CN103142703B - Processing technology of anti-mildew of frutus forsythiae - Google Patents
Processing technology of anti-mildew of frutus forsythiae Download PDFInfo
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- CN103142703B CN103142703B CN 201310126920 CN201310126920A CN103142703B CN 103142703 B CN103142703 B CN 103142703B CN 201310126920 CN201310126920 CN 201310126920 CN 201310126920 A CN201310126920 A CN 201310126920A CN 103142703 B CN103142703 B CN 103142703B
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Abstract
The invention relates to an anti-mildew processing process of fructus forsythiae. The fructus forsythiae are green fructus forsythiae, the processing process comprises four steps including raw material selection, fructus forsythiae leaf digestion, green fructus forsythiae steaming and green fructus forsythiae drying treatment, the fructus forsythia adopts the high-pressure steaming, the time is saved, active enzyme ingredients which can easily cause the mildew in the fructus forsythiae can also be fast killed, and the fructus forsythiae core mildew is avoided, so the extraction rate of fructus forsythiae volatile oil is ensured. In the high-temperature steaming treatment process of the fructus forsythiae, fructus forsythiae leaching liquid is continually sprayed, the action range of the pesticide effect can be increased, the exertion of the pesticide effect of the fructus forsythiae is promoted, in addition, the fragrance of the fructus forsythiae can be enhanced, and people can easily accept the process. In the drying treatment method of the fructus forsythiae, hot air drying and low-frequency microwave treatment are combined, the drying velocity can be obviously improved, and in addition, the drying energy consumption can be obviously reduced. The microwaves have extremely high penetrability, the internal and external simultaneous heating can be realized, the moisture moving from inside to outside is accelerated, and the thorough drying of the fructus forsythiae from inside to outside is realized, the fructus forsythiae core mildew is avoided, and the extraction rate of the fructus forsythiae volatile oil is ensured.
Description
Technical field
The invention belongs to the Chinese medicine processing field, relate generally to a kind of processing procedure of Fructus Forsythiae, specifically the anti-processing procedure that goes mouldy of a kind of Fructus Forsythiae.
Background technology
Fructus Forsythiae is one of clinical Chinese medicine commonly used of China, the dry fruit that Fructus Forsythiae that records of Pharmacopoeia of the People's Republic of China version in 2005 is Oleaceae forsythia Fructus Forsythiae, fruit just ripe still gathering when band is green is called green grass or young crops and sticks up, and gathers to be called always during the well-done color jaundice of fruit and sticks up.Pharmacological action such as that Fructus Forsythiae has is antibiotic, heart tonifying, diuresis, town are told, diseases such as the acute anemopyretic cold of forsythia fruit for treating commonly used, carbuncle sore tumefacting virus, tuberculous lymphadenitis, urinary tract infection are the primary raw material of Chinese medicine preparation such as SHUANGHUANGLIAN KOUFUYE, SHUANGHUANGLIAN FENZHENJI, QINGRE JIEDU KOUFUYE, the careless analgesic oral liquid of company, flos ionicerae and fructus forsythiae infusion for detoxication.But the traditional processing procedure of Fructus Forsythiae is processed with drying the method for drying with diaphoresis naturally for the fresh fruit of gathering annual August, the general easy core of Fructus Forsythiae that causes is mouldy, because the effective ingredient volatile oil of Fructus Forsythiae mainly concentrates in the Fructus Forsythiae core, therefore very big to the influence of extracting Forsythia volatile oil.
Summary of the invention
The purpose of this invention is to provide the anti-processing procedure that goes mouldy of a kind of Fructus Forsythiae, this technology can avoid the Fructus Forsythiae core mouldy, guarantees the extraction ratio of Forsythia volatile oil, and drug effect plays a role by force, and saves the processing procedure time.
