapidly, can with any type surfactant compound.Adopt alkyl glycoside as promoting agent, surfactivity, intermiscibility and the soil release performance of the novel high brightness environmental protection stainless steel wire drawing compound greatly having improved, its addition accounts for 2～8% of novel high brightness environmental protection stainless steel wire drawing compound part by weight, and the promoting agent of suitable proportion can impel novel high brightness environmental protection stainless steel wire drawing compound to have powerful clean effect.
Novel high brightness environmental protection stainless steel wire drawing compound of the present invention is prepared by the following method, and all raw materials, according to its mass percent mixing and stirring, are obtained to novel high brightness environmental protection stainless steel wire drawing compound of the present invention.
Foam and clustering phenomena that novel high brightness environmental protection stainless steel wire drawing compound of the present invention has avoided oildag to occur in drawing process, avidity and oilness to metallic surface are improved, extend the work-ing life to wire-drawing die, it is high that the product that drawing is produced can reach surface brightness, smooth finish is good, do not need to carry out electrolysis, reduce the pollution to environment, ensure the stable and uniform of STAINLESS STEEL WIRE hardness and intensity, can accurately be controlled in the scope of HRC ± 1, can produce higher-grade simultaneously, high-grade stainless steel light wire rod, improve value and the profit of product, and can be used as the bus base material of follow-up high-grade deep processed product.
Embodiment
Following examples are to further illustrate of the present invention, instead of limitation of the present invention.
Embodiment 1:
Aqueous graphite is purchased from Qingdao Run Ba graphite product company limited.
Get aqueous graphite 60g, linear alkylbenzene sulphonic acid 24g, sodium lauryl sulphate 15g, alpha-olefin sodium sulfonate 12g, polyoxyethylenated alcohol sodium sulfate 15g, alkylol amide 6g and alkyl glycoside 12g.
By above-mentioned each composition mixing and stirring, obtain novel high brightness environmental protection stainless steel wire drawing compound.
Diameter is the cloudy surface Stainless Steel Wire that φ 0.90～6.00mm tensile strength is 700MPa～1500MPa, the drawing draft of single pass is 7%-23%, when drawing, the temperature of mould inner surface reaches 400-600 degree, the novel high brightness environmental protection stainless steel wire drawing compound that adopts the present embodiment to prepare can significantly reduce the temperature of die surface, the temperature of die surface can be down to 60 DEG C, the workspace circumference that wire rod enters mould is subject to violent crimp, under the provide protection of lubricant, wire surface does not produce corrosion and oxidation, the temperature of lubricant does not raise, do not produce two kinds of liquid separation and throw out yet, the more lubricated light of the circumference in mold work district, the wire surface pulling out reaches the Xiao Guo≤Ra0.25 of bright, need not carry out electrolysis and also can reach the luminance brightness standard of product.
Novel high brightness environmental protection stainless steel wire drawing compound prepared by the present embodiment, in not changing aqueous graphite performance, oilness and the control oiliness of lubricant are increased, in the process of drawing wires, the avidity of lubricant is very good, all the time make novel high brightness environmental protection stainless steel wire drawing compound keep liquid state, its lubricant effect can not reduce, in drawing process, do not produce throw out and conglomeration, and also there will not be foam, thereby avidity and oilness to metallic surface are improved, extend the work-ing life to wire-drawing die, its degreasing result is good, chemical stability is strong.
The wortle that the novel high brightness environmental protection stainless steel wire drawing compound that the present embodiment is prepared and natural diamond manufacture is used in combination, can drawing go out the STAINLESS STEEL WIRE of high brightness best bright finish, STAINLESS STEEL WIRE surfaceness (luminance brightness, smooth finish) Da Dao≤Ra0.25, do not need to carry out electrolysis, thereby reduce the pollution to environment, ensure the stable and uniform of STAINLESS STEEL WIRE hardness and intensity, can accurately be controlled in the scope of HRC ± 1, stablize the mechanical property of wire rod, enhance productivity, yield rate is up to more than 98%, drawing speed can reach 8m/s, thereby can produce higher-grade, high-grade stainless steel light wire rod, improve value and the profit of product, and can be used as the bus base material of follow-up high-grade deep processed product.
Embodiment 2:
Aqueous graphite is purchased from Qingdao Run Ba graphite product company limited.
Get aqueous graphite 85g, linear alkylbenzene sulphonic acid 30g, sodium lauryl sulphate 20g, alpha-olefin sodium sulfonate 13g, polyoxyethylenated alcohol sodium sulfate 17g, alkylol amide 8g and alkyl glycoside 18g.
By above-mentioned each composition mixing and stirring, obtain novel high brightness environmental protection stainless steel wire drawing compound.
Diameter is the cloudy surface Stainless Steel Wire that φ 0.90～6.00mm tensile strength is 700MPa～1500MPa, the drawing draft of single pass is 7%-23%, when drawing, the temperature of mould inner surface reaches 400-600 degree, the novel high brightness environmental protection stainless steel wire drawing compound that adopts the present embodiment to prepare can significantly reduce the temperature of die surface, the temperature of die surface can be down to 40 DEG C, the workspace circumference that wire rod enters mould is subject to violent crimp, under the provide protection of lubricant, wire surface does not produce corrosion and oxidation, the temperature of lubricant does not raise, do not produce two kinds of liquid separation and throw out yet, the more lubricated light of the circumference in mold work district, the wire surface pulling out reaches the Xiao Guo≤Ra0.25 of bright, need not carry out electrolysis and also can reach the luminance brightness standard of product.
