CN103169118B - Method for preparing turbid blueberry and Chinese yam juice drink - Google Patents

Method for preparing turbid blueberry and Chinese yam juice drink Download PDF

Info

Publication number
CN103169118B
CN103169118B CN201310120554.0A CN201310120554A CN103169118B CN 103169118 B CN103169118 B CN 103169118B CN 201310120554 A CN201310120554 A CN 201310120554A CN 103169118 B CN103169118 B CN 103169118B
Authority
CN
China
Prior art keywords
blueberry
yam
cloudy
chinese yam
drink
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201310120554.0A
Other languages
Chinese (zh)
Other versions
CN103169118A (en
Inventor
谢志镭
徐志宏
林露
潘艳琴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANGHAI INSTITUTE OF FOOD
NANJING XINDELI FOOD CO Ltd
Original Assignee
SHANGHAI INSTITUTE OF FOOD
NANJING XINDELI FOOD CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANGHAI INSTITUTE OF FOOD, NANJING XINDELI FOOD CO Ltd filed Critical SHANGHAI INSTITUTE OF FOOD
Priority to CN201310120554.0A priority Critical patent/CN103169118B/en
Publication of CN103169118A publication Critical patent/CN103169118A/en
Application granted granted Critical
Publication of CN103169118B publication Critical patent/CN103169118B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention relates to a method for preparing turbid blueberry and Chinese yam juice drink and blueberry and Chinese yam juice drink obtained by the method. The method comprises the following steps: performing boiling and curing, cooling and ageing and separating starch gel removal treatment on Chinese yam powder, performing enzymolysis and centrifugal separation to obtain the destarched Chinese yam juice; sequentially adding a mixed solution of pectin and high fructose corn syrups and concentrated blueberry juice into the destarched Chinese yam juice, uniformly mixing, regulating pH by using citric acid and sodium citrate, diluting, canning and sterilizing, and thus obtaining the turbid blueberry and Chinese yam juice drink. The turbid uniform fruit and vegetable juice drink prepared by the method has the quality guarantee period of one year at normal temperature, has a little precipitation after being stood for a long time and is not layered.

