CN103015232B - Method for preparing color Setaria viridis - Google Patents
Method for preparing color Setaria viridis Download PDFInfo
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- CN103015232B CN103015232B CN201310012118.1A CN201310012118A CN103015232B CN 103015232 B CN103015232 B CN 103015232B CN 201310012118 A CN201310012118 A CN 201310012118A CN 103015232 B CN103015232 B CN 103015232B
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Abstract
The invention discloses a method for preparing color Setaria viridis. The method comprises the following steps of: primarily soaking and drying greig, spilling and drying the greig, secondarily soaking and drying the greig, boiling silk, blackening, sand washing, dying plant dye, dying reactive dyes, dying acid dye and softening and treating. The color Setaria viridis prepared by using the method has both the wearability same as that of gambiered Guangdong silk and is in different colors, so that the defect that the gambiered Guangdong silk fabric is single in color is overcome; and the color Setaria viridis prepared by using the method is not only high in color fastness but also is bright in color, so that the gambiered Guangdong silk fabric has greater development prospect in application in clothes.
Description
Technical field
The present invention relates to textile material technical field, particularly relate to a kind of method preparing color Liang.
Background technology
Gambiered Guangdong silk also known as gambiered Guangdong gauze, the weaving face fabric of be that to take Real Silk Habotai as end base through natural dye yam juice the contaminate front gloss black that formed with the mineral instrumentality in mud again after Exposure to Sunlight and the sub-light coffee color of reverse side.Be used as the dye yam of dyestuff, its main component is be easy to polyphenol and the tannin (tannin matter) that oxidative deformation produces freezing action, and itself can do Chinese herbal medicine.With gambiered Guangdong silk that dye yam is dyed there is nice and cool, sweat proof, easily wash, sun-proof, the wearability such as antibacterial.But the color of gambiered Guangdong silk is more single, only have the coffee-like dichromatism of the black in front and reverse side, this makes the application of gambiered Guangdong silk in design and on clothes have great limitation.
Summary of the invention
The object of the invention is to the defect for overcoming prior art, and provide a kind of and prepare the method that the wearability both with gambiered Guangdong silk has the color Liang of different colours.
For achieving the above object, the present invention is by the following technical solutions: a kind of method preparing color Liang, comprises the following steps:
(1) just greig is shone in leaching: be that 1:1-3 formulated the first dye yam immersion steep greig 10-14h with dye yam fruit and the mass ratio of water, is then dewatered and is laid on meadow and be exposed to the sun to doing; First dye yam liquid preferably uses dye yam fruit with the mass ratio of water for 1:2 is formulated, the time preferred 12h that greig soaks;
(2) spill solarization greig: be that formulated the second dye yam liquid of 3-4:200 is evenly spread across on the greig that processes through step (1) with dye yam fruit and the mass ratio of water, to be then laid on meadow and to be exposed to the sun to dry; Repeat to spill and shine greig 5-7 time; Second dye yam liquid preferably uses dye yam fruit with the mass ratio of water for 3:200 is formulated, repeats to spill the number of times preferably 6 times shining greig;
(3) greig is shone in secondary leaching: be after 2-3:100 formulated the 3rd dye yam immersion steep greig 1-5 minute that processes through step (2) with dye yam fruit and the mass ratio of water, takes out and is exposed to the sun to doing; Repeat time leaching and shine greig 5-7 time; 3rd dye yam liquid preferably uses dye yam fruit with the mass ratio of water for 2:100 is formulated, repeats the number of times preferably 6 times that greig is shone in time leaching;
(4) boil silk fabric: the greig adding the 3rd dye yam liquid and process through step (3) in saucepan, turn in 45-50 DEG C and boil 4-5min, then dewater and dry; Described saucepan preferably copper pot;
(5) repeat time leaching and shine greig 12 times, then repeat to boil silk fabric once, and then repetition time leaching shines greig once;
(6) excessively black: the river silt containing ferric ion is applied on a surface of second order of the greig processed through step (5), and before sunrise, greig is laid on 30min on meadow, then the river silt on it is cleaned up and be refitted on meadow and dry with the sunlight in 3h after sunrise, then with the 3rd dye yam immersion bubble 1h, then 40min on the meadow being laid on post sunset;
(7) sand washing: the greig processed through step (6) being placed in sand washing consistent lubricant content is that the water of 5-15g/L soaks 30-60min, then adding sand washing powder wherein makes the content of sand washing powder in solution be 5-20g/L, at room temperature sand washing 30-90min, then with being cleaned up by greig after weak acid neutralization solution and dewatering; Described weak acid preferable formic acid or acetic acid; The preferred 10g/L of content of sand washing consistent lubricant, the preferred 15g/L of content of sand washing powder, sand washing time preferred 60min;