Novel high brightness environmental protection stainless steel wire drawing compound prepared by the present embodiment, in not changing aqueous graphite performance, oilness and the control oiliness of lubricant are increased, in the process of drawing wires, the avidity of lubricant is very good, all the time make novel high brightness environmental protection stainless steel wire drawing compound keep liquid state, its lubricant effect can not reduce, in drawing process, do not produce throw out and conglomeration, and also there will not be foam, thereby avidity and oilness to metallic surface are improved, extend the work-ing life to wire-drawing die, its degreasing result is good, chemical stability is strong.
The wortle that the novel high brightness environmental protection stainless steel wire drawing compound that the present embodiment is prepared and natural diamond manufacture is used in combination, can drawing go out the STAINLESS STEEL WIRE of high brightness best bright finish, STAINLESS STEEL WIRE surfaceness (luminance brightness, smooth finish) Da Dao≤Ra0.25, do not need to carry out electrolysis, thereby reduce the pollution to environment, ensure the stable and uniform of STAINLESS STEEL WIRE hardness and intensity, can accurately be controlled in the scope of HRC ± 1, stablize the mechanical property of wire rod, enhance productivity, yield rate is up to more than 98%, drawing speed can reach 8m/s, thereby can produce higher-grade, high-grade stainless steel light wire rod, improve value and the profit of product, and can be used as the bus base material of follow-up high-grade deep processed product.
Claims (2)
1. a high brightness environmental protection stainless steel wire drawing compound, it is characterized in that, by total mass mark 100%, comprise aqueous graphite 60～85%, composition 15～40%, described composition, by total mass mark 100%, comprises linear alkylbenzene sulphonic acid 24～30%, sodium lauryl sulphate 15～20%, alpha-olefin sodium sulfonate 12～13%, polyoxyethylenated alcohol sodium sulfate 15～17%, alkylol amide 6～8% and alkyl glycoside 12～18%.
2. a preparation method for high brightness environmental protection stainless steel wire drawing compound claimed in claim 1, is characterized in that, the each composition in claim 1, according to its mass percent mixing and stirring, is obtained to high brightness environmental protection stainless steel wire drawing compound.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310111046.6A CN103215111B (en) | 2013-04-01 | 2013-04-01 | Novel high-brightness environment-friendly stainless steel wire drawing lubricant |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310111046.6A CN103215111B (en) | 2013-04-01 | 2013-04-01 | Novel high-brightness environment-friendly stainless steel wire drawing lubricant |
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| Publication Number | Publication Date |
|---|---|
| CN103215111A CN103215111A (en) | 2013-07-24 |
| CN103215111B true CN103215111B (en) | 2014-06-18 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310111046.6A Active CN103215111B (en) | 2013-04-01 | 2013-04-01 | Novel high-brightness environment-friendly stainless steel wire drawing lubricant |
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| Country | Link |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2773817A1 (en) * | 1998-01-22 | 1999-07-23 | Cfpi Ind | A new lubricating composition for the pretreatment of steel components before cold forming |
| CN102559350A (en) * | 2011-12-28 | 2012-07-11 | 上海中孚特种油品有限公司 | High-speed copper tube drawing lubricant and preparing method thereof |
| CN102660372A (en) * | 2012-05-24 | 2012-09-12 | 刘彦辉 | Lubricant for drawing superfine stainless steel wire and preparation method |
-
2013
- 2013-04-01 CN CN201310111046.6A patent/CN103215111B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2773817A1 (en) * | 1998-01-22 | 1999-07-23 | Cfpi Ind | A new lubricating composition for the pretreatment of steel components before cold forming |
| CN102559350A (en) * | 2011-12-28 | 2012-07-11 | 上海中孚特种油品有限公司 | High-speed copper tube drawing lubricant and preparing method thereof |
| CN102660372A (en) * | 2012-05-24 | 2012-09-12 | 刘彦辉 | Lubricant for drawing superfine stainless steel wire and preparation method |
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| Publication number | Publication date |
|---|---|
| CN103215111A (en) | 2013-07-24 |
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Inventor after: Zhu Zengyu Inventor after: Luo Guowei Inventor after: Lv Wanghua Inventor after: Zhai Xiufeng Inventor after: Zhu Dandan Inventor before: Zhu Zengyu Inventor before: Lv Wanghua |
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Address after: 526200 Guangdong city of Zhaoqing Province Sihui City Nanjiang Industrial Park Yongsheng Road No. 11 Patentee after: GUANGDONG YATAI NEW MATERIAL TECHNOLOGY Co.,Ltd. Address before: 526200 Guangdong city of Zhaoqing Province Sihui City Nanjiang Industrial Park Yongsheng Road No. 11 Patentee before: GUANGDONG YATAI STAINLESS STEEL PRODUCTS Co.,Ltd. |
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Denomination of invention: A high brightness environmental protection stainless steel wire drawing lubricant Effective date of registration: 20220124 Granted publication date: 20140618 Pledgee: Zhaoqing SME Financing Guarantee Co.,Ltd. Pledgor: GUANGDONG YATAI NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2022980001052 |
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Granted publication date: 20140618 Pledgee: Zhaoqing SME Financing Guarantee Co.,Ltd. Pledgor: GUANGDONG YATAI NEW MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2022980001052 |
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Denomination of invention: A High Brightness and Environmentally Friendly Stainless Steel Wire Drawing Lubricant Granted publication date: 20140618 Pledgee: Zhaoqing SME Financing Guarantee Co.,Ltd. Pledgor: GUANGDONG YATAI NEW MATERIAL TECHNOLOGY Co.,Ltd.|Guangdong Yaxin Nonmetallic Material Technology Co.,Ltd.|GUANGDONG ASIA-PACIFIC LIGHTWEIGHT TECHNOLOGY RESEARCH Co.,Ltd. Registration number: Y2024980002168 |