Description

A kind of preparation method of Cloudy blueberry yam drink
Technical field
The preparation method who the present invention relates to a kind of Cloudy blueberry yam drink, belongs to health food drink manufacture field.
Background technology
Blueberry is that the fruit pulp that a kind of nutritive value is very high is rich in the nutrients such as abundant vitamin, physiological activator and mineral matter, wherein in blueberry, unique precious anthocyanin pigment proportion in many fruit is height very, also have in blueberry and be rich in the nutrients such as rich in protein, dietary fiber, fat, vitamin, the nutrition that the nutrient that in blueberry, these are rich in is all rich in higher than other fruit.In blueberry, also comprising the trace quantity mineral substance elements such as abundant calcium, iron, phosphorus, zinc, these mineral elements exist ratio apparently higher than other fruit.So blueberry is a kind of fruit of high nutrition.
The anthocyanin pigment that in blueberry, content is very high has the effect of maintenance well to the eyes of human body, it can relieving eye strain, improve people's eyesight, promote the regeneration of visual purple (Rhodopsin) in retina cell, in blueberry, be rich in nutritional labelings such as enriching vitamin, mineral matter and fiber element, the more edible blueberry can improve body immunity, improves human quality.In blueberry, abundant vitamin C has pre-anti-cancer in addition, resists cardiopathic effect.Blueberry pectin is abundant, can dilute body fat, the health of protection human body cardiovascular and cerebrovascular.In addition, in blueberry, also has abundant antioxidant, aging that can delaying human body.
Modern pharmacological research confirms, RHIIZOMA DIOSCOREAE from Henan of China has nutritious tonifying, induce disturb element, strengthen immunity of organisms, excretion in scheduling, tonifying Qi are promoted blood circulation, kobadrin, relieving asthma etc. and to help to change, coronary artery and micro-samsara blood flow can be improved, chronic bronchitis, hat unpleasantness, angina pectoris etc. can be treated.Iron rod yam has the function of qi invigorating and lung moistening, both can cut into slices to decoct juice and work as tea-drinking, can chop up to cook congee again and drink, and void cough and tuberculosis fever patient are had to good treatment results.Spring, weather was more uninteresting, and easily impariment of the lung Tianjin, causes the deficiency of Yin, occurs the illnesss such as dry, dry throat, parched lips, dry cough, and the Chinese yam of now nourishing is the most applicable, because Chinese yam is the product of safe calmness, was that product on lung are supported in enriching yin.
In daily life, blueberry Chinese yam is one cuisines, there is not yet but blueberry is combined with Chinese yam make on blueberry yam drink market, the present invention based on blueberry and Chinese yam combination are made to a kind of popular health beverages that is easy to carry, conveniently drinks, provides a kind of preparation for processing just.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of Cloudy blueberry yam drink, first yam flour carried out to poach slaking, cool aging and separate desizing Gel Treatment, then enzymolysis and centrifugation obtain destarch Succus Rhizoma Dioscoreae; Then the mixed liquor and the concentrated blueberry juice that in destarch Succus Rhizoma Dioscoreae, successively add pectin and fruit glucose syrup, mix, and regulates sterilization after pH, dilution tinning afterwards with citric acid and natrium citricum, obtains described Cloudy blueberry yam drink.
The present invention is achieved by the following technical solutions:
A preparation method for Cloudy blueberry yam drink, specifically comprises the following steps:
(1) in yam flour, add water, heating is stirred to complete slaking;
(2) cooling leaving standstill to the abundant aging formation gel of starch in Chinese yam;
(3) starch gel is removed in centrifugation, obtains just destarch Succus Rhizoma Dioscoreae;
(4) heat above-mentioned just destarch Succus Rhizoma Dioscoreae, then add amylase that remaining amylorrhexis is become to dextrin;
(5) centrifugation again, obtains destarch Succus Rhizoma Dioscoreae;