The present invention realizes that the technical scheme that above-mentioned purpose adopts is: the anti-processing procedure that goes mouldy of Fructus Forsythiae, and described Fructus Forsythiae is that green grass or young crops sticks up, and may further comprise the steps:
Step 1, raw material are chosen
Major ingredient: green grass or young crops sticks up, and the amount of choosing is 95-99 part according to parts by weight;
Batching: Folium Forsythiae, the amount of choosing is 1-5 part according to parts by weight;
Remove impurity respectively, standby;
The lixiviate of step 2, Folium Forsythiae
The ready Folium Forsythiae of step 1 is cleaned with clear water, drained, place to decoct in the container, add 30-50 water doubly by Folium Forsythiae weight then, decoct 2-5h, filter, obtain the Folium Forsythiae lixiviating solution, standby;
What step 3, green grass or young crops stuck up steams
The ready green grass or young crops of step 1 is stuck up the steaming of the putting into the steaming and decocting under high pressure device enterprising horizontal high voltage of combing to be steamed, steaming pressure is 0.1-0.25MPa, steaming time is 1.5h, when beginning to steam, the Folium Forsythiae lixiviating solution that step 2 is obtained by the spray equipment on the steaming and decocting under high pressure device sprays on green grass or young crops sticks up, and spraying method is that every 15min sprays once, and the Folium Forsythiae lixiviating solution sprays in 1h and finishes, after steaming end, namely obtain sticking up through the green grass or young crops that steams, standby;
The dried that step 4, green grass or young crops stick up
The green grass or young crops that step 3 is steamed sticks up inserts in the box drier while hot, the pathogenic wind-warm of box drier is set to 70-80 ℃, wind speed 1m/s, green grass or young crops stuck up carry out dried, be dried to green grass or young crops stick up moisture content be below 45% after, green grass or young crops is stuck up taking-up leave standstill 20min, and then put into the low frequency microwave oven and carry out microwave drying, microwave frequency during microwave drying is 915MHz, microwave power is: every gram green grass or young crops sticks up 0.05W, in microwave drying process, adopt the blue or green temperature of sticking up the surface of infrared thermometry method monitoring, close microwave when green grass or young crops sticks up when surface temperature reaches 80 ℃, leave standstill 10-30min after, start the low frequency microwave oven again and carry out microwave drying by above-mentioned parameter, green grass or young crops sticks up when surface temperature reaches 80 ℃ closes microwave, leaves standstill 10-30min; The process that repeats above-mentioned microwave drying and leave standstill is stuck up moisture content≤4% until green grass or young crops, namely finishes the process of preparing Chinese medicine.
Beneficial effect of the present invention:
One, Fructus Forsythiae adopt high pressure steaming, not only saved than the room temperature dry in the sun and manyed a times time, also can kill fast and easily cause the organized enzyme composition that goes mouldy in the Fructus Forsythiae, avoid the Fructus Forsythiae core mouldy, thereby guarantee the extraction ratio of Forsythia volatile oil, through test determination, the Forsythia volatile oil that the Fructus Forsythiae after high pressure steams processing extracts exceeds twice than the volatilization oil mass of the Fructus Forsythiae extraction of conventional process.
Two, Folium Forsythiae has effects such as heat-clearing and toxic substances removing, promoting the production of body fluid to quench thirst, antibiotic diuresis, invigorating the stomach and promoting digestion, enhancing immunity, and fragrance is pure, flavour is dense, the present invention is in carrying out Fructus Forsythiae high temperature steaming processing procedure, spray the Folium Forsythiae lixiviating solution in batches, be conducive to Folium Forsythiae lixiviating solution infiltration green grass or young crops and stick up, can not only increase the drug action scope, promote human consumption to absorb, strengthen the performance of Fructus Forsythiae drug effect, and can increase the fragrance of Fructus Forsythiae, the easier people of allowing accept; The spray process is finished at 1h, and remaining 0.5h steams the effective ingredient that makes Folium Forsythiae and fragrance is abundant and green grass or young crops sticks up combination.
Three, first hot air drying in the drying method of Fructus Forsythiae of the present invention, low frequency microwave drying again with hot air drying and low frequency microwave treatment reasonable combination, can obviously improve dry rate, and can obviously reduce energy consumption for drying.Microwave has extremely strong penetrance, heating simultaneously inside and outside can realizing, under the condition of low power density, can accelerate moisture migration from inside to outside, realize Fructus Forsythiae finish-drying from inside to outside, avoided the Fructus Forsythiae core mouldy, guaranteed the extraction ratio of Forsythia volatile oil, and fluffy through the Fructus Forsythiae structure of high pressure steaming processing, help to accelerate rate of drying and improve drying efficiency.Leave standstill earlier during microwave drying and begin microwave again, can effectively reduce the number of times that microwave is closed, prolong the microwave time, strengthen drying efficiency, and the low frequency cold drying can effectively reduce the nutritional labeling forfeiture.
