CN103142437B - Application of Amygdalus pedunculatus pall oil to cosmetic field - Google Patents
Application of Amygdalus pedunculatus pall oil to cosmetic field Download PDFInfo
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- CN103142437B CN103142437B CN201310092086.0A CN201310092086A CN103142437B CN 103142437 B CN103142437 B CN 103142437B CN 201310092086 A CN201310092086 A CN 201310092086A CN 103142437 B CN103142437 B CN 103142437B
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Abstract
The invention discloses application of Amygdalus pedunculatus pall oil to the cosmetic field, wherein the Amygdalus pedunculatus pall oil is used as base oil to be massaged on the skin of the face and the body directly or after being added with essential oil; or the Amygdalus pedunculatus pall oil is used as one of raw materials to make moisturizer, skincare lotion, pasty mask, or hand cream and the like for daily nursing care of the skin; or the Amygdalus pedunculatus pall oil is used as one of raw materials to make cleansing oil and facial cleanser for cleaning the skin of the face; or the Amygdalus pedunculatus pall oil is adopted as an ultravioresistant oil-soluble main element to protect the skin; or the Amygdalus pedunculatus pall oil is adopted as one of raw materials of liquid shampoo, hair conditioner or hair oil for the daily nursing care of the hair.
Description
Technical field
The present invention relates to the application of amygdalus pedunculata pall oil in cosmetics.
Background technology
Prunus pedunculata Maxim. have another name called handle almond, Fructus seu semen pruni szechuanicae (
amygdalus pedunculatapall.), be the machaka of Rosaceae Amygdalus, be distributed in NORTHWEST CHINA arid, the mountain region of semiarid zone and desert region, mainly also have distribution in some areas such as North Shaanxi, Banner North Yinshan Mountain, Inner Mongolia Middle hills, Xinjiang, Ningxia, Hebei.Prunus pedunculata Maxim. has stronger preventing and fixing sand ability, and its kernel is rich in oils and fats, crude protein, has higher economic worth, is the first-selected seeds of administering development woody oleiferous plants base, northern Desert Area.2011, the State Administration of Forestry have approved 1,000,000 mu, Yulin Prefecture Prunus pedunculata Maxim. planting scheme.At present, begin to take shape in Prunus pedunculata Maxim. base.
Summary of the invention
The object of the invention is to provide the application of amygdalus pedunculata pall oil in cosmetic field, and amygdalus pedunculata pall oil can effectively nursing skin and hair, effects such as having deep layer nourishing, moisturizing, uvioresistant, clean, beautify.
Implementation procedure of the present invention is as follows:
(1) Prunus pedunculata Maxim. kernel is through decortication, remove impurity, drying;
(2) Prunus pedunculata Maxim. kernel carries out squeezing and gets oil, and feeding temperature is no more than 35 DEG C, and oil outlet temperature is no more than 50 DEG C;
(3) oils and fats after squeezing is through precipitating, filtering and obtain amygdalus pedunculata pall oil.
Amygdalus pedunculata pall oil can be used for cosmetic field, and described cosmetics are quintessence oil, emollient cream, makeup remover, facial milk cleanser, surfactant, hand cream, facial film, suntan lotion, hair conditioner, shampoo or hair oil.
Oil based on amygdalus pedunculata pall oil; directly or the skin massaging added for face and health after quintessence oil; or make emollient cream, surfactant, cream pack or hand cream etc. as one of raw material; for skin daily nursing, or as making one of the raw material of makeup remover, facial milk cleanser, clean for skin of face; or as anti-ultraviolet major oil soluble components; can skin be protected, or as one of the raw material of shampoo, hair conditioner or hair oil, for the daily nursing of hair.
Prunus pedunculata Maxim. kernel oil content is 45% ~ 58%, and in its oils and fats, unsaturated fatty acid content is up to 96% ~ 98%, is mainly 66% ~ 72% oleic acid, 26% ~ 30% linoleic acid, and rich in vitamin E, content is higher than 40mg/100g.The oils and fats that oleic acid content is high effectively can suppress the generation of peroxide, and vitamin E also has stronger oxidation resistance, therefore, amygdalus pedunculata pall oil good stability, not perishable.Amygdalus pedunculata pall oil relative density is 0.900 ~ 0.960; saponification number is 185 ~ 193, and iodine number is 106 ~ 120 (see table 1), is a kind of semi-drying oils and fats; amygdalus pedunculata pall oil, as one of the raw material of cosmetics, uses the rear effect can played protection to skin and hair and nourish.The characteristic that amygdalus pedunculata pall oil is different from other plant oil can also keep liquid condition when temperature is reduced to subzero 5 DEG C.It also has the ultraviolet performance of absorption preferably.Therefore, amygdalus pedunculata pall oil can as high-quality crude vegetal used for cosmetic.