(8) vegetable colour contaminates: be added to the water by vegetable colour with through the greig that step (7) processes, room temperature is warming up to 90 DEG C after entering to contaminate 10min and is incubated 40min, and then wash with water clean; The mass ratio of greig and vegetable colour is 100:1.5-2.5, and bath raio is 1:18-22;
(9) REACTIVE DYES contaminates: by REACTIVE DYES, levelling agent with put into water through the greig that step (8) processes and be heated to 60 DEG C, insulation 30min, the mass ratio of greig, REACTIVE DYES and levelling agent is 100:1.5-2.5:0.2, and bath raio is 1:18-22; Then in solution, add glauber salt makes the content of glauber salt in solution be 50-90g/L, and wherein glauber salt is divided into three parts, adds portion every 15min; Then in solution, add sodium carbonate makes the content of sodium carbonate in solution be clean greig with water after 18-22g/L, 45min; The mass ratio of greig, REACTIVE DYES and levelling agent is preferably 100:2:0.2, the preferred 70g/L of content of glauber salt;
(10) ACID DYES contaminates: be added to the water by ACID DYES with through the greig that step (9) processes, room temperature adds sodium sulphate after entering to contaminate 10min, in 45min, temperature from ambient is risen to 90 DEG C and is incubated 40min, cleaning with water, then add color-fixing agent, and then wash with water clean and dry; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent is 100:1.5-2.5:2-5:1-2, and bath raio is 1:18-22; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent is preferably 100:2:3:2;
(11) sofening treatment: be added to the water by softener with through the greig that step (10) is processed, soak 1-3 hour at 45-50 DEG C, then cleaning, drying; In water, the content of softener is 5-20g/L, and bath raio is 1:18-22; The preferred 15g/L of content of softener.
Dewater described in above-mentioned steps preferred natural-dehydration.
Compared with prior art, the invention has the beneficial effects as follows: color Liang prepared by application the present invention had both had the wearability identical with gambiered Guangdong silk, can have again various different color simultaneously, compensate for the shortcoming that gambiered Guangdong silk fabric shade is single; Color Liang prepared by the present invention not only COLOR FASTNESS is high but also bright in colour, makes the application of gambiered Guangdong silk fabric on clothes have larger development prospect.
Detailed description of the invention
In order to more fully understand technology contents of the present invention, below in conjunction with specific embodiment technical scheme of the present invention being introduced further and illustrating.
Embodiment
The preparation method of a kind of color Liang comprises the following steps:
(1) just greig is shone in leaching: be that formulated the first dye yam liquid of 1:2 (mass ratio of dye yam fruit and water can in the scope of 1:1-3 in other embodiments) soaks greig 12h with dye yam fruit and the mass ratio of water, soak time can be 10-14h in other embodiments, then its natural-dehydration is laid on and meadow is exposed to the sun to dry.
(2) solarization greig is spilt: be that (dye yam fruit can in the scope of 3-4:200 with the mass ratio of water in other embodiments for formulated the second dye yam liquid of 3:200 with dye yam fruit and the mass ratio of water, do not affect effect of the present invention) be evenly spread across on the greig that processes through step (1), to be then laid on meadow and to be exposed to the sun to dry; Repeat to spill and shine greig 6 times, repeating to spill the number of times shining greig in other embodiments can for 5-7 time.
(3) greig is shone in secondary leaching: be that (dye yam fruit can in the scope of 2-3:100 with the mass ratio of water in other embodiments for formulated the 3rd dye yam liquid of 2:100 with dye yam fruit and the mass ratio of water, do not affect effect of the present invention) soak greig 1-5 minute that processes through step (2) after, take out and be exposed to the sun to dry; Repeat secondary leaching and shine greig 6 times, repeating time number of times of leaching solarization greig in other embodiments can be 5-7 time.
(4) boil silk fabric: the greig adding the 3rd dye yam liquid and process through step (3) in copper pot, turn in 45 DEG C and boil 4min, then natural-dehydration drying; Can prevent the intertwined point of greig from blocking by boiling silk fabric.
(5) repeat time leaching and shine greig 12 times, then repeat to boil silk fabric once, and then repetition time leaching shines greig once.
(6) excessively black: the river silt containing ferric ion is applied on a surface of second order of the greig processed through step (5), and before sunrise, greig is laid in 30min on meadow, then the river silt on it is cleaned up and be refitted on meadow and dry with the sunlight in 3h after sunrise, then with the 3rd dye yam immersion bubble 1h, then 40min on the meadow being laid on post sunset.