The specific embodiment
The anti-processing procedure that goes mouldy of Fructus Forsythiae, described Fructus Forsythiae is that green grass or young crops sticks up, and may further comprise the steps:
Step 1, raw material are chosen
Major ingredient: green grass or young crops sticks up, and the amount of choosing is 95-99 part according to parts by weight;
Batching: Folium Forsythiae, the amount of choosing is 1-5 part according to parts by weight;
Remove impurity respectively, standby;
The lixiviate of step 2, Folium Forsythiae
The ready Folium Forsythiae of step 1 is cleaned with clear water, drained, place to decoct in the container, add 30-50 water doubly by Folium Forsythiae weight then, decoct 2-5h, filter, obtain the Folium Forsythiae lixiviating solution, standby;
What step 3, green grass or young crops stuck up steams
The ready green grass or young crops of step 1 is stuck up the steaming of the putting into the steaming and decocting under high pressure device enterprising horizontal high voltage of combing to be steamed, steaming pressure is 0.1-0.25MPa, steaming time is 1.5h, when beginning to steam, the Folium Forsythiae lixiviating solution that step 2 is obtained by the spray equipment on the steaming and decocting under high pressure device sprays on green grass or young crops sticks up, and spraying method is that every 15min sprays once, and the Folium Forsythiae lixiviating solution sprays in 1h and finishes, after steaming end, namely obtain sticking up through the green grass or young crops that steams, standby;
The dried that step 4, green grass or young crops stick up
The green grass or young crops that step 3 is steamed sticks up inserts in the box drier while hot, the pathogenic wind-warm of box drier is set to 70-80 ℃, wind speed 1m/s, green grass or young crops stuck up carry out dried, be dried to green grass or young crops stick up moisture content be below 45% after, green grass or young crops is stuck up taking-up leave standstill 20min, and then put into the low frequency microwave oven and carry out microwave drying, microwave frequency during microwave drying is 915MHz, microwave power is: every gram green grass or young crops sticks up 0.05W, in microwave drying process, adopt the blue or green temperature of sticking up the surface of infrared thermometry method monitoring, close microwave when green grass or young crops sticks up when surface temperature reaches 80 ℃, leave standstill 10-30min after, start the low frequency microwave oven again and carry out microwave drying by above-mentioned parameter, green grass or young crops sticks up when surface temperature reaches 80 ℃ closes microwave, leaves standstill 10-30min; The process that repeats above-mentioned microwave drying and leave standstill is stuck up moisture content≤4% until green grass or young crops, namely finishes the process of preparing Chinese medicine.
The present invention will be further described below in conjunction with specific embodiment:
Embodiment 1:
The anti-processing procedure that goes mouldy of Fructus Forsythiae, described Fructus Forsythiae is that green grass or young crops sticks up, and may further comprise the steps:
Step 1, raw material are chosen
Major ingredient: green grass or young crops sticks up, and the amount of choosing is 99 parts according to parts by weight;
Batching: Folium Forsythiae, the amount of choosing is 1 part according to parts by weight;
Remove impurity respectively, standby;
The lixiviate of step 2, Folium Forsythiae
The ready Folium Forsythiae of step 1 is cleaned with clear water, drained, place to decoct in the container, add 30 times water then by Folium Forsythiae weight, decoct 2h, filter, obtain the Folium Forsythiae lixiviating solution, standby;
What step 3, green grass or young crops stuck up steams
The ready green grass or young crops of step 1 is stuck up the steaming of the putting into the steaming and decocting under high pressure device enterprising horizontal high voltage of combing to be steamed, steaming pressure is 0.1MPa, steaming time is 1.5h, when beginning to steam, the Folium Forsythiae lixiviating solution that step 2 is obtained by the spray equipment on the steaming and decocting under high pressure device sprays on green grass or young crops sticks up, and spraying method is that every 15min sprays once, and the Folium Forsythiae lixiviating solution sprays in 1h and finishes, after steaming end, namely obtain sticking up through the green grass or young crops that steams, standby;
The dried that step 4, green grass or young crops stick up
The green grass or young crops that step 3 is steamed sticks up inserts in the box drier while hot, the pathogenic wind-warm of box drier is set to 70 ℃, wind speed 1m/s, green grass or young crops stuck up carry out dried, be dried to green grass or young crops stick up moisture content be below 45% after, green grass or young crops is stuck up taking-up leave standstill 20min, and then put into the low frequency microwave oven and carry out microwave drying, microwave frequency during microwave drying is 915MHz, microwave power is: every gram green grass or young crops sticks up 0.05W, in microwave drying process, adopt the blue or green temperature of sticking up the surface of infrared thermometry method monitoring, close microwave when green grass or young crops sticks up when surface temperature reaches 80 ℃, leave standstill 10min after, start the low frequency microwave oven again and carry out microwave drying by above-mentioned parameter, green grass or young crops sticks up when surface temperature reaches 80 ℃ closes microwave, leaves standstill 10min; The process that repeats above-mentioned microwave drying and leave standstill is stuck up moisture content≤4% until green grass or young crops, namely finishes the process of preparing Chinese medicine.
