CN103194340A - Bacteria resisting amur corktree bark compound soap - Google Patents
Bacteria resisting amur corktree bark compound soap Download PDFInfo
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- CN103194340A CN103194340A CN2013101481343A CN201310148134A CN103194340A CN 103194340 A CN103194340 A CN 103194340A CN 2013101481343 A CN2013101481343 A CN 2013101481343A CN 201310148134 A CN201310148134 A CN 201310148134A CN 103194340 A CN103194340 A CN 103194340A
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- corktree bark
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Abstract
The invention discloses a bacteria resisting amur corktree bark compound soap. The soap comprises the following raw materials in parts by weight: 0.05-0.15 part of amur corktree bark extract, 15-25 parts of sodium cocoate, 50-70 parts of sodium palmitate, 3-5 parts of cocamidopropylamine oxide, 3-5 parts of sodium N-lauroyl sarcosinate and 20 parts of water. The bacteria resisting amur corktree bark compound soap is exquisite and stable in foam, has mild properties and low skin irritation and can further resist and inhibit bacteria effectively especially after the amur corktree bark extract is added.
Description
Technical field:
The present invention relates to a kind of perfumed soap, particularly the antibiotic composite soap of a kind of golden cypress.
Background technology:
Perfumed soap (soap) is one of skin, hair washing and nursing article, is a kind of daily necessities.Perfumed soap is to be main raw material with sodium soap and other tensio-active agents, adds quality improver and outward appearance modifying agent, through the product of making after the machine-shaping.
Perfumed soap is requisite washing and nursing article in the daily life, is main raw material with sodium soap and other tensio-active agents, adds quality improver and outward appearance modifying agent, through the product of making after the machine-shaping.The function of perfumed soap is the cleaning washing, be used in that yes above the skin and remove earth dirt, skin secretion, movement, chemical substance or bacterium etc., in today of stressing cosmetic result, makeup, skin care products or the medicine of removing skin surface also are one of its main purposes.
In the prior art, the many insights of perfumed soap are that fatty acid sodium salt is the Cake-shape soap of soap base, though have cleaning force, whipability and easy washability preferably, but not anti-hard water, can produce incrustation scale during washing, form the calcium magnesium soap, degreasing power is strong, the soap of human body life-time service meta-alkalescence can make skin feel dry and astringent, and excitement is arranged.
Golden cypress, English name: Amur Corktree Bark, another name: cork tree (Collective Notes to the Canon of Materia medica), first cypress, bark of a cork tree wood (" herbal classic "), bark of a cork tree skin (treatise on Febrile Diseases).Section belongs to: Rutaceae, Phellodendron.Proterties: Cortex Phellodendri is en plaque or shallow slot shape, and length and width differ, thick 3～6mm.Outside surface tawny or yellowish brown, smooth or tool longitudinal furrow line, the visible hole skin trace that has and remaining beige tertia.Internal surface dark yellow or light brown, the vertical rib that tool is fine and closely woven.Body is light, and matter is hard, and section fibrous is the splintery layering, deep yellow.Gas is little, and flavor is very bitter, the toughness of chewing.
Thick 2～the 4mm of CORTEX PHELLODENDRI AMURENE.Outside surface yellow-green colour or light brown yellow, more smooth, irregular longitudinal crack is arranged, the hole skin trace is little and rare, and idol has linen tertia residual.Bone surface yellow or yellowish brown.Body is light, and matter is harder, section aureus or yellow-green colour.
Meridian distribution of property and flavor: hardship, cold.Return kidney, bladder, large intestine channel.