Note: C
n:w, wherein n represents carbon number in fatty acid carbon chain, and w represents the number of unsaturated bond.
Advantage of the present invention:
(1) the present invention with the psammophytes amygdalus pedunculata pall oil of high-quality for raw material, for aspects such as massage oil, emollient cream, surfactant, cream pack, facial milk cleanser, effectively can improve skin, improve skin moisturizing degree, resist ultraviolet radiation, reach the object of skin nursing; For aspects such as shampoo, hair conditioner, hair oil, can reach clean, nurse, beautify the object of hair.
(2) with psammophytes Prunus pedunculata Maxim. for raw material, can be on the one hand the oiliness raw material that cosmetic field provides novel, Desert Control and resource made full use of combine on the other hand, there is wide DEVELOPMENT PROSPECT.
Accompanying drawing explanation
Fig. 1 is that amygdalus pedunculata pall oil is used in hand one week front and back design sketch as skin protection base oil, and A figure is before using, and B figure is after using;
Fig. 2 is that the facial cream containing amygdalus pedunculata pall oil is used in face two weeks front and back design sketchs, and A figure is before using, and B figure is after using;
Fig. 3 is the UV extinction spectrum figure of amygdalus pedunculata pall oil;
Fig. 4 is that amygdalus pedunculata pall oil is used on the forearm containing color make-up as makeup remover and common makeup remover, and A place is the action effect of amygdalus pedunculata pall oil, and B place is the action effect of common makeup remover.
Detailed description of the invention
(1) Prunus pedunculata Maxim. kernel is after shelling, remove impurity, and use drying equipment hot air drying, kernel temperature is lower than 50 DEG C, and moisture is lower than 6wt%;
(2) Prunus pedunculata Maxim. kernel is put into oil press to carry out squeezing and get oil, during charging, Prunus pedunculata Maxim. kernel temperature is no more than 35 DEG C, and oil outlet temperature is no more than 50 DEG C;
(3) oils and fats after squeezing is amygdalus pedunculata pall oil after precipitation, simple filtration, for subsequent use.
Embodiment 1: get appropriate amygdalus pedunculata pall oil and be directly applied in hand, face or body skin, gently rubs and is massaged into skin absorption, is used in hand one week front and back design sketch from Fig. 1 amygdalus pedunculata pall oil; Amygdalus pedunculata pall oil makes Skin Cell softness flexible, can reach effect of moisturizing skin.
Embodiment 2: similar to Example 1, difference is when using facial cream or emulsion, drips 1 ~ 2 amygdalus pedunculata pall oil, can form hydrophobic film at skin surface, and the facial cream containing amygdalus pedunculata pall oil from Fig. 2 is used in face two weeks front and back design sketchs; Facial cream containing amygdalus pedunculata pall oil can suppress the evaporation of transepidermal water, prevents xerosis cutis, coarse.
Embodiment 3: similar to Example 1, gets appropriate amygdalus pedunculata pall oil and is directly applied in hand, face or body skin, and gently rub and be massaged into skin absorption, amygdalus pedunculata pall oil can strengthen the anti-ultraviolet ability of skin, provides protective effect.
Embodiment 4: similar to Example 1, get appropriate amygdalus pedunculata pall oil and be directly applied in face containing color make-up, soft massage, face is rinsed with clear water, forearm Contrast on effect containing color make-up is used in as makeup remover and common makeup remover: amygdalus pedunculata pall oil can removal color make-up, improves the cleannes of skin from Fig. 3 amygdalus pedunculata pall oil.
Embodiment 5: similar to Example 1, difference is when using makeup remover, drips 2 ~ 3 amygdalus pedunculata pall oils, directly can be used in face, increases the ability of product cleaning skin, and in use by massage face, can reach the object of skin protection.
Embodiment 6: because essential oil concentration is higher, directly uses the zest of skin comparatively strong, by oil based on amygdalus pedunculata pall oil, can add quintessence oil and use.For 10ml amygdalus pedunculata pall oil, add 2 ~ 3 Flos Rosae Rugosae quintessence oils, directly can be applied to face, life-time service, can mottle be desalinated, fair skin.
