CN103202467B - Jinxianlian instant powder and preparation method thereof - Google Patents
Jinxianlian instant powder and preparation method thereof Download PDFInfo
- Publication number
- CN103202467B CN103202467B CN201310094347.2A CN201310094347A CN103202467B CN 103202467 B CN103202467 B CN 103202467B CN 201310094347 A CN201310094347 A CN 201310094347A CN 103202467 B CN103202467 B CN 103202467B
- Authority
- CN
- China
- Prior art keywords
- filter residue
- ultrafiltration
- terminal bud
- roxburgh anoectochilus
- anoectochilus terminal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention provides Jinxianlian instant powder and a preparation method thereof and belongs to the technical field of medical or healthcare food. The preparation method includes: utilizing Jinxianlian as raw materials, subjecting the Jinxianlian to digesting, enzymolysis, filtering, ultrafiltering, reverse osmosis concentration, drying, packaging and code printing to obtain finished products. The Jinxianlian instant powder and the preparation method have the advantages that technique is advanced, effective components of Jinxianlian are reserved to the greatest extent, and the instant powder can be instantly dissolved in water and is convenient to carry and store.
Description
Technical field
The bright a kind of roxburgh anoectochilus terminal bud instant powder and preparation method thereof that relates to of we.
Background technology
Roxburgh anoectochilus terminal bud: sweet, flat; Return lung, liver, kidney, urinary bladder channel; Clearing heat and cooling blood, expelling wind and removing dampness, for ephritis, cystitis, diabetes, bronchus, rheumatic arthritis, acute infantile convulsion etc.After roxburgh anoectochilus terminal bud is extracted, concentrates, filters, sprayed, make pulvis, product has been preserved the effective ingredient of roxburgh anoectochilus terminal bud to greatest extent, the water-soluble applicable old man of energy speed, children taking.
Summary of the invention
The invention provides a kind of roxburgh anoectochilus terminal bud instant powder and preparation method thereof, belong to medicine or health food technology field.Its preparation method is for take roxburgh anoectochilus terminal bud as raw material, through lixiviate enzymolysis, filtration, ultrafiltration, reverse osmosis concentration, dry, packing, coding, finished product.Advanced technologies of the present invention, product has been preserved the effective ingredient of roxburgh anoectochilus terminal bud to greatest extent, and can fast water-soluble use, carry store convenient.
We are bright takes following scheme:
A roxburgh anoectochilus terminal bud instant powder, take roxburgh anoectochilus terminal bud as raw material, comprises following steps: lixiviate, enzymolysis, filtration, ultrafiltration, reverse osmosis concentration, dry being prepared from, wherein concrete:
1) lixiviate: roxburgh anoectochilus terminal bud is pulverized, crossed 50-100 mesh sieve, add the 60%-90%vol ethanol of 4-8 times of weight, at 40-50 ℃ of refluxing extraction 0.5-1.5 hour, cross 50-100 mesh sieve, obtain extract a and filter residue;
2) enzymolysis: the water of filter residue and 4-8 times of weight of filter residue weight being mixed, then add the pectase of the 1-1.5% of filter residue and water gross weight, is lixiviate 1-2 time that refluxes under 4.5-5.5 in pH value, temperature 55-60 ℃, at every turn 0.5-1.5 hour; Then at temperature 55-60 ℃, pH value is for adding the tannase of the 1-1.5% of filter residue and water gross weight under 4.5-5.0, and enzymolysis 0.5-1.0 hour, filters through 50-100 eye mesh screen, collects extract b;
3) filtration, ultrafiltration: extract a, b are mixed, after initial filter, obtain just filtrate; By milipore filter, carry out ultrafiltration again;
4) reverse osmosis concentration, dry: the product after step 3) ultrafiltration is carried out to reverse osmosis concentration, be condensed into the concentrate that relative density is 1.05-1.10, in concentrate, add the dextrin of the 3-5wt% that accounts for concentrate, dry after stirring.