The pharmacological action of golden cypress is as follows:
1. anti-microbial effect:
The golden cypress antibiotic effective ingredient is Berberine, thus its pharmacological action and coptis broadly similar, but content is low than the coptis.In vitro tests to streptococcus aureus, streptococcus pneumoniae, diphtheria corynebacterium, Streptococcus viridans, dysentery bacterium (except Song Nei Shi), Hemolytic streptococcus, meningococcus, vibrio cholerae, anthrax bacillus all effectively or stronger restraining effect arranged; Bacillus subtilus, bordetella pertussis, tetanus bacillus also there is restraining effect; H37Rv, mycobacterium tuberculosis are not had direct repression, but the bacterium number is reduced, present bacteriostatic action but concentration reaches at 1% o'clock.When inoculating mycobacterium hominis (H37Rv) do experiment treatment with cavy, curative effect oral or injection is all very poor.To the cavy of inoculation Mycobacterium bovis, during the hydrochloric acid crystallisate intramuscular injection of Cortex Phellodendri extract, certain curative effect is arranged.Golden cypress is taken a favorable turn to clinical symptom and the X ray examination of tuberculosis patient, and is better than the coptis.In test tube, golden cypress decoction or preserved material have in various degree bacteriostatic action to common pathogenic fungus.Its water decoction can not kill Leptospira (dosage needs than the big I of the coptis doubly).External trichomonas vaginitis also there is weak effect.It is reported that golden cypress acid-base method extract is made 1:1 golden cypress liquid, can treat bacillary dysentery with enema, can fully recover in general 2-4 days.The golden cypress treatment solution imports the treatment chronic prostatitis with direct current, and total effective rate reaches 97.3%.
2. antifungic action:
The ether extractive substance of CORTEX PHELLODENDRI AMURENE and Cortex Phellodendri has stronger bacteriostatic action to Cryptococcus neoformans and trichophyton purpureatum, and its effect is stronger than nystatin, but a little less than the oidiomycetic restraining effect of white enjoyed than mildew making.
3. antitussive effect:
The volatilization of golden cypress fruit has antitussive effect, and its antibechic composition is mainly myrcene.And from volatile oil, get Berberine and 5,5'-dimethyl furfural ether.
4. hypotensive effect:
Golden cypress can produce remarkable and lasting hypotensive effect to anesthetized animal intravenous injection or abdominal injection, and the carotid artery injection is more intravenous stronger, so step-down may be central.To the Phellodendrine change of quaternary ammonium type and compound name former times sieve woods (Xylopinin) of synthetic tertiary amine-type also can cause rapid, remarkable step-down; Between I-II cervical vertebra, cut off spinal cord then step-down disappear, thereby prove that also step-down belongs to central.In addition, former times sieve woods stronger antiadrenergic drug sample effect is arranged, to compressing carotid artery, suffocate, sympathetic ganglion causes on booster reaction that the electricity irritation greater splanchnic nerve causes and injection suprarenin or the electricity irritation neck instant embrane contractile response all is suppressed.
5. anti-trichomonal effect:
The golden cypress decoction, 10% concentration and trichomonad liquid 1:1 are mixed to be cultivated, and Trichomonas vaginalis is had restraining effect.
6. antihepatitic activity:
Golden cypress decoction 6.25-100% in vitro tests has restraining effect to Australia antigen(AA).Phellodendrine has certain effect to chronic hepatitis.
7. to Immune Effects:
The golden cypress decoction, 100% concentration, 0.3ml/ only irritates stomach, continuous 7 days, can increase mice spleen plaque-forming bacteria number.
8. antiulcer action:
Cortex Phellodendri extract (removing Berberine) 100mg/kg subcutaneous injection, 100,1000mg/kg irritates stomach or intradermal injection, the rat gastric ulcer that ethanol, Asprin or pylorus ligation are brought out has restraining effect.
9. other effect:
Phellodendrine and former times sieve woods central nervous system is had restraining effect, the spontaneous activity of mouse, various reflection all are suppressed; Give not anaesthetize rabbit former times sieve woods, the amplitude slow wave can appear in brain wave.Phellodendrine has slight curariform action mask, and frog rectus abdominis muscle tensity is not had influence, but can suppress the contractile response that caused by vagusstoff.To the isolated rabbit intestines, the golden cypress powder can strengthen its amplitude, and obakunone can strengthen its tension force and amplitude; Obakulactone then suppresses intestinal tube.On one's body the rabbit that has the pancreas fistula, golden cypress has the effect that promotes pancreatic secretion.Obakulactone can reduce rabbit blood glucose near lethal quantity (0.05-0.1g/kg) time, obakunone does not have this effect.It is said that obakunone has the hematoblastic effect of protection.Golden cypress has killing action to wriggler (10ppm can kill 62% in 18 hours), housefly.In addition, also have diuresis, stomach invigorating, external application to promote effects such as subcutaneous hemorrhage absorption.