Embodiment 2:
The anti-processing procedure that goes mouldy of Fructus Forsythiae, described Fructus Forsythiae is that green grass or young crops sticks up, and may further comprise the steps:
Step 1, raw material are chosen
Major ingredient: green grass or young crops sticks up, and the amount of choosing is 95 parts according to parts by weight;
Batching: Folium Forsythiae, the amount of choosing is 5 parts according to parts by weight;
Remove impurity respectively, standby;
The lixiviate of step 2, Folium Forsythiae
The ready Folium Forsythiae of step 1 is cleaned with clear water, drained, place to decoct in the container, add 50 times water then by Folium Forsythiae weight, decoct 5h, filter, obtain the Folium Forsythiae lixiviating solution, standby;
What step 3, green grass or young crops stuck up steams
The ready green grass or young crops of step 1 is stuck up the steaming of the putting into the steaming and decocting under high pressure device enterprising horizontal high voltage of combing to be steamed, steaming pressure is 0.25MPa, steaming time is 1.5h, when beginning to steam, the Folium Forsythiae lixiviating solution that step 2 is obtained by the spray equipment on the steaming and decocting under high pressure device sprays on green grass or young crops sticks up, and spraying method is that every 15min sprays once, and the Folium Forsythiae lixiviating solution sprays in 1h and finishes, after steaming end, namely obtain sticking up through the green grass or young crops that steams, standby;
The dried that step 4, green grass or young crops stick up
The green grass or young crops that step 3 is steamed sticks up inserts in the box drier while hot, the pathogenic wind-warm of box drier is set to 80 ℃, wind speed 1m/s, green grass or young crops stuck up carry out dried, be dried to green grass or young crops stick up moisture content be below 45% after, green grass or young crops is stuck up taking-up leave standstill 20min, and then put into the low frequency microwave oven and carry out microwave drying, microwave frequency during microwave drying is 915MHz, microwave power is: every gram green grass or young crops sticks up 0.05W, in microwave drying process, adopt the blue or green temperature of sticking up the surface of infrared thermometry method monitoring, close microwave when green grass or young crops sticks up when surface temperature reaches 80 ℃, leave standstill 30min after, start the low frequency microwave oven again and carry out microwave drying by above-mentioned parameter, green grass or young crops sticks up when surface temperature reaches 80 ℃ closes microwave, leaves standstill 30min; The process that repeats above-mentioned microwave drying and leave standstill is stuck up moisture content≤4% until green grass or young crops, namely finishes the process of preparing Chinese medicine.
Embodiment 3:
The anti-processing procedure that goes mouldy of Fructus Forsythiae, described Fructus Forsythiae is that green grass or young crops sticks up, and may further comprise the steps:
Step 1, raw material are chosen
Major ingredient: green grass or young crops sticks up, and the amount of choosing is 97 parts according to parts by weight;
Batching: Folium Forsythiae, the amount of choosing is 3 parts according to parts by weight;
Remove impurity respectively, standby;
The lixiviate of step 2, Folium Forsythiae
The ready Folium Forsythiae of step 1 is cleaned with clear water, drained, place to decoct in the container, add 40 times water then by Folium Forsythiae weight, decoct 3.5h, filter, obtain the Folium Forsythiae lixiviating solution, standby;
What step 3, green grass or young crops stuck up steams
The ready green grass or young crops of step 1 is stuck up the steaming of the putting into the steaming and decocting under high pressure device enterprising horizontal high voltage of combing to be steamed, steaming pressure is 0.175MPa, steaming time is 1.5h, when beginning to steam, the Folium Forsythiae lixiviating solution that step 2 is obtained by the spray equipment on the steaming and decocting under high pressure device sprays on green grass or young crops sticks up, and spraying method is that every 15min sprays once, and the Folium Forsythiae lixiviating solution sprays in 1h and finishes, after steaming end, namely obtain sticking up through the green grass or young crops that steams, standby;
The dried that step 4, green grass or young crops stick up
The green grass or young crops that step 3 is steamed sticks up inserts in the box drier while hot, the pathogenic wind-warm of box drier is set to 75 ℃, wind speed 1m/s, green grass or young crops stuck up carry out dried, be dried to green grass or young crops stick up moisture content be below 45% after, green grass or young crops is stuck up taking-up leave standstill 20min, and then put into the low frequency microwave oven and carry out microwave drying, microwave frequency during microwave drying is 915MHz, microwave power is: every gram green grass or young crops sticks up 0.05W, in microwave drying process, adopt the blue or green temperature of sticking up the surface of infrared thermometry method monitoring, close microwave when green grass or young crops sticks up when surface temperature reaches 80 ℃, leave standstill 20min after, start the low frequency microwave oven again and carry out microwave drying by above-mentioned parameter, green grass or young crops sticks up when surface temperature reaches 80 ℃ closes microwave, leaves standstill 20min; The process that repeats above-mentioned microwave drying and leave standstill is stuck up moisture content≤4% until green grass or young crops, namely finishes the process of preparing Chinese medicine.