The preparation method of described a kind of roxburgh anoectochilus terminal bud instant powder is:
1) lixiviate: roxburgh anoectochilus terminal bud is pulverized, crossed 50-100 mesh sieve, add the 60%-90%vol ethanol of 4-8 times of weight, at 40-50 ℃ of refluxing extraction 0.5-1.5 hour, obtain extract a and filter residue;
2) enzymolysis: the water of filter residue and 4-8 times of weight of filter residue weight being mixed, then add the pectase of the 1-1.5% of filter residue and water gross weight, is lixiviate 1-2 time that refluxes under 4.5-5.5 in pH value, temperature 55-60 ℃, at every turn 0.5-1.5 hour; Then at temperature 55-60 ℃, pH value is for adding the tannase of the 1-1.5% of filter residue and water gross weight under 4.5-5.0, and enzymolysis 0.5-1.0 hour, filters through 50-100 eye mesh screen, collects extract b;
3) filtration, ultrafiltration: extract a, b are mixed, after initial filter, obtain just filtrate; By milipore filter, carry out ultrafiltration again;
4) reverse osmosis concentration, dry: the product after step 3) ultrafiltration is carried out to reverse osmosis concentration, be condensed into the concentrate that relative density is 1.05-1.10, in concentrate, add the dextrin of the 3-5wt% that accounts for concentrate, dry after stirring.
It is 200 object screen clothes that initial filter described in step 3) adopts order number, and described milipore filter molecular weight is 10000-100000, and ultrafiltration condition used is under the pressure of 0.4-0.6Mpa, to carry out ultrafiltration.
Reverse osmosis concentration described in step 4) is used face Nai Ya≤30kgf/cm
2the rolling full film again of aromatic polyamide, temperature used is 20-50 ℃, concentrated pressure is 10-25kgf/cm
2.
Described dry process using spraying is dry, and spray-dired condition is inlet temperature 200-300 ℃, outlet temperature 80-95 ℃, and pressure is 7-20Mpa.
Advantage of the present invention: the present invention is according to roxburgh anoectochilus terminal bud modern pharmacology pharmacodynamics, with advanced technologies, develop with roxburgh anoectochilus terminal bud instant powder, this product not only has significant Antialcoholic liver-protecting function, obviously alleviate because of insobriety or the drunk headache causing, dizziness, drowsiness, weak, thirsty, vomiting, the symptom such as fidgety, and there is the health care prophylactic function of soothing liver and strengthening spleen, refreshment and tranquilization, clearing heat and detoxicating, nourishing qi and blood, carry in addition the feature easily of storing simultaneously.
The specific embodiment
In order to make content of the present invention more be convenient to understand, below in conjunction with the specific embodiment, technical solutions according to the invention are described further, but the present invention is not limited only to this.
Embodiment 1
1) roxburgh anoectochilus terminal bud of 100g is pulverized, crossed 100 eye mesh screens, add the 80%vol ethanol of 500ml, 45 ℃ of refluxing extraction 1.5 hours, through 100 eye mesh screens, filter, obtain extract a and filter residue;
2) enzymolysis: the water of filter residue and 5 times of amounts of filter residue bulking value being mixed, then add the pectase of filter residue and water gross weight 1%, is 4.5 times backflow lixiviates 2 times in pH value, 55 ℃ of temperature, each 1.5 hours; Then 55 ℃ of temperature, pH value is the tannase that adds filter residue and water gross weight 1.5% for 5.0 times, and enzymolysis 1.0 hours filters through 100 eye mesh screens, collects extract b;
3) filtration, ultrafiltration: extract a, b are mixed, through 200 eye mesh screens, filter, then under the pressure of 0.6Mpa, the milipore filter by 15000 molecular weight carries out ultrafiltration;
4) reverse osmosis concentration, dry: the product after step 3) ultrafiltration is used to the withstand voltage 30kgf/cm of face
2the rolling full film again of aromatic polyamide, 40 ℃ of temperature, concentrated pressure 20kgf/cm
2under carry out reverse osmosis concentration, be concentrated into relative density and be 1.05 concentrate, in concentrate, add the dextrin of the 3wt% of concentrate, after stirring, spray dry, 200 ℃ of inlet temperatures, 80 ℃ of outlet temperatures, pressure is under 7Mpa condition, to spray to be dried.