At present, golden cypress is not applied among the perfumed soap in the prior art.
Summary of the invention:
At the prior art above shortcomings, technical problem to be solved by this invention provides the antibiotic composite soap of a kind of golden cypress.
Technical problem of the present invention is achieved by following technical proposals:
The antibiotic composite soap of a kind of golden cypress comprises the raw material of following weight part: Cortex Phellodendri extract 0.05-0.15 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, cocamidopropyl propyl amide amine oxide 3-5 part, N-sodium lauroyl sareosine 3-5 part, 20 parts in water.
Preferably, the antibiotic composite soap of a kind of golden cypress comprises the raw material of following weight part: Cortex Phellodendri extract 0.05-0.15 part, sequestrant 0.5-1.5 part, cocamidopropyl propyl amide amine oxide 3-5 part, N-sodium lauroyl sareosine 3-5 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, 20 parts in water.
Described sequestrant is made of by weight following component: methylglycine oxalic acid trisodium salt 40-60 part and hydroxyethyl diamine tetraacethyl trisodium salt 40-60 part.
Below, part material involved in the present invention is made simple declaration:
Cortex Phellodendri extract of the present invention can pass through commercially available getting, as the Cortex Phellodendri extract of Shenzhen BoDun spice Co., Ltd's production.This Cortex Phellodendri extract also can adopt following method preparation and get: after golden cypress is pulverized, the deionized water that adds the 6-10 times of weight, soaked 1-3 hour, ultrasonic extraction 10-15 minute, filter, centrifugal, discard precipitation with supernatant concentration, make Cortex Phellodendri extract, control Cortex Phellodendri extract density is at 1.05g/cm
3About.
The cocamidopropyl propyl amide amine oxide, CAS accession number: 68155-09-9.
The N-sodium lauroyl sareosine, CAS accession number: 137-16-6.
Described methylglycine oxalic acid trisodium salt, CAS accession number: 170492-24-7, its English name: L-Alanine, N, N-bis (carboxymethyl)-, sodium salt (1:3).It has better biological degradability than sequestrant EDTA, NTA commonly used, and is more stable under wideer PH scope and high temperature, has higher calcium sequestration capacity, and inorganic sediment is had higher solubility property, and heavy metal is had sequestering power preferably.Select for use BASF AG to produce in the present invention
Described hydroxyethyl diamine tetraacethyl trisodium salt, CAS accession number: 207386-87-6, its English name: Glycine, N-[2-[bis (carboxymethyl) amino] ethyl]-N-(2-hydroxyethyl)-, trisodium salt, hydrate (9CI).
In addition, in the present invention, can also add other functional ingredient commonly used in the common perfumed soap, for example: antiseptic-germicide, pigment, essence, oxidation inhibitor, titanium dioxide etc., to realize corresponding function respectively.As add the antiseptic-germicide of 0.2-0.8 weight part, the antioxidant of 0.05-0.20 weight part, the sanitas of 0.02-0.2 weight part, the white dyes of the titanium dioxide of 0.02-2 weight part, 0.001-0.05 weight part or the essence of 0.2-1.2 weight part on prescription of the present invention basis.
The antibiotic composite soap of golden cypress of the present invention can adopt the general soapmaking step of the common perfumed soap of the industry to be prepared, as:
(a) spice of kneading: the various raw materials of said components are taken by weighing in proportion join in the kneading machine that conventional soapmaking uses, kneading mixes.
(b) grind: the material after mixing will kneaded, enter in the shredder, carry out soap body and grind.
(c) vacuum press strip: the soap body after will grinding, enter vacuum plodder, carry out the vacuum press strip.