Embodiment 7: similar to Example 6, difference adds 4 ~ 6 Herba Lysimachiae foenum-graeci quintessence oil in 10ml amygdalus pedunculata pall oil, and for the massage of health skin, life-time service, can help skin toxin expelling, improving water flood, and with rear lubricious and oiliness, oiliness sense is little.
Embodiment 8: a kind of natural skin care quintessence oil, each component and content (in mass fraction) thereof are: amygdalus pedunculata pall oil 90% ~ 98%; White oil 1% ~ 6%; All the other are alginic acid, are applicable to daily skin protection and use.
Embodiment 9: a kind of moisturizing hand cream, each component and content (in mass fraction) thereof are: amygdalus pedunculata pall oil 10% ~ 24%; Stearic acid 2% ~ 7%; Glycerol monostearate 1% ~ 3%; Lanoline 1% ~ 6%; Glycerol 4% ~ 8%; Vitamin E 0.1% ~ 1%; Essence is appropriate; All the other are deionized water.
Embodiment 10: a kind of facial milk cleanser, each component and content (in mass fraction) thereof are: amygdalus pedunculata pall oil 8% ~ 15%; Stearic acid 3% ~ 6%; Glycerol monostearate 7% ~ 13%; Hexadecanol-octadecanol (mixed alcohol) 3% ~ 9%; Glycerol 4% ~ 8%; Triethanolamine 1% ~ 2%; Camomile extract 1% ~ 2%; Preservative qs; Essence is appropriate; All the other are deionized water.
Embodiment 11: a kind of anti-ultraviolet skin protection water, each component and content (in mass fraction) thereof are: amygdalus pedunculata pall oil 4% ~ 8%; Sodium lactate 3% ~ 6%; Polyoxyethylene hardened castor oil 0.1% ~ 1%; Citric acid 1% ~ 2%; Sodium hydroxide 0.1% ~ 0.5%; Lanoline is appropriate, and essence is appropriate; Preservative qs; All the other are deionized water.
Embodiment 12: a kind of gentle emollient cream, each component and content thereof are (in mass fraction): amygdalus pedunculata pall oil 15% ~ 25%; Glycerol 3% ~ 6%; Lecithin 8% ~ 12%; Butyl myristate 5% ~ 9%; Essence is appropriate; Preservative qs; Aloe extract 1% ~ 5%, all the other are deionized water.
Embodiment 13: a kind of cream pack, each component and content thereof are (in mass fraction): glycerol 7% ~ 15%; Emulsified silicone oil 4% ~ 7%; Amygdalus pedunculata pall oil 5% ~ 13%; Sorbitol 2% ~ 4%; Kaolin 18% ~ 30%; Zinc oxide 2% ~ 3%; Chitin 1% ~ 3%; Lauryl alcohol 4% ~ 6%; Triethanolamine 0.1% ~ 1%; Preservative qs; Essence is appropriate; All the other are deionized water.
Embodiment 14: a kind of natural sun-prevention oil, each component and content thereof are (in mass fraction): amygdalus pedunculata pall oil 45% ~ 60%; Olive oil 15% ~ 23%; Liquid paraffin 5% ~ 15%; Essence is appropriate; All the other are salicylic acid peppermint ester.
Embodiment 15: a kind of moist type hair conditioner, each component and content thereof are (in mass fraction): amygdalus pedunculata pall oil 6% ~ 18%; Alkyl imidazoline 15% ~ 20%; Sodium alginate 1% ~ 2%; Glycerol 4% ~ 6%; Glyceryl monostearate 2% ~ 5%; Vitamin E 0.1% ~ 1%; Antiseptic 0.2% ~ 0.5%; Antioxidant 0.03% ~ 0.5%; Essence 0.3% ~ 0.5%; All the other are deionized water.
Embodiment 16: a kind of conditioning shampoo, each component and content thereof are (in mass fraction): amygdalus pedunculata pall oil 5% ~ 15%; Sodium laurylsulfate 3% ~ 8%; Cation guar gum 0.3% ~ 1%; Polyvinylpyrrolidone 0.5% ~ 1%; Citric acid 0.1% ~ 1%; Ethylene glycol bis stearate 0.2% ~ 1.5%; EDTA0.05% ~ 0.1%; Propylene glycol 0.1% ~ 1%; Preservative qs; Essence 0.2% ~ 1%; All the other are deionized water.