(7) sand washing: the greig processed through step (6) being placed in sand washing consistent lubricant content is that the water of 10g/L soaks 50min, then adding sand washing powder wherein makes the content of sand washing powder in solution be 15g/L, at room temperature sand washing 60min, then with being cleaned up by greig after formic acid or acetic acid neutralization solution and natural-dehydration, other weak acid neutralization solution can be used in other embodiments; The content of sand washing consistent lubricant can be 5-15g/L in other embodiments, and the content of sand washing powder can be 5-20g/L, and the sand washing time can be 30-90min.
(8) vegetable colour contaminates: be added to the water by vegetable colour with through the greig that step (7) processes, room temperature is warming up to 90 DEG C after entering to contaminate 10min and is incubated 40min, and then wash with water clean; The mass ratio of greig and vegetable colour is 100:2, and bath raio is 1:20; In other embodiments, the mass ratio of greig and vegetable colour can be 100:1.5-2.5, and vegetable colour is Flos Carthami dyestuff (in other embodiments, visual required the going up of vegetable colour contaminates color and select, as Radix Isatidis and bush etc.).
(9) REACTIVE DYES contaminates: by REACTIVE DYES, levelling agent with put into water through the greig that step (8) processes and be heated to 60 DEG C, insulation 30min, the mass ratio of greig, REACTIVE DYES and levelling agent is 100:2:0.2, and bath raio is 1:20; Then in solution, add glauber salt makes the content of glauber salt in solution be 75g/L, and wherein glauber salt is divided into three parts, adds portion every 15min; Then in solution, add sodium carbonate makes the content of sodium carbonate in solution be clean greig with water after 20g/L, 45min; In other embodiments, the mass ratio of greig, REACTIVE DYES and levelling agent can be 100:1.5-2.5:0.2, and the content of glauber salt can be 50-90g/L; REACTIVE DYES is BF type REACTIVE DYES, and levelling agent is polyoxyethylene ether; Levelling agent is that silvalin, line or fabric are in dyeing course, for impelling even dyeing, do not produce the fault such as vitta, color spot and the material added, dyestuff and levelling agent first generate certain " complex " in dye bath, in dyeing course, disengage dyestuff gradually and reach the effect of level dyeing, the material belonging to this type of has some nonionic surface active agent, as the polyoxyethylene ether etc. of fatty alcohol or alkyl phenol.
(10) ACID DYES contaminates: be added to the water by ACID DYES with through the greig that step (9) processes, room temperature adds sodium sulphate after entering to contaminate 10min, in 45min, temperature from ambient is risen to 90 DEG C and is incubated 40min, cleaning with water, then add color-fixing agent, and then wash with water clean and dry; The mass ratio of greig, azo dyes, sodium sulphate and color-fixing agent is 100:2:3:2, and bath raio is 1:20; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent can be 100:1.5-2.5:2-5:1-2 in other embodiments; ACID DYES is sulfonate sodium dyestuff (in other embodiments, also ACID DYES made by available anthraquinone dye or kiton colors, do not affect effect of the present invention), and color-fixing agent is dicyandiamide formaldehyde resin.
(11) sofening treatment: be added to the water by softener with through the greig that step (10) is processed, soaks 2 hours, then cleaning, drying at 45 DEG C; In water, the content of softener is 15g/L, and bath raio is 1:20; The content of softener can be 5-20g/L in other embodiments; Softener is block polyether.
The above only further illustrates technology contents of the present invention with embodiment, so that reader is easier to understand, but does not represent embodiments of the present invention and is only limitted to this, and any technology done according to the present invention extends or recreation, all by protection of the present invention.