Claims (5)
1. a roxburgh anoectochilus terminal bud instant powder, take roxburgh anoectochilus terminal bud as raw material, comprises following steps: lixiviate, enzymolysis, filtration, ultrafiltration, reverse osmosis concentration, dry being prepared from, wherein concrete:
1) lixiviate: roxburgh anoectochilus terminal bud is pulverized, crossed 50-100 mesh sieve, add the 60%-90%vol ethanol of 4-8 times of weight, at 40-50 ℃ of refluxing extraction 0.5-1.5 hour, cross 50-100 mesh sieve, obtain extract a and filter residue;
2) enzymolysis: the water of filter residue and 4-8 times of weight of filter residue weight being mixed, then add the pectase of the 1-1.5% of filter residue and water gross weight, is lixiviate 1-2 time that refluxes under 4.5-5.5 in pH value, temperature 55-60 ℃, at every turn 0.5-1.5 hour; Then at temperature 55-60 ℃, pH value is for adding the tannase of the 1-1.5% of filter residue and water gross weight under 4.5-5.0, and enzymolysis 0.5-1.0 hour, filters through 50-100 eye mesh screen, collects extract b;
3) filtration, ultrafiltration: extract a, b are mixed, after initial filter, obtain just filtrate; By milipore filter, carry out ultrafiltration again;
4) reverse osmosis concentration, dry: the product after step 3) ultrafiltration is carried out to reverse osmosis concentration, be condensed into the concentrate that relative density is 1.05-1.10, in concentrate, add the dextrin of the 3-5wt% that accounts for concentrate, dry after stirring.
2. the preparation method of a kind of roxburgh anoectochilus terminal bud instant powder as claimed in claim 1 is:
1) lixiviate: roxburgh anoectochilus terminal bud is pulverized, crossed 50-100 mesh sieve, add the 60%-90%vol ethanol of 4-8 times of weight, at 40-50 ℃ of refluxing extraction 0.5-1.5 hour, obtain extract a and filter residue;
2) enzymolysis: the water of filter residue and 4-8 times of weight of filter residue weight being mixed, then add the pectase of the 1-1.5% of filter residue and water gross weight, is lixiviate 1-2 time that refluxes under 4.5-5.5 in pH value, temperature 55-60 ℃, at every turn 0.5-1.5 hour; Then at temperature 55-60 ℃, pH value is for adding the tannase of the 1-1.5% of filter residue and water gross weight under 4.5-5.0, and enzymolysis 0.5-1.0 hour, filters through 50-100 eye mesh screen, collects extract b;
3) filtration, ultrafiltration: extract a, b are mixed, after initial filter, obtain just filtrate; By milipore filter, carry out ultrafiltration again;
4) reverse osmosis concentration, dry: the product after step 3) ultrafiltration is carried out to reverse osmosis concentration, be condensed into the concentrate that relative density is 1.05-1.10, in concentrate, add the dextrin of the 3-5wt% that accounts for concentrate, dry after stirring.
3. a kind of roxburgh anoectochilus terminal bud instant powder as claimed in claim 1, it is characterized in that it is 200 object screen clothes that initial filter described in step 3) adopts order number, described milipore filter molecular weight is 10000-100000, and ultrafiltration condition used is under the pressure of 0.4-0.6Mpa, to carry out ultrafiltration.
4. a kind of roxburgh anoectochilus terminal bud instant powder as claimed in claim 1, is characterized in that the use of reverse osmosis concentration described in step 4) face Nai Ya≤30kgf/cm
2the rolling full film again of aromatic polyamide, temperature used is 20-50 ℃, concentrated pressure is 10-25kgf/cm
2.