Embodiment 17: a kind of natural hair oil, each component and content thereof are (in mass fraction): amygdalus pedunculata pall oil 60% ~ 80%; Olive oil 10% ~ 20%; All the other are Oleum Gossypii semen; Essence is appropriate; Antioxidant is appropriate; Pigment is appropriate.
Experimental example 1: amygdalus pedunculata pall oil is to the moisturizing effect of skin
1. physical data
Ginseng survey personnel: dry 20 examples of hand skin, dry 20 examples of skin of face, dry 20 examples of body skin.
Sex: women 35 example, male 25 example.
Age: 15 years old ~ 20 years old, 10 examples; 20 years old ~ 25 years old, 10 examples; 25 years old ~ 30 years old, 10 examples; 30 years old ~ 35 years old, 10 examples; 35 years old ~ 40 years old, 10 examples; 40 years old ~ 45 years old, 10 examples.
Result of use: 1 grade of 41 example, 2 grade of 6 example, 3 grade of 3 example, 4 grade of 0 example.
Blank group, 30 examples, women 20 example, male 10 example.
2. life cycle and using method
Life cycle: surrounding is a cycle.
Using method: amygdalus pedunculata pall oil is evenly applied to hand, face and body skin, every day 2 times, each 1 time sooner or later.
3. effect criterion
Effect is divided into 4 grades
In 1 grade: 7 days, xerosis cutis is obviously improved, and improves more than 90%.
In 2 grades: 14 days, xerosis cutis improves, and improves 70% ~ 90%.
In 3 grades: 21 days, xerosis cutis makes moderate progress, and improves 30% ~ 70%.
In 4 grades: 28 days, xerosis cutis is improved very little, improves less than 30%.
4. result of use is in table 2
5. blank group observed result is in table 3
6. conclusion
Amygdalus pedunculata pall oil has moisturizing effect, has significant curative effect to hand, face and body skin are dry.Remained the bioactive ingredients of pure natural by the amygdalus pedunculata pall oil of low temperature pressing, be mainly unsaturated fatty acid, with human body lipid closely, thus ooze skin better, human body skin is also easy to absorb.Continue to use the cosmetics containing amygdalus pedunculata pall oil, dry skin will improve greatly, and skin can be more moist, smooth, flexible.
7. exemplary subject person
Experimenter one:
Zhang, women, 24 years old, university students, hand skin was dry, and with the amygdalus pedunculata pall oil every day of outer painting sooner or later, after using one week continuously, hand skin moistens smooth, conscious skin comfort.
Experimenter two:
Yan, women, 40 years old, accounting, often used computer office, the dry coarse tarnish of skin of face, and with the amygdalus pedunculata pall oil every day of outer painting sooner or later, after two weeks, the coarse situation of xerosis cutis is obviously improved, and continues use after two months, and face moistens fine and smooth glossy.
Experimenter three:
Deng, male, 33 years old, outdoor coach, worked for a long time out of doors, body skin is dry, desquamation, and with the amygdalus pedunculata pall oil every day of outer painting sooner or later, after using two weeks continuously, desquamation alleviates, subjective symptoms makes moderate progress, and after one month, skin smooth moistens comfortable, recovers normal.
Experimental example 2: the facial cream containing amygdalus pedunculata pall oil is to the moist effect of face
1. physical data
Ginseng survey personnel: dry desquamation 20 example of skin of face, wherein women 8 example, male 12 example, 18 ~ 45 years old age.
2. life cycle and using method
Life cycle: surrounding is a cycle.
Using method: the facial cream every day containing amygdalus pedunculata pall oil 2 times, each 1 time sooner or later, is evenly applied to face.
3. effect criterion
In 1 grade: 7 days, facial dry desquamation phenomenon disappears.
In 2 grades: 14 days, facial dry desquamation phenomenon improves, and improves more than 70%.
In 3 grades: 21 days, facial dry desquamation phenomenon makes moderate progress, and improves 30% ~ 70%.
In 4 grades: 28 days, facial dry desquamation phenomenon is improved very little, improves less than 30%.
4. result
1 grade of 13 example, 2 grade of 4 example, 3 grade of 3 example, 4 grade of 0 example, how working after one week in use, skin of face moistens glossy, without any untoward reaction.
5. conclusion
Product of the present invention has moisturizing effect, has good curative effect to facial xerosis cutis desquamation.