(6) pectin is sneaked into fruit glucose syrup, then join in above-mentioned destarch Succus Rhizoma Dioscoreae, be mixed, then add concentrated blueberry juice, stirring is mixed;
(7) adjust pH to 3.0~3.5 with aqueous citric acid solution and sodium citrate aqueous solution, obtain blueberry Chinese yam slip;
(8) be diluted with water;
(9) tinning after heating, more coolingly after water dip sterilization obtain described Cloudy blueberry yam drink.
Wherein,
In step (1), described yam flour is 100% pure yam flour, and granularity is 80~100 orders; After Chinese yam is dried, pulverize and make through powder beater.
In step (1), the ratio of the weight of described yam flour and water is 0.5-4:80-120, is preferably 1-2:80-120; The temperature that adds thermal agitation is 85-95 DEG C, is preferably 90-95 DEG C; The time that adds thermal agitation is 5-10 minute, is preferably 8-10 minute.
In step (2), described cooling standing temperature is 5-10 DEG C, is preferably 5-8 DEG C; The cooling standing time is 8-12 hour, is preferably 10-12 hour.
In step (3), the rotating speed of described centrifugation is 2500-3000rpm; The time of centrifugation is 15-30 minute.
In step (4), the ratio of described just destarch Succus Rhizoma Dioscoreae and diastatic weight is 80-120:0.01-0.1, is preferably 100-120:0.01-0.05; The temperature of enzymolysis is 70-95 DEG C, is preferably 93-95 DEG C; The time of enzymolysis is 5-40 minute, is preferably 5-10 minute.
In step (5), the rotating speed of described centrifugation is 2500-3000rpm, is preferably 2800-3000rpm; The time of centrifugation is 15-30 minute, is preferably 25-30 minute.
In step (6), the ratio of the weight of described pectin, fruit glucose syrup, destarch Succus Rhizoma Dioscoreae and blueberry inspissated juice is 0.1-0.6:5-12:80-120:0.5-1.5, is preferably 0.1-0.3:7-10:80-120:0.8-1.2.
Preferably, described concentrated blueberry juice is the concentrated blueberry juice of imported from America.
In step (7), in described aqueous citric acid solution, the concentration of citric acid is 2-15wt%; In sodium citrate aqueous solution, the concentration of natrium citricum is 2-10wt%.
In step (8), described in be diluted with water the mixing quality of process blueberry Chinese yam slip and water ratio be 95-99.9:0.1-5.
In step (9), the temperature of described heating is 80-85 DEG C, is preferably 80-83 DEG C; The temperature of described water-bath is 90-95 DEG C, is preferably 93-95 DEG C; The time of described sterilization is 10-15 minute, is preferably 12-15 minute.
The Cloudy blueberry yam drink that the inventive method obtains is the uniform fruit-vegetable juice beverage of a kind of Cloudy, and the normal temperature shelf-life is 1 year, has a small amount of precipitation after being long placed in, but there will not be upper and lower lamination.The sweet middle band acid of this beverage, good palatability.Be particularly suitable for long-term sitting, the white collar personnel of excess eye-using drink.Can strengthen white collar personnel's immunocompetence, improve visual fatigue.
Detailed description of the invention
By specific instantiation, technical scheme of the present invention is described below.Should be understood that one or more method steps that the present invention mentions do not repel between the step that also has additive method step or clearly mention at these before and after described combination step can also insert additive method step; Should also be understood that these embodiment are only not used in and limit the scope of the invention for the present invention is described.And, except as otherwise noted, the numbering of various method steps is only for differentiating the convenient tool of various method steps, but not for limiting the ordering of various method steps or limiting the enforceable scope of the present invention, the change of its relativeness or adjustment, in the situation that changing technology contents without essence, when being also considered as the enforceable category of the present invention.
Embodiment 1
Prepare a kind of Cloudy blueberry yam drink:
Primary raw material:
Composition Manufacturer, model or purity
Yam flour 100% pure yam flour, 80-100 order
Alpha-amylase 18000U-25000U/g
Blueberry inspissated juice Imported from America, 68Brix
HFCS 77Brix
Pectin Food stage
Citric acid Food stage
Natrium citricum Food stage
Water Pure water
Preparation method:
(1) get 2 Keshan medicinal powder, add 98 grams of water, stir, be heated to 95 DEG C, continue heat and stir 5 minutes, to the complete slaking of Chinese yam;
(2) be cooled to 8 DEG C, then leave standstill 10 hours to the abundant aging formation gel of starch in Chinese yam;
(3) with centrifuge centrifugation 20 minutes under the rotating speed of 3000rpm, remove starch gel precipitation, obtain approximately 90 grams at the beginning of destarch Succus Rhizoma Dioscoreae;
(4) above-mentioned just destarch Succus Rhizoma Dioscoreae is heated to 95 DEG C, then adds 0.01 gram of alpha-amylase, enzymolysis 5 minutes, becomes dextrin by remaining amylorrhexis at 95 DEG C;
(5) with centrifuge centrifugation 20 minutes under 3000rpm speed, remove a small amount of residue, obtain approximately 88 grams of destarch Succus Rhizoma Dioscoreaes;
(6) 0.12 gram of pectin is sneaked in 9 grams of fruit glucose syrups, then join in above-mentioned destarch Succus Rhizoma Dioscoreae, after being uniformly mixed, add 1 gram of concentrated blueberry juice, stir 5 minutes to even;
(7) sodium citrate aqueous solution that the aqueous citric acid solution that compound concentration is 10wt% and concentration are 10wt% is adjusted liquid as pH, and regulating and obtaining pH is 99 grams of 3.2 blueberry Chinese yam slips;
(8) be diluted with water to 100 grams;
(9) be heated to 80 DEG C and pack in three beverage cans, approximately 310 milliliters of filling amounts, sealing machine sealing, then through 90 DEG C of water-baths sterilization in 10 minutes, after cooling described Cloudy blueberry yam drink.
The blueberry yam drink obtaining is the uniform fruit-vegetable juice beverage of lavender Cloudy, and the lower shelf-life of normal temperature is 1 year, after being long placed in, has microprecipitation, but there will not be lower leaf.Taste is sour-sweet moderate, is lavender Cloudy beverage, is applicable to sitting and visual fatigue white collar personage and drinks.
Embodiment 2
Prepare a kind of Cloudy blueberry yam drink:
Primary raw material:
Composition Manufacturer, model or purity
Yam flour 100% pure yam flour, 80-100 order
Middle temperature amylase 3000U-8000U/g
Blueberry inspissated juice Imported from America, 68Brix
HFCS 77Brix
Pectin Food stage
Citric acid Food stage
Natrium citricum Food stage
Water Pure water
Preparation method:
(1) get 1.5 Keshan medicinal powder, add 98.5 grams of water, stir, be heated to 95 DEG C, continue heat and stir 5 minutes, to the complete slaking of Chinese yam;
(2) be cooled to 10 DEG C, then leave standstill 12 hours to the abundant aging formation gel of starch in Chinese yam;
(3) with centrifuge centrifugation 30 minutes under the rotating speed of 2750rpm, remove starch gel precipitation, obtain approximately 90 grams at the beginning of destarch Succus Rhizoma Dioscoreae;
(4) above-mentioned just destarch Succus Rhizoma Dioscoreae is heated to 95 DEG C, then adds 0.03 gram of middle temperature amylase, enzymolysis 30 minutes, becomes dextrin by remaining amylorrhexis at 70 DEG C;
(5) with centrifuge centrifugation 30 minutes under 2800rpm speed, remove a small amount of residue, obtain approximately 88 grams of destarch Succus Rhizoma Dioscoreaes;
(6) 0.14 gram of pectin is sneaked in 10 grams of fruit glucose syrups, then join in above-mentioned destarch Succus Rhizoma Dioscoreae, stir 15 minutes to evenly, then add 0.9 gram of concentrated blueberry juice, stir 5 minutes extremely evenly;
(7) sodium citrate aqueous solution that the aqueous citric acid solution that compound concentration is 10wt% and concentration are 10wt% is adjusted liquid as pH, and regulating and obtaining pH is 99.5 grams of 3.0 blueberry Chinese yam slips;
(8) be diluted with water to 100 grams;
(9) be heated to 80 DEG C and pack in three beverage cans, approximately 310 milliliters of filling amounts, sealing machine sealing, then through 90 DEG C of water-baths sterilization in 10 minutes, after cooling described Cloudy blueberry yam drink.
The blueberry yam drink obtaining is the uniform fruit-vegetable juice beverage of lavender Cloudy, and the lower shelf-life of normal temperature is 1 year, after being long placed in, has microprecipitation, but there will not be lower leaf.Taste is sour-sweet moderate, is lavender Cloudy beverage, is applicable to sitting and visual fatigue white collar personage and drinks.