Claims (4)
1. prepare a method of color Liang, it is characterized in that comprising the following steps:
(1) just greig is shone in leaching: be that 1:1-3 formulated the first dye yam immersion steep greig 10-14h with dye yam fruit and the mass ratio of water, is then dewatered and is laid on meadow and be exposed to the sun to doing;
(2) spill solarization greig: be that formulated the second dye yam liquid of 3-4:200 evenly spills on the greig processed through step (1) with dye yam fruit and the mass ratio of water, to be then laid on meadow and to be exposed to the sun to dry; Repeat to spill and shine greig 5-7 time;
(3) greig is shone in secondary leaching: be after 2-3:100 formulated the 3rd dye yam immersion steep greig 1-5 minute that processes through step (2) with dye yam fruit and the mass ratio of water, takes out and is exposed to the sun to doing; Repeat time leaching and shine greig 5-7 time;
(4) boil silk fabric: the greig adding the 3rd dye yam liquid and process through step (3) in saucepan, turn in 45-50 DEG C and boil 4-5min, then dewater and dry;
(5) repeat time leaching and shine greig 12 times, then repeat to boil silk fabric once, and then repetition time leaching shines greig once;
(6) excessively black: the river silt containing ferric ion is applied on a surface of second order of the greig processed through step (5), and before sunrise, greig is laid on 30min on meadow, then the river silt on it is cleaned up and be refitted on meadow and dry with the sunlight in 3h after sunrise, then with the 3rd dye yam immersion bubble 1h, then 40min on the meadow being laid on post sunset;
(7) sand washing: the greig processed through step (6) is placed in sand washing consistent lubricant content be 5-15g/L water soak 1 hour, then adding sand washing powder wherein makes the content of sand washing powder in solution be 5-20g/L, at room temperature sand washing 30-90min, then with being cleaned up by greig after weak acid neutralization solution and dewatering;
(8) vegetable colour contaminates: be added to the water by vegetable colour with through the greig that step (7) processes, room temperature is warming up to 90 DEG C after entering to contaminate 10min and is incubated 40min, and then wash with water clean; The mass ratio of greig and vegetable colour is 100:1.5-2.5, and bath raio is 1:18-22;
(9) REACTIVE DYES contaminates: by REACTIVE DYES, levelling agent with put into water through the greig that step (8) processes and be heated to 60 DEG C, insulation 30min, the mass ratio of greig, REACTIVE DYES and levelling agent is 100:1.5-2.5:0.2, and bath raio is 1:18-22; Then in solution, add glauber salt makes the content of glauber salt in solution be 50-90g/L, and wherein glauber salt is divided into three parts, adds portion every 15min; Then in solution, add sodium carbonate makes the content of sodium carbonate in solution be clean greig with water after 18-22g/L, 45min;
(10) ACID DYES contaminates: be added to the water by ACID DYES with through the greig that step (9) processes, room temperature adds sodium sulphate after entering to contaminate 10min, in 45min, temperature from ambient risen to 90 DEG C and be incubated 40min, clean with water, then add color-fixing agent, and then wash with water clean and dry; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent is 100:1.5-2.5:2-5:1-2, and bath raio is 1:18-22;
(11) sofening treatment: be added to the water by softener with through the greig that step (10) is processed, soak 1-3 hour at 45-50 DEG C, then cleaning, drying; In water, the content of softener is 5-20g/L, and bath raio is 1:18-22.
2. a kind of method preparing color Liang according to claim 1, it is characterized in that, described dehydration is natural-dehydration.
3. a kind of method preparing color Liang according to claim 1, it is characterized in that, the saucepan in described step (4) is copper pot.
4. a kind of method preparing color Liang according to claim 1, it is characterized in that, the weak acid in described step (7) is formic acid or acetic acid.
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| CN201310012118.1A CN103015232B (en) | 2013-01-14 | 2013-01-14 | Method for preparing color Setaria viridis |
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| CN201310012118.1A CN103015232B (en) | 2013-01-14 | 2013-01-14 | Method for preparing color Setaria viridis |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103950349A (en) * | 2014-05-08 | 2014-07-30 | 何炽斌 | Method to draw on gambiered Guangdong gauze |
| CN106149405B (en) * | 2015-04-17 | 2018-06-15 | 深圳市梁子时装实业有限公司 | A kind of preparation method of coloured silk Liang and products thereof and application |
| CN108914559A (en) * | 2018-09-18 | 2018-11-30 | 昆明滇艺非物质文化遗产研发有限公司 | A kind of production method of refrigerant gambiered Guangdong gauze |
| CN110130123A (en) * | 2019-04-20 | 2019-08-16 | 深圳市易菲妮时装有限公司 | The preparation process of high-performance antimildew and antibacterial gelsemium cotton |
| CN112458757B (en) * | 2020-11-25 | 2022-05-13 | 浙江喜得宝丝绸科技有限公司 | Printing and dyeing method of gambiered canton |
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| CN100575595C (en) * | 2008-05-13 | 2009-12-30 | 杭州喜得宝集团有限公司 | Wash-free dyeing method for silk |
| CN102061631A (en) * | 2009-11-12 | 2011-05-18 | 上海甲秀工业设计有限公司 | Modern gambiered Canton gauze product processing and manufacturing method |
| CN102312374B (en) * | 2011-03-17 | 2013-07-03 | 苏州金科达纺织科技股份有限公司 | Dyeing method of interwoven fabric made of cuprammonium fibers and tencels |
| CN102733182B (en) * | 2012-07-11 | 2014-04-09 | 周晓刚 | Process for producing double-sided gambiered Guangdong silk |
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