(d) print: the rectangular soap body that plodder extrudes directly enters printer and prints, and obtains the soap body of moulding.
The antibiotic composite soap of golden cypress of the present invention, foam is fine and smooth stable, the performance gentleness is low to the pungency of skin, add Cortex Phellodendri extract especially after, more effective antibacterial bacteriostatic.
Embodiment:
Following embodiment further specifies of the present invention, rather than limits the scope of the invention.In the present invention, if no special instructions, each raw material is 100% in working substance content all.
Embodiment 1
Embodiment 1 data by table 1 correspondence take by weighing each raw material.
(a) spice of kneading: various raw materials are joined soap with in the kneading machine, and kneading mixes.
(b) grind: the material after mixing will kneaded, enter in the shredder, carry out soap body and grind.
(c) vacuum press strip: the soap body after will grinding, enter vacuum plodder, carry out the vacuum press strip.
(d) print: the rectangular soap body that plodder extrudes directly enters printer and prints, and obtains the soap body of moulding.
Embodiment 2
Embodiment 2 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Embodiment 3
Embodiment 3 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Embodiment 4
Embodiment 4 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Comparative Examples 1
Comparative Examples 1 data by table 1 correspondence take by weighing each raw material.Method by embodiment 1 prepares perfumed soap.
Table 1: perfumed soap formula table unit: kilogram
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Comparative Examples 1 |
| Cortex Phellodendri extract | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 |
| Coconut oil sodium | 20 | 20 | 20 | 20 | 20 |
| Sodium pentadecanecarboxylate | 60 | 60 | 60 | 60 | 60 |
| The cocamidopropyl propyl amide amine oxide | 4 | 4 | 4 | 4 | / |
| The N-sodium lauroyl sareosine | 4 | 4 | 4 | 4 | / |
| α-lauryl alkyl betaine | / | / | / | / | 8 |
| Methylglycine oxalic acid trisodium salt | / | 1 | / | 0.5 | / |
| Hydroxyethyl diamine tetraacethyl trisodium salt | / | / | 1 | 0.5 | / |
| Water | 20 | 20 | 20 | 20 | 20 |
Test case 1:
Experiment is 5wt% with soap lye concentration, and when consumption was 0.3ml, by HET VAM measurements determination skin reaction classification (values classification relatively), intense stimulus＞2.0 stimulated 1.2-2.0, medium stimulation 0.8-1.2, minimal irritation 0.0-0.8.
Use the Luo Shi Latherometer to carry out the foaming properties test, soap lye concentration is 2.5wt%, tests the foam height of 0 minute and 5 minutes respectively.
Table 2: test data table
The test data of experiment of associative list 2, the present invention selects cocamidopropyl propyl amide amine oxide and N-sodium lauroyl sareosine built-up soap fundamental mode anion surfactant coconut oil sodium and Sodium pentadecanecarboxylate for use initiatively, can effectively reduce the pungency of perfumed soap; Select the composite interpolation of sequestrant methylglycine oxalic acid trisodium salt and hydroxyethyl diamine tetraacethyl trisodium salt initiatively for use, further can promote foaming power and the foam stability of perfumed soap.Above-mentioned difference technical characterictic did not have open in the prior art, was not common practise yet.
Claims (3)
1. the antibiotic composite soap of golden cypress is characterized in that, comprises the raw material of following weight part: Cortex Phellodendri extract 0.05-0.15 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, cocamidopropyl propyl amide amine oxide 3-5 part, N-sodium lauroyl sareosine 3-5 part, 20 parts in water.
2. golden cypress perfumed soap as claimed in claim 1, it is characterized in that, the raw material that comprises following weight part: Cortex Phellodendri extract 0.05-0.15 part, sequestrant 0.5-1.5 part, cocamidopropyl propyl amide amine oxide 3-5 part, N-sodium lauroyl sareosine 3-5 part, coconut oil sodium 15-25 part, Sodium pentadecanecarboxylate 50-70 part, 20 parts in water.
