CN102992891B - Zirconia-carried mulberry fertilizer and preparation method thereof - Google Patents
Zirconia-carried mulberry fertilizer and preparation method thereof Download PDFInfo
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- CN102992891B CN102992891B CN201210452399.8A CN201210452399A CN102992891B CN 102992891 B CN102992891 B CN 102992891B CN 201210452399 A CN201210452399 A CN 201210452399A CN 102992891 B CN102992891 B CN 102992891B
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Abstract
The invention discloses a zirconia-carried mulberry fertilizer and a preparation method thereof. The zirconia-carried mulberry fertilizer comprises the following raw materials in parts by weight: 33-35 parts of inorganic fertilizer, 22-25 parts of shrimp shell, 14-16 parts of zeolite powder, 2-3 parts of calcium bicarbonate, 0.1-0.3 part of ammonium molybdate, 0.7-0.9 part of silicate potash fertilizer, 1.2-1.4 parts of calcium superphosphate, 1.3-2.0 parts of humic acid, 1.6-2.3 parts of trace element fertilizer, 7-9 parts of modified vermiculite powder, 2-3 parts of zirconia, 0.5-0.7 part of sodium dodecyl benzene sulfonate, 0.8-1.0 part of glyceryl monostearate, 1-3 parts of vinyl acetate-acrylate latex, 2-3 parts of oxalic acid, 5-7 parts of tung oil, 1.5-2.5 parts of dimethylbenzene and 8-10 parts of sepiolite powder. The fertilizer uses the inorganic fertilizer, shrimp shell and zeolite powder as the raw materials, and mulberry trees have developed root systems and long economic life, grow vigorously, and are easily planted and managed, so that water loss and soil erosion are reduced, the construction quality of biological environments is improved, and meanwhile, the raw materials include the modified vermiculite powder and zirconia as the filler, not only the absorption structures are increased, but also agglomeration is prevented and the disperstiveness is increased; and the zirconia-carried mulberry fertilizer and the preparation method thereof are beneficial for effective release of the fertilizer effect and the full absorption by plants.
Description
Technical field
The present invention relates to the required fertilizer of a plant growth, be specifically related to Mulberry fertilizer of a kind of loaded zirconia and preparation method thereof.
Background technology
Silkworm and mulberry are traditional rural industries of China, are divided into two large classes, the one, plant mulberry, and the 2nd, breed silkworms.The mulberry leaf that mulberry tree produces number and quality, the quality and quantity that directly impact is bred silkworms.In traditional managing of mulberry field, do not apply fertilizer or execute farm manure and a small amount of simple substance fertilizer, the mulberry leaf of mulberry tree output are in output and all can not meet qualitatively the needs of supporting mulberry, become one of important factor of restriction sericulture there development.Research shows, nitrogen is too much, and mulberry leaf are soft, are generally bad mulberry; When phosphorus, potassium deficiency, this tendency is more obvious; Once phosphorus lacks, the nitrogen component in mulberry leaf and sugar degree are obviously influenced, especially make free smart nitronic acid abnormal accumulation, after silkworm is edible, there will be death; If potassium lacks, photosynthesis is suppressed, the resistivity of disease is weakened, but the excessive balance that easily causes Mg/K in mulberry leaf easily causes magnesium deficiency symptom, therefore, will supplement in right amount the content of nitrogen, phosphorus, potassium, improves the quality and quantity of mulberry leaf.
Summary of the invention
The object of the present invention is to provide Mulberry fertilizer of a kind of loaded zirconia and preparation method thereof, it is main raw material that fertilizer of the present invention be take mineral manure, shrimp shell and zeolite powder, mulberry tree well developed root system, grow vigorous, easily plant, manageability and the economical life long, reduced soil erosion, improve improvement of the ecological environment quality, in raw material of the present invention, added PERFORMANCE OF MODIFIED VERMICULITE powder and zirconium white as stopping composition simultaneously, increased adsorption structure, anti-caking, increases its dispersiveness simultaneously; The effective release, the crop that are conducive to fertilizer efficiency fully absorb.
The present invention adopts following technical scheme to achieve these goals:
The Mulberry fertilizer of loaded zirconia, the weight part of its constitutive material is: mineral manure 33-35, shrimp shell 22-25, zeolite powder 14-16, Calcium hydrogen carbonate 2-3, ammonium molybdate 0.1-0.3, silicate potash fertilizer 0.7-0.9, calcium superphosphate 1.2-1.4, humic acid 1.3-2.0, trace element fertilizer 1.6-2.3, PERFORMANCE OF MODIFIED VERMICULITE powder 7-9, zirconium white 2-3, Sodium dodecylbenzene sulfonate 0.5-0.7, stearic acid
monoglyceride0.8-1.0, acrylate and vinyl acetate emulsion 1-3, oxalic acid 2-3, tung oil 5-7, dimethylbenzene 1.5-2.5 and sepiolite powder 8-10.
The Mulberry fertilizer of loaded zirconia, the weight part of its constitutive material is: mineral manure 34, shrimp shell 24, zeolite powder 15, Calcium hydrogen carbonate 2.5, ammonium molybdate 0.2, silicate potash fertilizer 0.8, calcium superphosphate 1.3, humic acid 1.7, trace element fertilizer 2.0, PERFORMANCE OF MODIFIED VERMICULITE powder 8, zirconium white 2.5, Sodium dodecylbenzene sulfonate 0.6, stearic acid
monoglyceride0.9, acrylate and vinyl acetate emulsion 2, oxalic acid 2.5, tung oil 6, dimethylbenzene 2 and sepiolite powder 9.
The preparation method of the Mulberry fertilizer of loaded zirconia, comprises the following steps:
(1) by the weight part of constitutive material, take each raw material, mineral manure, shrimp shell, zeolite powder, PERFORMANCE OF MODIFIED VERMICULITE powder and zirconium white are added in stirrer, it is fully mixed;
(2) in step (1), by the weight part of constitutive material, add Calcium hydrogen carbonate, ammonium molybdate, silicate potash fertilizer, calcium superphosphate, humic acid, trace element fertilizer, Sodium dodecylbenzene sulfonate, stearic acid
monoglycerideand acrylate and vinyl acetate emulsion, mix, regulate the water content 37-45% of compound, with oxalic acid, regulate PH to 5.7-6.4;
(3) compound in step (2) is carried out to just fermentation, fermentation 3-5 days, leavening temperature is controlled at 55-65 ℃;
(4) whipping step (3) solution, then carries out Secondary Fermentation, fermentation 9-11 days, and leavening temperature is controlled at 63-68 ℃;
(5) by the weight part of constitutive material, tung oil, dimethylbenzene and sepiolite powder are mixed, then carry out the fermented product coating of step (4) and process, last granulation obtains Mulberry fertilizer.
The preparation method of described PERFORMANCE OF MODIFIED VERMICULITE powder is by vermiculite scaling loss 3-4 hour at temperature 680-850 ℃, rear grind into powder, admix that to be equivalent to the Di(dioctylpyrophosphato) ethylene titanate agitating of powder weight 2-4% even, dry, be ground into powder.
Beneficial effect of the present invention:
It is main raw material that fertilizer of the present invention be take mineral manure, shrimp shell and zeolite powder, mulberry tree well developed root system, grow vigorous, easily plant, manageability and the economical life long, reduced soil erosion, improved improvement of the ecological environment quality, PERFORMANCE OF MODIFIED VERMICULITE powder and zirconium white in raw material of the present invention, have been added as stopping composition simultaneously, increased adsorption structure, anti-caking, increases its dispersiveness simultaneously; The effective release, the crop that are conducive to fertilizer efficiency fully absorb.
Embodiment
Embodiment 1: the Mulberry fertilizer of loaded zirconia, the weight part of its constitutive material is: mineral manure 34, shrimp shell 24, zeolite powder 15, Calcium hydrogen carbonate 2.5, ammonium molybdate 0.2, silicate potash fertilizer 0.8, calcium superphosphate 1.3, humic acid 1.7, trace element fertilizer 2.0, PERFORMANCE OF MODIFIED VERMICULITE powder 8, zirconium white 2.5, Sodium dodecylbenzene sulfonate 0.6, stearic acid
monoglyceride0.9, acrylate and vinyl acetate emulsion 2, oxalic acid 2.5, tung oil 6, dimethylbenzene 2 and sepiolite powder 9.
The preparation method of the Mulberry fertilizer of loaded zirconia, comprises the following steps:
(1) by the weight part of constitutive material, take each raw material, mineral manure, shrimp shell, zeolite powder, PERFORMANCE OF MODIFIED VERMICULITE powder and zirconium white are added in stirrer, it is fully mixed;
(2) in step (1), by the weight part of constitutive material, add Calcium hydrogen carbonate, ammonium molybdate, silicate potash fertilizer, calcium superphosphate, humic acid, trace element fertilizer, Sodium dodecylbenzene sulfonate, stearic acid
monoglycerideand acrylate and vinyl acetate emulsion, mix, regulate the water content 37-45% of compound, with oxalic acid, regulate PH to 5.7-6.4;
(3) compound in step (2) is carried out to just fermentation, fermentation 3-5 days, leavening temperature is controlled at 55-65 ℃;
(4) whipping step (3) solution, then carries out Secondary Fermentation, fermentation 9-11 days, and leavening temperature is controlled at 63-68 ℃;
(5) by the weight part of constitutive material, tung oil, dimethylbenzene and sepiolite powder are mixed, then carry out the fermented product coating of step (4) and process, last granulation obtains Mulberry fertilizer.
The preparation method of described PERFORMANCE OF MODIFIED VERMICULITE powder is by vermiculite scaling loss 3-4 hour at temperature 680-850 ℃, rear grind into powder, admix that to be equivalent to the Di(dioctylpyrophosphato) ethylene titanate agitating of powder weight 2-4% even, dry, be ground into powder.
Use the fertilizer efficiency of the above-mentioned Mulberry fertilizer making to use result:
Claims (2)
1. a Mulberry fertilizer for loaded zirconia, is characterized in that the weight part of its constitutive material is: mineral manure 33-35, shrimp shell 22-25, zeolite powder 14-16, Calcium hydrogen carbonate 2-3, ammonium molybdate 0.1-0.3, silicate potash fertilizer 0.7-0.9, calcium superphosphate 1.2-1.4, humic acid 1.3-2.0, trace element fertilizer 1.6-2.3, PERFORMANCE OF MODIFIED VERMICULITE powder 7-9, zirconium white 2-3, Sodium dodecylbenzene sulfonate 0.5-0.7, stearic acid monoglyceride 0.8-1.0, acrylate and vinyl acetate emulsion 1-3, oxalic acid 2-3, tung oil 5-7, dimethylbenzene 1.5-2.5 and sepiolite powder 8-10;
The preparation method of described PERFORMANCE OF MODIFIED VERMICULITE powder is by vermiculite scaling loss 3-4 hour at temperature 680-850 ℃, rear grind into powder, admix that to be equivalent to the Di(dioctylpyrophosphato) ethylene titanate agitating of powder weight 2-4% even, dry, be ground into powder;
The preparation method of the Mulberry fertilizer of described loaded zirconia, comprises the following steps:
(1) by the weight part of constitutive material, take each raw material, mineral manure, shrimp shell, zeolite powder, PERFORMANCE OF MODIFIED VERMICULITE powder and zirconium white are added in stirrer, it is fully mixed;
(2) in step (1), by the weight part of constitutive material, add Calcium hydrogen carbonate, ammonium molybdate, silicate potash fertilizer, calcium superphosphate, humic acid, trace element fertilizer, Sodium dodecylbenzene sulfonate, stearic acid monoglyceride and acrylate and vinyl acetate emulsion, mix, regulate the water content 37-45% of compound, with careless acid for adjusting pH to 5.7-6.4;
(3) compound in step (2) is carried out to just fermentation, fermentation 3-5 days, leavening temperature is controlled at 55-65 ℃;
(4) whipping step (3) solution, then carries out Secondary Fermentation, fermentation 9-11 days, and leavening temperature is controlled at 63-68 ℃;
(5) by the weight part of constitutive material, tung oil, dimethylbenzene and sepiolite powder are mixed, then carry out the fermented product coating of step (4) and process, last granulation obtains Mulberry fertilizer.
2. the Mulberry fertilizer of loaded zirconia according to claim 1, is characterized in that the weight part of its constitutive material is: mineral manure 34, shrimp shell 24, zeolite powder 15, Calcium hydrogen carbonate 2.5, ammonium molybdate 0.2, silicate potash fertilizer 0.8, calcium superphosphate 1.3, humic acid 1.7, trace element fertilizer 2.0, PERFORMANCE OF MODIFIED VERMICULITE powder 8, zirconium white 2.5, Sodium dodecylbenzene sulfonate 0.6, stearic acid monoglyceride 0.9, acrylate and vinyl acetate emulsion 2, oxalic acid 2.5, tung oil 6, dimethylbenzene 2 and sepiolite powder 9.
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CN103724118A (en) * | 2013-12-20 | 2014-04-16 | 当涂县科辉商贸有限公司 | Mulberry compound fertilizer and preparation method thereof |
CN103980057B (en) * | 2014-05-31 | 2015-10-07 | 重庆市中绿农业开发有限责任公司 | Silkworm and mulberry tree organic-inorganic compound fertilizer special |
CN104557267A (en) * | 2014-12-18 | 2015-04-29 | 广西大学 | Synergistic sustained-release fertilizer for mulberry and preparation method thereof |
CN104829332A (en) * | 2015-04-22 | 2015-08-12 | 广德县菁菁果业专业合作社 | Mulberry tree cultivation special-purpose fertilizer |
CN106431776A (en) * | 2016-12-23 | 2017-02-22 | 李梦 | Special fertilizer for oilseed rapes and preparation method of special fertilizer |
CN107197708A (en) * | 2017-06-27 | 2017-09-26 | 安徽省瑞森生物科技有限责任公司 | A kind of preparation method of the composite modified sulfate organic nutrient soil of fermentation of seaweed |
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CN110511094A (en) * | 2019-10-09 | 2019-11-29 | 扬州大学 | A kind of rice composite Nano matrix fertilizer and preparation method thereof |
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JPS623721A (en) * | 1985-06-28 | 1987-01-09 | 有限会社 ジヤパンセラミツクス | Plant growth promoting article |
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SU711023A1 (en) * | 1976-12-07 | 1980-01-25 | Украинский научно-исследовательский институт огнеупоров | Method of powder granulation |
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Effective date of registration: 20170517 Address after: 226200, four villages, Xinzhuang Town, Qidong, Jiangsu, Nantong Patentee after: Qidong Qixiu Vegetable & Fruit professional cooperatives Address before: 231200, Jinniu street, Shannan town, Feixi County, Hefei, Anhui 22 Patentee before: Feixi Jinniu Silkworm and Mulberry Specialized Farmer Cooperatives |