Claims (8)

1. a preparation method for Cloudy blueberry yam drink, comprises following concrete steps:
(1) in yam flour, add water, heating is stirred to complete slaking;
(2) cooling leaving standstill to the abundant aging formation gel of starch in Chinese yam;
(3) starch gel is removed in centrifugation, obtains just destarch Succus Rhizoma Dioscoreae;
(4) heat above-mentioned just destarch Succus Rhizoma Dioscoreae, then add amylase that remaining amylorrhexis is become to dextrin;
(5) centrifugation again, obtains destarch Succus Rhizoma Dioscoreae;
(6) pectin is sneaked into fruit glucose syrup, then join in above-mentioned destarch Succus Rhizoma Dioscoreae, be mixed, then add concentrated blueberry juice, stirring is mixed;
(7) adjust pH to 3.0~3.5 with aqueous citric acid solution and sodium citrate aqueous solution, obtain blueberry Chinese yam slip;
(8) be diluted with water;
(9) tinning after heating, more coolingly after water dip sterilization obtain described Cloudy blueberry yam drink;
In step (1), the ratio of the weight of described yam flour and water is 0.5-4:80-120; The temperature that adds thermal agitation is 85-95 DEG C; The time that adds thermal agitation is 5-10 minute;
In step (2), described cooling standing temperature is 5-10 DEG C; The cooling standing time is 8-12 hour;
In step (4), the ratio of described just destarch Succus Rhizoma Dioscoreae and diastatic weight is 80-120:0.01-0.1; The temperature of enzymolysis is 70-95 DEG C; The time of enzymolysis is 5-40 minute;
In step (6), the ratio of the weight of described pectin, fruit glucose syrup, destarch Succus Rhizoma Dioscoreae and blueberry inspissated juice is 0.1-0.6:5-12:80-120:0.5-1.5.
2. the preparation method of a kind of Cloudy blueberry yam drink as claimed in claim 1, is characterized in that, in step (1), described yam flour is 100% pure yam flour, and granularity is 80~100 orders.
3. the preparation method of a kind of Cloudy blueberry yam drink as claimed in claim 1, is characterized in that, in step (3), the rotating speed of described centrifugation is 2500-3500rpm; The time of centrifugation is 15-30 minute.
4. the preparation method of a kind of Cloudy blueberry yam drink as claimed in claim 1, is characterized in that, in step (5), the rotating speed of described centrifugation is 2500-3000rpm; The time of centrifugation is 15-30 minute.
5. the preparation method of a kind of Cloudy blueberry yam drink as claimed in claim 1, is characterized in that, in step (7), in described aqueous citric acid solution, the concentration of citric acid is 2-15wt%; The concentration of sodium citrate aqueous solution natrium citricum is 2-10wt%.
6. the preparation method of a kind of Cloudy blueberry yam drink as claimed in claim 1, is characterized in that, in step (8), described in be diluted with water the mixed weight of process blueberry Chinese yam slip and water ratio be 95-99.9:0.1-5.
7. the preparation method of a kind of Cloudy blueberry yam drink as claimed in claim 1, is characterized in that, in step (9), the temperature of described heating is 80-85 DEG C; The temperature of described water-bath is 90-95 DEG C, and the time of described sterilization is 10-15 minute.
8. a kind of Cloudy blueberry yam drink being made by the arbitrary described preparation method of claim 1-7.
CN201310120554.0A 2013-04-09 2013-04-09 Method for preparing turbid blueberry and Chinese yam juice drink Expired - Fee Related CN103169118B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310120554.0A CN103169118B (en) 2013-04-09 2013-04-09 Method for preparing turbid blueberry and Chinese yam juice drink

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310120554.0A CN103169118B (en) 2013-04-09 2013-04-09 Method for preparing turbid blueberry and Chinese yam juice drink

Publications (2)

Publication Number Publication Date
CN103169118A CN103169118A (en) 2013-06-26
CN103169118B true CN103169118B (en) 2014-09-10

Family

ID=48629661

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310120554.0A Expired - Fee Related CN103169118B (en) 2013-04-09 2013-04-09 Method for preparing turbid blueberry and Chinese yam juice drink

Country Status (1)

Country Link
CN (1) CN103169118B (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104770811A (en) * 2014-01-14 2015-07-15 王志华 Technical process for solving precipitation of Chinese chestnut-containing beverage
CN105982139A (en) * 2016-01-06 2016-10-05 王龙云 Qi regulating and phlegm eliminating beverage containing tuber borchii and yolk and preparation method of Qi regulating and phlegm eliminating beverage
CN106722516A (en) * 2016-11-24 2017-05-31 贵州盛禾特色农产品有限公司 A kind of processing method of blueberry canned Chinese yam
CN107997100A (en) * 2017-10-19 2018-05-08 重庆德庄农产品开发有限公司 A kind of boiling hot food water-soaked food is not easy the chafing dish bottom flavorings and manufacture craft of muddiness
CN108208662A (en) * 2018-03-24 2018-06-29 厦门市诚安毅科技有限公司 A kind of formula and preparation method for compounding nutritional Chinese yam brewed powder