5. a kind of roxburgh anoectochilus terminal bud instant powder as claimed in claim 1, is characterized in that described dry process using spraying is dry, and spray-dired condition is inlet temperature 200-300 ℃, outlet temperature 80-95 ℃, and pressure is 7-20Mpa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310094347.2A CN103202467B (en) | 2013-03-23 | 2013-03-23 | Jinxianlian instant powder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310094347.2A CN103202467B (en) | 2013-03-23 | 2013-03-23 | Jinxianlian instant powder and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103202467A CN103202467A (en) | 2013-07-17 |
| CN103202467B true CN103202467B (en) | 2014-11-05 |
Family
ID=48750050
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310094347.2A Active CN103202467B (en) | 2013-03-23 | 2013-03-23 | Jinxianlian instant powder and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103202467B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105942082A (en) * | 2016-04-29 | 2016-09-21 | 长泰县吉泰食品技术研发中心 | Anoectochilus roxburghii beverage and production process thereof |
| CN105918557A (en) * | 2016-05-14 | 2016-09-07 | 福建金草生物集团股份有限公司 | Plant substitute tea capable of tonifying spleen and soothing nerves and preparation method thereof |
| CN107897928A (en) * | 2017-12-25 | 2018-04-13 | 云南保山嘉宏农业开发（集团）有限公司 | Roxburgh anoectochilus terminal bud oral liquid and manufacture craft |
| CN109588595A (en) * | 2018-12-24 | 2019-04-09 | 福建省农业科学院农业生态研究所 | A kind of heat-clearing beverage and preparation method thereof rich in Coixol |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01171294A (en) * | 1987-12-25 | 1989-07-06 | Nec Kansai Ltd | Soldering method |
| JPH1171294A (en) * | 1997-08-29 | 1999-03-16 | Pias Arise Kk | Collagenase inhibitor |
| CN102150913B (en) * | 2011-02-06 | 2012-08-15 | 杨军 | Health care anoectochilus roxburghii drink and preparation method |
| CN102150855B (en) * | 2011-02-10 | 2012-05-23 | 杨军 | Preparation method for fresh anoectochilus roxburghii juice, and oral liquid, capsules and dissolved granules |
| CN102763749B (en) * | 2012-08-08 | 2013-07-24 | 罗劭蕾 | Instant osmanthus and fissidens tea |
-
2013
- 2013-03-23 CN CN201310094347.2A patent/CN103202467B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN103202467A (en) | 2013-07-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103202467B (en) | Jinxianlian instant powder and preparation method thereof | |
| CN104996645A (en) | Processing method of schisandra chinensis tea essence | |
| CN103829344B (en) | A kind of Cordyceps militaris composite beverage | |
| CN104292200B (en) | The process for extracting tea polyphenol of a kind of low caffeine, high-catechin | |
| CN103965152A (en) | Extraction and preparation method for licorice effective ingredients | |
| CN104543150A (en) | Preparation method of low-fluorine instant tea powder | |
| CN104106685B (en) | A kind of flower class health tea and its preparation method | |
| CN104206576A (en) | Preparation method of tea polyphenol-rich instant tea powder | |
| CN101129433A (en) | Method for extracting active component of edible burdock | |
| CN103798439A (en) | Chuzhou chrysanthemum instant tea powder | |
| CN102344882B (en) | Ginkgo and giant knotweed health wine and preparation method thereof | |
| CN105145987B (en) | Three leaf raspberry bealth-care instant teas and preparation method thereof | |
| CN103951713A (en) | Comprehensive utilization method for improving value of cucumis sativus seed medicinal materials | |
| CN103549610B (en) | A kind of blood-tonifying health-care beverage and preparation method | |
| CN103099213A (en) | Preparation technology for extracting water-insoluble dietary fiber by use of tea leaves | |
| CN102552839B (en) | Liquid medicine for preventing and treating alopecia | |
| CN101632403B (en) | Method for preparing honey green tea tablet | |
| CN101433322B (en) | Functional food rich in anthocyanidin and preparation method thereof | |
| CN105566507A (en) | Preparation method of tea polysaccharides | |
| CN101069719A (en) | Selenium-rich tea pigment extracting technology | |
| CN101264159A (en) | Method for processing deer fetus donkey-hide gelatin granule | |
| CN102835490A (en) | Common fenugreek seed health tea with functions of kidney warming and yang strengthening | |
| CN104365912A (en) | Method for preparing and extracting theabrownin | |
| CN105726837A (en) | Method for extracting effective components of pinelliae rhizoma praeparatumcum zingibere et alumina through ultrasonic-assisted solvent method | |
| CN103230013A (en) | Preparation method of alkekengi powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |