CN102965867A - Degumming process of natural yellow silk fabrics - Google Patents

Degumming process of natural yellow silk fabrics Download PDF

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Publication number
CN102965867A
CN102965867A CN2012103788277A CN201210378827A CN102965867A CN 102965867 A CN102965867 A CN 102965867A CN 2012103788277 A CN2012103788277 A CN 2012103788277A CN 201210378827 A CN201210378827 A CN 201210378827A CN 102965867 A CN102965867 A CN 102965867A
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China
Prior art keywords
degumming
yellow silk
natural yellow
fabric
unstuck
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Pending
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CN2012103788277A
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Chinese (zh)
Inventor
刘双双
李艳清
张红霞
祝成炎
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High Fashion Silk (Zhejiang) Co., Ltd.
Zhejiang Sci Tech University ZSTU
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Zhejiang Sci Tech University ZSTU
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Priority to CN2012103788277A priority Critical patent/CN102965867A/en
Publication of CN102965867A publication Critical patent/CN102965867A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a degumming process of natural yellow silk fabrics. The degumming process comprises the following steps: 1) preparing a degumming reagent into a solution of which the concentration is 4-6g/L; 2) placing a natural yellow silk fabric into the solution prepared in the step 1), wherein the bath ratio is 1:100, heating to 80-85 DEG C, and degumming for 30-70 minutes. The degumming process is suitable for a degumming process of the natural yellow silk fabric; with the adoption of the degumming process, proper silk gum dissolve-loss ratio is obtained through controlling the factors such as the degumming time, the degumming temperature and the degumming reagent and the like, colors are retained to a large extent, and the problems that degumming is not uniform and colors are not uniform in the traditional degumming process are overcomesolved, so that not only is the gum-containing rate of the fabric is ensured, but also the natural color value of the fabric is retained to a large extent; and the degumming process of the natural yellow silk fabrics has the advantages of good degumming effect and, environmental protection friendliness,and short time and the like, and can be used for natural yellow silk fabrics of various tissues.

Description

A kind of degumming tech of natural yellow silk fabric
Technical field
The present invention relates to a kind of degumming tech of silk fabric, especially a kind of degumming tech of natural yellow silk fabric.
Background technology
The natural yellow silk fabric before use must be through coming unstuck, and in traditional yellow silk degumming tech, the impact of the factors such as reagent, temperature, concentration owing to come unstuck, being easy to generation comes unstuck irregular, the problems such as the color stream vector is large, have a strong impact on the natural colored of colorful silk fabric, thereby affect the quality of silk silk fabric, do not reach environmental requirement.This just needs a kind of degumming tech for the natural yellow silk fabric, makes the yellow silk fabric after coming unstuck both have suitable sericin degumming loss percentage, keeps substantially again its natural aberration.
The content of invention
The object of the present invention is to provide a kind of degumming tech of natural yellow silk fabric, by factors such as control usually time, the temperature of coming unstuck, the reagent that comes unstuck, obtaining suitable sericin degumming loss percentage, and maximization keeps color.
For achieving the above object, technical scheme of the present invention is:
A kind of degumming tech of natural yellow silk fabric may further comprise the steps: the reagent that 1) will come unstuck is mixed with the solution that concentration is 4-6 g/L; 2) solution that the natural yellow silk fabric is placed step 1) prepare, bath raio is 1: 100; Be warming up to 80-85 ℃, 30-70 min comes unstuck.
The reagent that comes unstuck in the described step 1) adopts a kind of in sodium bicarbonate, neutral soap, the sodium carbonate.
The described reagent that comes unstuck is sodium bicarbonate, and solution concentration is 4g/L, and bath raio is 1: 100, and the temperature of coming unstuck is 82 ℃, and usually time is 70min.
The invention has the beneficial effects as follows: the degumming tech of a kind of natural yellow silk fabric that the application of the invention provides, be applicable to the natural yellow silk fabric process of coming unstuck, by factors such as control usually time, the temperature of coming unstuck, the reagent that comes unstuck, obtaining suitable sericin degumming loss percentage, and maximization keeps color.The present invention has overcome tradition and has come unstuck and come unstuck irregular in the process and the problem such as unevenness of tint, both guaranteed the gum content of fabric, the natural colour value that has farthest kept again fabric, and the advantage such as have that degumming effect is good, environmental protection and time are short, and can be used for the natural yellow silk fabric of various tissues.
  
Description of drawings
Fig. 1 is the schematic diagram of the natural yellow silk fabric that uses of the present invention;
Fig. 2 is the relationship analysis figure of the present invention usually time, sericin degumming loss percentage and the aberration that use optimised process and obtain.
The specific embodiment
Embodiment 1
Use the Digieye colour photometer to select the CIELAB colour space, the yellow silk fabric is carried out colour examining, measure the color value L of the front fabric that comes unstuck *(lightness)=85.50, a *(green/red)=5.87, b *(indigo plant/Huang)=42.06; With sodium bicarbonate (NaHCO 3) be mixed with the solution that concentration is 4g/L; Then the natural yellow silk fabric is placed as shown in Figure 1 the solution of above-mentioned preparation, bath raio is 1: 100; Be warming up to 82 ℃, 70min comes unstuck.Re-use the Digieye colour photometer and select the CIELAB colour space, carry out colour examining after the yellow silk fabric is come unstuck, measure the color value L of the rear fabric that comes unstuck *(lightness)=73.76, a *(green/red)=3.94, b *(indigo plant/Huang)=31.55, selecting the CIEDE2000 colour difference formula to calculate aberration is 9.09, the sericin degumming loss percentage of natural yellow silk fabric is 22.7%.The total silk gum amount of this fabric is 28.8%, when sericin degumming loss percentage is 22.7%, can obtain preferably pliability.
  
The degumming tech of a kind of natural yellow silk fabric that present embodiment provides, be applicable to the natural yellow silk fabric process of coming unstuck, by factors such as control usually time, the temperature of coming unstuck, the reagent that comes unstuck, obtaining suitable sericin degumming loss percentage, and maximization keeps color.The present invention has overcome tradition and has come unstuck and come unstuck irregular in the process and the problem such as unevenness of tint, both guaranteed the gum content of fabric, the natural colour value that has farthest kept again fabric, and the advantage such as have that degumming effect is good, environmental protection and time are short, and can be used for the natural yellow silk fabric of various tissues.
   
Embodiment 2
Use the Digieye colour photometer to select the CIELAB colour space, the yellow silk fabric is carried out colour examining, measure the color value L of the front fabric that comes unstuck *(lightness)=85.50, a *(green/red)=5.87, b *(indigo plant/Huang)=42.06; Neutral soap is mixed with the solution that concentration is 5g/L; Then the natural yellow silk fabric is placed as shown in Figure 1 the solution of above-mentioned preparation, bath raio is 1: 100; Be warming up to 80 ℃, 50min comes unstuck.Re-use the Digieye colour photometer and select the CIELAB colour space, carry out colour examining after the yellow silk fabric is come unstuck, measure the color value L of the rear fabric that comes unstuck *(lightness)=73.50, a *(green/red)=4.20, b *(indigo plant/Huang)=32.00, selecting the CIEDE2000 colour difference formula to calculate aberration is 9.18, the sericin degumming loss percentage of natural yellow silk fabric is 23.2%.
  
The degumming tech of a kind of natural yellow silk fabric that present embodiment provides, be applicable to the natural yellow silk fabric process of coming unstuck, by factors such as control usually time, the temperature of coming unstuck, the reagent that comes unstuck, obtaining suitable sericin degumming loss percentage, and maximization keeps color.The present invention has overcome tradition and has come unstuck and come unstuck irregular in the process and the problem such as unevenness of tint, both guaranteed the gum content of fabric, the natural colour value that has farthest kept again fabric, and the advantage such as have that degumming effect is good, environmental protection and time are short, and can be used for the natural yellow silk fabric of various tissues.
Embodiment 3
Use the Digieye colour photometer to select the CIELAB colour space, the yellow silk fabric is carried out colour examining, measure the color value L of the front fabric that comes unstuck *(lightness)=85.50, a *(green/red)=5.87, b *(indigo plant/Huang)=42.06; Sodium carbonate is mixed with the solution that concentration is 6g/L; Then the natural yellow silk fabric is placed as shown in Figure 1 the solution of above-mentioned preparation, bath raio is 1: 100; Be warming up to 85 ℃, 30min comes unstuck.Re-use the Digieye colour photometer and select the CIELAB colour space, carry out colour examining after the yellow silk fabric is come unstuck, measure the color value L of the rear fabric that comes unstuck *(lightness)=74.20, a *(green/red)=3.90, b *(indigo plant/Huang)=30.50, selecting the CIEDE2000 colour difference formula to calculate aberration is 9.02, the sericin degumming loss percentage of natural yellow silk fabric is 22.0%
The degumming tech of a kind of natural yellow silk fabric that present embodiment provides, be applicable to the natural yellow silk fabric process of coming unstuck, by factors such as control usually time, the temperature of coming unstuck, the reagent that comes unstuck, obtaining suitable sericin degumming loss percentage, and maximization keeps color.The present invention has overcome tradition and has come unstuck and come unstuck irregular in the process and the problem such as unevenness of tint, both guaranteed the gum content of fabric, the natural colour value that has farthest kept again fabric, and the advantage such as have that degumming effect is good, environmental protection and time are short, and can be used for the natural yellow silk fabric of various tissues.
Embodiment 4
1) reagent that will come unstuck is mixed with the solution that concentration is 4-6 g/L; 2) solution that the natural yellow silk fabric is placed step 1) prepare, bath raio is 1: 100; Be warming up to 80-85 ℃, keep coming unstuck temperature, come unstuck reagent and solution concentration, bath raio is constant, change usually time, obtain different sericin degumming loss percentages and aberration, with usually time, sericin degumming loss percentage and aberration mapping analysis, the relationship analysis figure that obtains sees such as Fig. 2, can obtain optimal degumming rate and less aberration from figure, keeps substantially natural colour.
The degumming tech of a kind of natural yellow silk fabric that present embodiment provides, be applicable to the natural yellow silk fabric process of coming unstuck, by factors such as control usually time, the temperature of coming unstuck, the reagent that comes unstuck, obtaining suitable sericin degumming loss percentage, and maximization keeps color.The present invention has overcome tradition and has come unstuck and come unstuck irregular in the process and the problem such as unevenness of tint, both guaranteed the gum content of fabric, the natural colour value that has farthest kept again fabric, and the advantage such as have that degumming effect is good, environmental protection and time are short, and can be used for the natural yellow silk fabric of various tissues.
The computing formula of sericin degumming loss percentage is in above-described embodiment:
Figure DEST_PATH_IMAGE002
, G 1Oven-dry weight for the front yellow silk fabrics of coming unstuck; G 2Oven-dry weight for the rear yellow silk fabrics of coming unstuck.
  

Claims (3)

1. the degumming tech of a natural yellow silk fabric, it is characterized in that may further comprise the steps: the reagent that 1) will come unstuck is mixed with the solution that concentration is 4-6 g/L; 2) solution that the natural yellow silk fabric is placed step 1) prepare, bath raio is 1: 100; Be warming up to 80-85 ℃, 30-70 min comes unstuck.
2. the degumming tech of a kind of natural yellow silk fabric according to claim 1, the reagent that it is characterized in that coming unstuck in the described step 1) adopt a kind of in sodium bicarbonate, neutral soap, the sodium carbonate.
3. the degumming tech of a kind of natural yellow silk fabric according to claim 1 and 2 is characterized in that the described reagent that comes unstuck is sodium bicarbonate, and solution concentration is 4g/L, and bath raio is 1: 100, and the temperature of coming unstuck is 82 ℃, and usually time is 70min.
CN2012103788277A 2012-10-09 2012-10-09 Degumming process of natural yellow silk fabrics Pending CN102965867A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104195777A (en) * 2014-09-16 2014-12-10 南通那芙尔服饰有限公司 Method for increasing color concentration of degummed natural colored mulberry silk fabrics
CN104264234A (en) * 2014-09-03 2015-01-07 苏州印丝特纺织数码科技有限公司 Silk degumming method for protecting silk quality
CN107190333A (en) * 2017-07-15 2017-09-22 合肥市聚丰制丝有限责任公司 A kind of stripping method
CN108385383A (en) * 2018-02-07 2018-08-10 嘉兴市桑田新材料科技有限公司 A kind of silk is scouringed and bleaching degumming tech

Citations (5)

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Publication number Priority date Publication date Assignee Title
JPS591768A (en) * 1982-06-08 1984-01-07 ヘンケル・コマンデイトゲゼルシヤフト・アウフ・アクテイ−ン Chemicals and method of refining natural silk yarn
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CN1043261C (en) * 1989-04-10 1999-05-05 平尾银藏 Natrual silk fibres and method for refining fabrics made from such fibres
CN101979725A (en) * 2010-11-15 2011-02-23 横县桂华茧丝绸有限责任公司 Processing method for keeping color of color silks
CN102337599A (en) * 2010-07-21 2012-02-01 吴佑林 Silk cotton degumming method

Patent Citations (5)

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JPS591768A (en) * 1982-06-08 1984-01-07 ヘンケル・コマンデイトゲゼルシヤフト・アウフ・アクテイ−ン Chemicals and method of refining natural silk yarn
CN1043261C (en) * 1989-04-10 1999-05-05 平尾银藏 Natrual silk fibres and method for refining fabrics made from such fibres
CN1191905A (en) * 1998-04-09 1998-09-02 俞祥根 Silk fibre pretreating process and product
CN102337599A (en) * 2010-07-21 2012-02-01 吴佑林 Silk cotton degumming method
CN101979725A (en) * 2010-11-15 2011-02-23 横县桂华茧丝绸有限责任公司 Processing method for keeping color of color silks

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王勇等: "蚕丝脱胶工艺条件的探讨", 《聊城师院学报(自然科学版)》, vol. 12, no. 1, 31 January 1999 (1999-01-31) *
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104264234A (en) * 2014-09-03 2015-01-07 苏州印丝特纺织数码科技有限公司 Silk degumming method for protecting silk quality
CN104195777A (en) * 2014-09-16 2014-12-10 南通那芙尔服饰有限公司 Method for increasing color concentration of degummed natural colored mulberry silk fabrics
CN107190333A (en) * 2017-07-15 2017-09-22 合肥市聚丰制丝有限责任公司 A kind of stripping method
CN108385383A (en) * 2018-02-07 2018-08-10 嘉兴市桑田新材料科技有限公司 A kind of silk is scouringed and bleaching degumming tech

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