Experimental example 3: amygdalus pedunculata pall oil compares with the uvioresistant effect of olive oil
1. analytical method
(1) amygdalus pedunculata pall oil, the appropriate cyclohexane extraction of olive oil are quantitatively diluted;
(2) wave spectrum collection of illustrative plates-ultraviolet spectrophotometer (Japanese Shimadzu SHIMADZU UV-2550) is adopted to analyze;
(3) absorbing wavelength selects 200 ~ 400nm.
2. conclusion
As shown in Figure 4, amygdalus pedunculata pall oil maximum absorption wavelength appears at 212nm place to experimental result, and olive oil maximum absorption wavelength appears at 208nm place, can illustrate that amygdalus pedunculata pall oil and olive oil have and absorb ultraviolet characteristic.And with the absorbance of the amygdalus pedunculata pall oil of concentration than the height of olive oil, further illustrating amygdalus pedunculata pall oil has the ultraviolet characteristic of stronger absorption, can better protect skin from ultraviolet invasion.
Experimental example 4: the action effect of the facial milk cleanser containing amygdalus pedunculata pall oil
1. object of study: general skin quality person 50 example.
2. using method: with the clean face of product of the present invention, early, evening is each once, uses 4 weeks continuously.
3. experimental result: feel comfortable person 44 example, sensation general person 6 example.
Experimental example 5: amygdalus pedunculata pall oil is as the action effect of cleansing cosmetic
Evaluate that amygdalus pedunculata pall oil comes off as the outward appearance of cleansing cosmetic, character, cosmetics, washability and combination property.
1. analytical method
(1) outward appearance
◇: transparent
Zero: translucent
(2) character
◇: aqueous
×: non-aqueous
(3) cosmetics come off
The dropping situations of lipstick: be coated on forearm by lipstick (Maybelline system), diameter is about 2cm, after leaving standstill drying in 2 hours, acts on about 2mL amygdalus pedunculata pall oil, and gently rubs massage with finger.Then use running water, observe the residual condition of lipstick, criterion is as follows.
The dropping situations of mascara: be coated on forearm by mascara (card appearance orchid system), diameter is about 2cm, after leaving standstill drying in 2 hours, acts on about 2mL amygdalus pedunculata pall oil, and gently rubs massage with finger.Then use running water, observe the residual condition of lipstick, criterion is as follows.
◇: the cosmetics situation that comes off is good
Zero: the cosmetics situation that comes off is general
△: the cosmetics situation that comes off is slightly poor
×: cosmetics come off situation difference
(4) washability
Amygdalus pedunculata pall oil is about about 2g and is applied in fore-arm, easy washability during evaluation warm water washing.
◇: easily rinse, without greasy feeling
Zero: easily rinse
△: difficult flushing
×: can not rinse, skin have oil residual
(5) combination property
By 20 cosmetics experts, the result of use of amygdalus pedunculata pall oil as makeup remover is evaluated.Lipstick and mascara are coated in face respectively, after dry 2 hours, get about 2g amygdalus pedunculata pall oil in moistening but not containing the palm of the globule, then act on face, softly massage, make amygdalus pedunculata pall oil spreadable in whole face, then use warm water washing.Evaluate amygdalus pedunculata pall oil as the cosmetics dropping situations of makeup remover, washability and comfort level.
In ◇: 20 people, 18 people and above answer are well
In zero: 20 people, 14 ~ 16 people answer
In △: 20 people, 9 ~ 11 people answer
×: in 20 people, 5 people and following answer are well
2. conclusion
Amygdalus pedunculata pall oil is as the action effect of cleansing cosmetic in table 4, and known by table 4, product makeup removing effect of the present invention is better, not only can improve skin clean degree, while using, also can be reached the object of skin protection by continuous massaging skin.
Claims (1)
1. amygdalus pedunculata pall oil is preparing the application in suntan lotion, it is characterized in that: in described amygdalus pedunculata pall oil, the mass percentage of unsaturated fatty acid is 96% ~ 98%, content of vitamin E is 40 ~ 120 mg/100g, relative density is 0.900 ~ 0.960, saponification number is 185 ~ 193, and iodine number is 106 ~ 120;
Above-mentioned amygdalus pedunculata pall oil adopts low-temperature cold pressing preparation, and preparation process is:
(1) Prunus pedunculata Maxim. kernel is through decortication, remove impurity, drying;
(2) Prunus pedunculata Maxim. kernel carries out squeezing and gets oil, and feeding temperature is no more than 35 DEG C, and oil outlet temperature is no more than 50 DEG C;
(3) oils and fats after squeezing is through precipitating, filtering and obtain amygdalus pedunculata pall oil.
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141224 |