3. the antibiotic composite soap of golden cypress as claimed in claim 2 is characterized in that: described sequestrant, formed by weight by following component: methylglycine oxalic acid trisodium salt 40-60 part and hydroxyethyl diamine tetraacethyl trisodium salt 40-60 part.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310148134.3A CN103194340B (en) | 2013-04-25 | 2013-04-25 | Bacteria resisting amur corktree bark compound soap |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310148134.3A CN103194340B (en) | 2013-04-25 | 2013-04-25 | Bacteria resisting amur corktree bark compound soap |
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| CN103194340A true CN103194340A (en) | 2013-07-10 |
| CN103194340B CN103194340B (en) | 2014-12-24 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103695210A (en) * | 2013-12-20 | 2014-04-02 | 苏黎 | Traditional Chinese medicine scented soap |
| CN104911047A (en) * | 2015-05-18 | 2015-09-16 | 彭婷婷 | Honeysuckle flower traditional Chinese medicine antibacterial soap |
| CN104946434A (en) * | 2015-07-21 | 2015-09-30 | 安徽建筑大学 | Pure natural skin care perfumed soap and preparation method thereof |
| CN105400619A (en) * | 2015-12-11 | 2016-03-16 | 梁文成 | Aloe powder mixed soap |
| CN105441232A (en) * | 2015-12-11 | 2016-03-30 | 梁文成 | Capsaicin composite soap |
| CN107893001A (en) * | 2017-11-29 | 2018-04-10 | 深圳市地藏心文化传播有限公司 | A kind of natural handmade soap of the extract solution containing vine tea |
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| CN1109502A (en) * | 1994-03-28 | 1995-10-04 | 吉林市日用化学工业公司 | Toilet soap special for women |
| CN1182788A (en) * | 1997-02-03 | 1998-05-27 | 熊光明 | Health care detergent for preventing and controlling venereal disease and infections disease |
| CN102363740A (en) * | 2010-12-10 | 2012-02-29 | 江南大学 | Low-irritation and high-foaminess fancy soap formula |
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2013
- 2013-04-25 CN CN201310148134.3A patent/CN103194340B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02155993A (en) * | 1988-12-08 | 1990-06-15 | Nippon Oil & Fats Co Ltd | Lowly irritant solid detergent |
| CN1109502A (en) * | 1994-03-28 | 1995-10-04 | 吉林市日用化学工业公司 | Toilet soap special for women |
| CN1182788A (en) * | 1997-02-03 | 1998-05-27 | 熊光明 | Health care detergent for preventing and controlling venereal disease and infections disease |
| CN102363740A (en) * | 2010-12-10 | 2012-02-29 | 江南大学 | Low-irritation and high-foaminess fancy soap formula |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103695210A (en) * | 2013-12-20 | 2014-04-02 | 苏黎 | Traditional Chinese medicine scented soap |
| CN104911047A (en) * | 2015-05-18 | 2015-09-16 | 彭婷婷 | Honeysuckle flower traditional Chinese medicine antibacterial soap |
| CN104946434A (en) * | 2015-07-21 | 2015-09-30 | 安徽建筑大学 | Pure natural skin care perfumed soap and preparation method thereof |
| CN105400619A (en) * | 2015-12-11 | 2016-03-16 | 梁文成 | Aloe powder mixed soap |
| CN105441232A (en) * | 2015-12-11 | 2016-03-30 | 梁文成 | Capsaicin composite soap |
| CN107893001A (en) * | 2017-11-29 | 2018-04-10 | 深圳市地藏心文化传播有限公司 | A kind of natural handmade soap of the extract solution containing vine tea |
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| CN103194340B (en) | 2014-12-24 |
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Effective date of registration: 20180920 Address after: 244000 the eastern side of the government of the grey River Township in the outskirts of Tongling, Anhui Patentee after: Anhui Jinguang Agricultural Service Co., Ltd. Address before: 201604 219, room 2, Lane 1000, Tower Road, Shek Hu Town, Songjiang District, Shanghai Patentee before: Shanghai Bafang Fine Chemical Engineering Co., Ltd. |
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