CN102964957A - Heat insulation and heat control coating material and preparation method thereof - Google Patents

Heat insulation and heat control coating material and preparation method thereof Download PDF

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Publication number
CN102964957A
CN102964957A CN2012105645418A CN201210564541A CN102964957A CN 102964957 A CN102964957 A CN 102964957A CN 2012105645418 A CN2012105645418 A CN 2012105645418A CN 201210564541 A CN201210564541 A CN 201210564541A CN 102964957 A CN102964957 A CN 102964957A
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China
Prior art keywords
heat insulation
heat
preparation
heat control
dimethylbenzene
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CN2012105645418A
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Chinese (zh)
Inventor
李光俊
孙运良
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QINGDAO XUANWEI COATING MATERIAL CO Ltd
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QINGDAO XUANWEI COATING MATERIAL CO Ltd
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Priority to CN2012105645418A priority Critical patent/CN102964957A/en
Publication of CN102964957A publication Critical patent/CN102964957A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a heat insulation and heat control coating material and a preparation method thereof. The heat insulation and heat control coating material is prepared from the following raw materials in percentage by weight: 50-60% of thermoplastic acrylic resin, 5-10% of nano level titanium dioxide, 5-10% of nano level barium sulfate, 5-10% of ceramic powder, 5-10% of vacuum glass microsphere, 1-2% of siloxane coupling agent, 0.2-1% of polytetrafluoroethylene wax, 0.1-0.5% of organosilicon defoaming agent and 5-10% of dimethylbenzene and butyl acetate mixture. The invention provides a heat insulation and heat control coating material which has high heat insulation effect and ultraviolet resistance, favorable anticorrosion capability, excellent weather resistance and high adhesive force, and a preparation method thereof.

Description

A kind of heat insulation and heat control coated material and preparation method thereof
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Technical field
The present invention relates to the coated material technical field, be specifically related to a kind of heat insulation and heat control coated material and preparation method thereof.
Background technology
During solar energy distributed, visible light and near-infrared band had accounted for most energy, account for respectively 44% and 51% of total energy, so energy-saving coatings is mainly by improving the purpose that the sunlight reflectivity of visible light and near-infrared band is reached cooling.The infrared external reflection heat insulating coat is a kind of novel functional type coating, near infrared light in the energy usable reflection sunlight, stop heat transfer from the source, effectively reduce coatingsurface and interior environment temperature, improve Working environment thereby reach, reduce the purpose of energy consumption, thereby be widely used in oil tank, gas-holder, oil transportation (gas) pipeline, oil gas transfer cart etc.
For example traditional oil tank, oil transportation (gas) pipeline, cooling use the brushing silver paint and use the spray water cooling, etching apparatus, waste energy, and service life of equipment are short, only has 1 year.The plant and instrument of same aircraft, factory etc. have reduced work-ing life or have reduced tolerance range, caused waste equally owing to being subject to thermal radiation or ir radiation.Lagging material of the prior art generally is the weighting material that has high-reflectivity by adding, makes the coating of its formation have high-reflectivity, reduces the surface temperature of object by reflection, produces heat-blocking action thereby further reduce internal temperature.Because the reflectivity of these lagging materials all can not reach 100%, therefore still can the coated Surface absorption of some heat that is not reflected, and inner in coating by the thermaltransmission mode savings, time one is long, the heat energy of savings is more and more, the coating temperature raises, and causes easily staining of coating, thereby affects effect of heat insulation.
Summary of the invention
For the deficiency that prior art exists, technical problem to be solved by this invention is, provide that a kind of effect of heat insulation is high, anti-uv-ray by force, antiseptic power preferably, and have heat insulation and heat control coated material of super-weathering resistance, strong adhesive force and preparation method thereof.
For solving the problems of the technologies described above, the technical solution used in the present invention is: a kind of heat insulation and heat control coated material, made by the raw material of following weight percent: thermoplastic acrylic resin 50-60%, Nano titanium dioxide 5-10%, nano level barium sulfate 5-10%, ceramics powder 5-10%, vacuum glass microballon 5-10%, siloxanes coupling agent 1-2%, tetrafluoroethylene wax 0.2-1%, silicone antifoam agent 0.1-0.5%, dimethylbenzene and N-BUTYL ACETATE mixture 5-10%.
Above-mentioned heat insulation and heat control coated material, the weight percent of described dimethylbenzene and N-BUTYL ACETATE mixture is 50%:50%.
A kind of preparation method of heat insulation and heat control coated material described above comprises the following steps:
(1) at first fully moistening rear placement 24-48 hour is stand-by with the siloxanes coupling agent with the vacuum glass microballon;
(2) thermoplastic acrylic resin, Nano titanium dioxide, nano level barium sulfate, ceramics powder, dimethylbenzene and N-BUTYL ACETATE mixture are distributed to below 10 microns with ultrasonic wave;
(3) material that step (2) is made and silicone antifoam agent, tetrafluoroethylene wax and moistening good vacuum glass microballon disperse with the stepless frequency conversion dispersion machine, are under the 300-600 rev/min of condition at rotating speed, stir packing warehouse-in after 0.5-1 hour.
The advantage of heat insulation and heat control coated material of the present invention and preparation method thereof is:
1, heat insulation and heat control coated material and preparation method thereof, science has designed coating structure and construction technology, has furtherd investigate anticorrosion bottom, the action principle of heat insulation middle layer, heat reflection and thermal radiation surface layer, comprehensive integration strong innovation.
2, heat insulation and heat control coated material and preparation method thereof, by the research and development of novel pigment filler, a painting anticorrosion life-span reaches 5-10.By to sun reflection of light, radiation iris action, make the coating equipment surface temperature fall 10-20 ℃, internal temperature reduces 8-10 ℃.
Embodiment
Below in conjunction with specific embodiment the present invention is described in further detail.
Embodiment 1, a kind of heat insulation and heat control coated material is made by the raw material of following weight percent: thermoplastic acrylic resin 58%, Nano titanium dioxide 8%, nano level barium sulfate 8%, ceramics powder 8%, vacuum glass microballon 8%, siloxanes coupling agent 1.2%, tetrafluoroethylene wax 0.6%, silicone antifoam agent 0.2%, dimethylbenzene and N-BUTYL ACETATE mixture 8%.
The weight percent of above-mentioned dimethylbenzene and N-BUTYL ACETATE mixture is 50%:50%.
The preparation method of the heat insulation and heat control coated material of preparation present embodiment may further comprise the steps:
(1) vacuum glass microballon 8% usefulness siloxanes coupling agent 1.2% abundant moistening rear placement 24-48 hour is stand-by;
(2) thermoplastic acrylic resin 58%, Nano titanium dioxide 8%, nano level barium sulfate 8%, ceramics powder 8%, dimethylbenzene and N-BUTYL ACETATE mixture 8% usefulness ultrasonic wave are distributed to below 10 microns;
(3) material that step (2) is made and silicone antifoam agent 0.2%, tetrafluoroethylene wax 0.6% and moistening good vacuum glass microballon disperse with the stepless frequency conversion dispersion machine, be under the 300-600 rev/min of condition at rotating speed, stir packing warehouse-in after 0.5-1 hour.
Embodiment 2, a kind of heat insulation and heat control coated material is made by the raw material of following weight percent: thermoplastic acrylic resin 56%, Nano titanium dioxide 9%, nano level barium sulfate 8.2%, ceramics powder 10%, vacuum glass microballon 6.2%, siloxanes coupling agent 1.7%, tetrafluoroethylene wax 0.8%, silicone antifoam agent 0.3%, dimethylbenzene and N-BUTYL ACETATE mixture 7.8%.
The weight percent of above-mentioned dimethylbenzene and N-BUTYL ACETATE mixture is 50%:50%.
The preparation method of the heat insulation and heat control coated material of preparation present embodiment may further comprise the steps:
(1) vacuum glass microballon 6.2% usefulness siloxanes coupling agent 1.7% abundant moistening rear placement 24-48 hour is stand-by;
(2) thermoplastic acrylic resin 56%, Nano titanium dioxide 9%, nano level barium sulfate 8.2%, ceramics powder 10%, dimethylbenzene and N-BUTYL ACETATE mixture 7.8% usefulness ultrasonic wave are distributed to below 10 microns;
(3) material that step (2) is made and silicone antifoam agent 0.3%, tetrafluoroethylene wax 0.8% and moistening good vacuum glass microballon disperse with the stepless frequency conversion dispersion machine, be under the 300-600 rev/min of condition at rotating speed, stir packing warehouse-in after 0.5-1 hour.
Embodiment 3, a kind of heat insulation and heat control coated material is made by the raw material of following weight percent: thermoplastic acrylic resin 60%, Nano titanium dioxide 6.5%, nano level barium sulfate 7%, ceramics powder 5%, vacuum glass microballon 9%, siloxanes coupling agent 2%, tetrafluoroethylene wax 1%, silicone antifoam agent 0.5%, dimethylbenzene and N-BUTYL ACETATE mixture 9%.
The weight percent of above-mentioned dimethylbenzene and N-BUTYL ACETATE mixture is 50%:50%.
The preparation method of the heat insulation and heat control coated material of preparation present embodiment may further comprise the steps:
(1) vacuum glass microballon 9% usefulness siloxanes coupling agent 2% abundant moistening rear placement 24-48 hour is stand-by;
(2) thermoplastic acrylic resin 60%, Nano titanium dioxide 6.5%, nano level barium sulfate 7%, ceramics powder 5%, dimethylbenzene and N-BUTYL ACETATE mixture 9% usefulness ultrasonic wave are distributed to below 10 microns;
(3) material that step (2) is made and silicone antifoam agent 0.5%, tetrafluoroethylene wax 1% and moistening good vacuum glass microballon disperse with the stepless frequency conversion dispersion machine, be under the 300-600 rev/min of condition at rotating speed, stir packing warehouse-in after 0.5-1 hour.
Certainly, above-mentioned explanation is not to be limitation of the present invention, and the present invention also is not limited to above-mentioned giving an example; those skilled in the art; in essential scope of the present invention, the variation of making, change, interpolation or replacement all should belong to protection scope of the present invention.

Claims (3)

1. heat insulation and heat control coated material, it is characterized in that: the raw material by following weight percent is made: thermoplastic acrylic resin 50-60%, Nano titanium dioxide 5-10%, nano level barium sulfate 5-10%, ceramics powder 5-10%, vacuum glass microballon 5-10%, siloxanes coupling agent 1-2%, tetrafluoroethylene wax 0.2-1%, silicone antifoam agent 0.1-0.5%, dimethylbenzene and N-BUTYL ACETATE mixture 5-10%.
2. according to claim 1 described heat insulation and heat control coated material, it is characterized in that: the weight percent of described dimethylbenzene and N-BUTYL ACETATE mixture is 50%:50%.
3. the preparation method of heat insulation and heat control coated material as claimed in claim 1 is characterized in that: comprise the following steps:
(1) at first fully moistening rear placement 24-48 hour is stand-by with the siloxanes coupling agent with the vacuum glass microballon;
(2) thermoplastic acrylic resin, Nano titanium dioxide, nano level barium sulfate, ceramics powder, dimethylbenzene and N-BUTYL ACETATE mixture are distributed to below 10 microns with ultrasonic wave;
(3) material that step (2) is made and silicone antifoam agent, tetrafluoroethylene wax and moistening good vacuum glass microballon disperse with the stepless frequency conversion dispersion machine, are under the 300-600 rev/min of condition at rotating speed, stir packing warehouse-in after 0.5-1 hour.
CN2012105645418A 2012-12-24 2012-12-24 Heat insulation and heat control coating material and preparation method thereof Pending CN102964957A (en)

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Application Number Priority Date Filing Date Title
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Cited By (6)

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Publication number Priority date Publication date Assignee Title
CN103214910A (en) * 2013-04-03 2013-07-24 上海三思电子工程有限公司 Radiation heat dissipation coating for reducing light-emitting diode (LED) chip junction temperature and preparation method thereof
CN103436123A (en) * 2013-08-28 2013-12-11 广西梧州龙鱼漆业有限公司 Solvent-type super-weather-proof exterior wall coating and preparation method thereof
CN104371400A (en) * 2013-09-30 2015-02-25 扬州润扬物流装备有限公司 Container paint and preparation method thereof
CN107216701A (en) * 2015-09-27 2017-09-29 朱海燕 A kind of self-cleaning ceramic coating
CN108504217A (en) * 2018-04-18 2018-09-07 合肥大麦灯箱器材有限公司 A kind of paint and preparation method thereof being applied to advisement exhibition apparatus surface
CN109233493A (en) * 2017-05-10 2019-01-18 上海大学 Hot coating of a kind of high reflectance acrylic acid screening and preparation method thereof

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103214910A (en) * 2013-04-03 2013-07-24 上海三思电子工程有限公司 Radiation heat dissipation coating for reducing light-emitting diode (LED) chip junction temperature and preparation method thereof
CN103436123A (en) * 2013-08-28 2013-12-11 广西梧州龙鱼漆业有限公司 Solvent-type super-weather-proof exterior wall coating and preparation method thereof
CN104371400A (en) * 2013-09-30 2015-02-25 扬州润扬物流装备有限公司 Container paint and preparation method thereof
CN107216701A (en) * 2015-09-27 2017-09-29 朱海燕 A kind of self-cleaning ceramic coating
CN107216701B (en) * 2015-09-27 2019-12-27 朱海燕 Self-cleaning ceramic coating
CN109233493A (en) * 2017-05-10 2019-01-18 上海大学 Hot coating of a kind of high reflectance acrylic acid screening and preparation method thereof
CN108504217A (en) * 2018-04-18 2018-09-07 合肥大麦灯箱器材有限公司 A kind of paint and preparation method thereof being applied to advisement exhibition apparatus surface

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Application publication date: 20130313