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101258938A (en) * 2008-04-17 2008-09-10 温书太 Method for manufacturing yam beverage
CN101756315A (en) * 2010-01-13 2010-06-30 焦作市怀山纯食品开发有限公司 Pure yam drink and preparation method thereof
CN102860550A (en) * 2011-07-05 2013-01-09 江苏亚帆生物科技有限公司 Functional beverage having functions of tonifying kidney, boosting virility and raising immunity and preparation method thereof
CN102894431A (en) * 2012-10-29 2013-01-30 郑州朴素堂食品股份有限公司 Method for making yam juice

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3766670B2 (en) * 2003-12-16 2006-04-12 花王株式会社 Container drink
JP2006180856A (en) * 2004-12-24 2006-07-13 Okinawa Bireley's:Kk Method for producing high concentration high viscosity guava fruit juice drink

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101258938A (en) * 2008-04-17 2008-09-10 温书太 Method for manufacturing yam beverage
CN101756315A (en) * 2010-01-13 2010-06-30 焦作市怀山纯食品开发有限公司 Pure yam drink and preparation method thereof
CN102860550A (en) * 2011-07-05 2013-01-09 江苏亚帆生物科技有限公司 Functional beverage having functions of tonifying kidney, boosting virility and raising immunity and preparation method thereof
CN102894431A (en) * 2012-10-29 2013-01-30 郑州朴素堂食品股份有限公司 Method for making yam juice

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
JP特开2006-180856A 2006.07.13
汪伦记,等.怀山药保健饮料生产工艺的研究.《食品研究与开发》.2005,第26卷(第4期),第80页右栏第3段-81页左栏第8段、第81页右栏第1段. *
赵静,等.新型山药饮料的开发.《食品研究与开发》.2009,第30卷(第3期),第68-70页. *

Also Published As

Publication number Publication date
CN103169118A (en) 2013-06-26

Similar Documents

Publication Publication Date Title
CN103169118B (en) Method for preparing turbid blueberry and Chinese yam juice drink
CN104017694A (en) Brewing technique of low-sugar red date rice wine
CN105368629A (en) Processing method of blueberry fruit wine
CN105941722A (en) Brown sugar and black tea compound drink and preparing method thereof
CN103734236A (en) Chinese chestnut and cheese biscuit and preparation method thereof
CN105454941A (en) Kiwi fruit and banana compound juice
CN103976021A (en) Preparation method of nut functional yogurt
CN106901116B (en) A kind of fermentation process of Amorphophallus rivieri beverage
CN103082079A (en) Cereal soya bean ice cream and production method thereof
CN103789130A (en) Composite fermentation production technology of winter-jujube healthcare wine
CN102550672A (en) Method for preparing sweet potato and black rice fermented milk
CN104472978A (en) Blueberry jelly and preparing method thereof
CN107410993A (en) Without chemistry addition blueberry jam and preparation method thereof
CN103622105A (en) Preparation method of hawthorn and smoked plum compound fruit flesh beverage concentrate
CN102405987A (en) Bean product with wine taste
CN107114488A (en) A kind of nutrient dried rolled bean curd of nourishing the stomach containing Chinese medicine and preparation method thereof
CN106720355A (en) A kind of workplace type wheat embryo composite milk powder and preparation method thereof
CN103271153A (en) Pearl powder-containing coffee yoghourt and preparation method thereof
CN102919371A (en) Pine flower milk tea and preparation method thereof
CN111955553A (en) Tartary buckwheat, inulin and pearl milk tea and preparation method thereof
CN105379842A (en) Composite yoghourt and preparation method thereof
CN107686786A (en) A kind of passion fruit fresh fruit rice makes brewage process
CN102204590B (en) Dairy product with reducing pathogenic fire
CN105594855A (en) Sour jujube-Chinese wolfberry yoghurt beverage and preparation method thereof
CN103636793A (en) Formula of purple sweet potato beverage

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140910

Termination date: 20180409