Claims (1)
1. the anti-processing procedure that goes mouldy of Fructus Forsythiae, described Fructus Forsythiae is that green grass or young crops sticks up, and it is characterized in that: may further comprise the steps:
Step 1, raw material are chosen
Major ingredient: green grass or young crops sticks up, and the amount of choosing is 95-99 part according to parts by weight;
Batching: Folium Forsythiae, the amount of choosing is 1-5 part according to parts by weight;
Remove impurity respectively, standby;
The lixiviate of step 2, Folium Forsythiae
The ready Folium Forsythiae of step 1 is cleaned with clear water, drained, place to decoct in the container, add 30-50 water doubly by Folium Forsythiae weight then, decoct 2-5h, filter, obtain the Folium Forsythiae lixiviating solution, standby;
What step 3, green grass or young crops stuck up steams
The ready green grass or young crops of step 1 is stuck up the steaming of the putting into the steaming and decocting under high pressure device enterprising horizontal high voltage of combing to be steamed, steaming pressure is 0.1-0.25MPa, steaming time is 1.5h, when beginning to steam, the Folium Forsythiae lixiviating solution that step 2 is obtained by the spray equipment on the steaming and decocting under high pressure device sprays on green grass or young crops sticks up, and spraying method is that every 15min sprays once, and the Folium Forsythiae lixiviating solution sprays in 1h and finishes, after steaming end, namely obtain sticking up through the green grass or young crops that steams, standby;
The dried that step 4, green grass or young crops stick up
The green grass or young crops that the process that step 3 is obtained steams sticks up inserts in the box drier while hot, the pathogenic wind-warm of box drier is set to 70-80 ℃, wind speed 1m/s, green grass or young crops stuck up carry out dried, be dried to green grass or young crops stick up moisture content be below 45% after, green grass or young crops is stuck up taking-up leave standstill 20min, and then put into the low frequency microwave oven and carry out microwave drying, microwave frequency during microwave drying is 915MHz, microwave power is: every gram green grass or young crops sticks up 0.05W, in microwave drying process, adopt the blue or green temperature of sticking up the surface of infrared thermometry method monitoring, close microwave when green grass or young crops sticks up when surface temperature reaches 80 ℃, leave standstill 10-30min after, start the low frequency microwave oven again and carry out microwave drying by above-mentioned parameter, green grass or young crops sticks up when surface temperature reaches 80 ℃ closes microwave, leaves standstill 10-30min; The process that repeats above-mentioned microwave drying and leave standstill is stuck up moisture content≤4% until green grass or young crops, namely finishes the process of preparing Chinese medicine.
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| CN104886273A (en) * | 2014-03-06 | 2015-09-09 | 洛阳春魁农业开发有限公司 | Weeping Forsythia seed oil-containing peony seed blend oil and preparation method thereof |
| CN106720214A (en) * | 2016-12-09 | 2017-05-31 | 广州聚禅现代农业研究院有限公司 | A kind of method that hot wind and microwave dries lichee bacterium |
| CN108434205A (en) * | 2018-05-25 | 2018-08-24 | 四川仟源中药饮片有限公司 | A kind of microwave processing method of Fructus Forsythiae |
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| CN101632405A (en) * | 2009-08-19 | 2010-01-27 | 阳城县析城山土特产开发有限公司 | Method for preparing weeping forsythia tea |
| CN102783340A (en) * | 2012-08-21 | 2012-11-21 | 屯留县民康中药材开发有限公司 | Cultivation method of Forsythia |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101632405A (en) * | 2009-08-19 | 2010-01-27 | 阳城县析城山土特产开发有限公司 | Method for preparing weeping forsythia tea |
| CN102783340A (en) * | 2012-08-21 | 2012-11-21 | 屯留县民康中药材开发有限公司 | Cultivation method of Forsythia |
Non-Patent Citations (2)
| Title |
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| 赵超等.陕西道地药材连翘鲜品蒸煮工艺研究.《时珍国医国药》.2011,第22卷(第02期),438-440. |
| 陕西道地药材连翘鲜品蒸煮工艺研究;赵超等;《时珍国医国药》;20111231;第22卷(第02期);438-440 * |
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