CN102960704A - Sugar-free compound sweetener suitable for neutral solid beverages and preparation method of sweetener - Google Patents
Sugar-free compound sweetener suitable for neutral solid beverages and preparation method of sweetener Download PDFInfo
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Abstract
The invention relates to a sugar-free compound sweetener suitable for neutral solid beverages and a preparation method of the sweetener. The sugar-free compound sweetener is prepared from the following components: 8.33-13.33% of sucralose, 30-33% of erythritol, 43.67-52.67% of isomaltose hypgather and 9-10% of xylitol; and the preparation method comprises the following process of: putting the sugar alcohols and isomaltose hypgather accounting for 50-60% of the total quantity into a multifunctional mixer for premixing; dissolving sucralose and the residual isomaltose hypgather in water, thereby obtaining mixed aqueous solution; feeding the mixture into a fluidized bed of spray fluidization equipment from the lower part of the fluidized bed, so that the mixture does accelerated spiral flow from bottom to top under positive pressure; and applying pulsed negative pressure to the upper part of the fluidized bed by adjusting the air volume and the air direction of an air inducing device so that a plurality of cloth bags on a porous separator vibrate up and down and hit the mixture into fine particles; and continuously spraying and dispersing the mixed aqueous solution to the particles in the fluidized bed by means of multi-point spray guns arranged on the sidewalls of the fluidized bed, thereby obtaining the compound sweetener.
Description
Technical field
The present invention relates to a kind of food additives, be specifically related to a kind of sugar-free composite sweetener that is applicable to neutral solid beverage and preparation method thereof.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, as the sweetener of food additives, one of its development priority is exactly safe, without nutritive value, empty calory or functional high sweetener extremely low in calories.The characteristics of functional high sweetener are use safe, and consumption is few, and sugariness is high, and use cost is generally all far below sucrose, and this also is the power place that Food Science man continually develops novel high-intensity sweetener.At present, about 20 kinds of the granted high sweetener in countries in the world obtains that kind that the majority state approval allows to use mainly contains that saccharin sodium, honey element, 3,4-Dihydro-6-methyl-1,2,3-oxathiazin-4-one 2,2-dioxide potassium salt, Aspartame, Sucralose, alitame, knob are sweet, glycyrrhizin, stevioside, Momordica grosvenori is sweet and Talin etc.These high sweeteners have plenty of artificial synthetic, and are sweet etc. such as Aspartame, Sucralose, knob; What have then is natural extract, sweet etc. such as sky chrysanthemum glycosides and arhat.No matter be artificial synthesis edulcorant or natural extraction sweetener, at sugariness, sweet taste, stable aspects its pluses and minuses arranged respectively all, therefore, want to give full play to the optimal efficacy of these sweeteners, reduce cost, the most frequently used means are exactly compound at present.By carrying out various sweeteners or sweet substance compound, bring into play may exist between the various sweeteners synergistic function, in the hope of as far as possible approaching or satisfy the requirement of desirable sweetener: safety non-toxic, sweet taste is pure similar to sucrose (this is to be popular generally accepted sweet tastes), high sugariness, low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
In the prior art, have with the composite composite sweetener of Sucralose, antierythrite, xylitol and oligoisomaltose, when being applied in the neutral solid beverages such as milk tea, soya-bean milk when these composite sweeteners, mouthfeel is not fine, and effect is unsatisfactory; And all used more xylitol and antierythrite in these composite sweeteners, this has improved the cost of product virtually.
Composite sweetener take Sucralose as main sweetening material in the prior art, can process by method or the spray-dired method of substep of simple blend, the composite sweetener that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material Sucralose can be uniformly dispersed, and this point can affect the quality of composite sweetener product to a great extent.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the granular sweetener by spraying respectively, the composite sweetener product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the composite sweetener product that additive method makes, but its shortcoming is: material loss is large, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, the cost of product is significantly increased, and therefore this method also has been subject to certain restriction in implementation process.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, provide that a kind of mouthfeel is better, cost is cheaper and be particularly suitable for sugar-free composite sweetener that uses in neutral solid beverage and preparation method thereof.
Purpose of the present invention is achieved through the following technical solutions:
A kind of sugar-free composite sweetener that is applicable to neutral solid beverage comprises following percentage by weight composition: Sucralose 8.33 ~ 13.33%, antierythrite 30 ~ 33%, oligoisomaltose 43.67 ~ 52.67%, xylitol 9 ~ 10%; Its preparation method comprises following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 50 ~ 60% are dropped in the Multidimensionblender, mixed 30 ~ 45 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of antierythrite, xylitol and oligoisomaltose;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, by the hot blast continuous drying, obtain described sugar-free composite sweetener again.
A kind of preparation method who is applicable to the sugar-free composite sweetener of neutral solid beverage of the present invention comprises following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 50 ~ 60% are dropped in the Multidimensionblender, mixed 30 ~ 45 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of antierythrite, xylitol and oligoisomaltose;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, by the hot blast continuous drying, obtain described sugar-free composite sweetener again.
Further, above-mentioned a kind of preparation method who is applicable to the sugar-free composite sweetener of neutral solid beverage, the fluid bed of described spray-fluidized equipment is the cylinder column, the height of fluid bed accounts for 1/2 ~ 2/3 of spray-fluidized device height.
Again further, above-mentioned a kind of preparation method who is applicable to the sugar-free composite sweetener of neutral solid beverage, step 4. in, the wind pushing temperature of fluid bed is at 40 ~ 100 ℃; When the mixed aqueous solution spraying disperseed, the wind pushing temperature of control fluid bed was at 40 ~ 70 ℃, and the wind pushing temperature of control fluid bed is at 70 ~ 100 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
The present invention has controlled the ratio of composite sweetener mesoerythrit and xylitol subtly, when the sugariness multiple of composite sweetener and sucrose is in about 50 ~ 80 times scope, composite sweetener product of the present invention can be applied in the neutral solid beverages such as milk tea, soya-bean milk well, improves mouthfeel and the local flavor of application; In addition because composition of raw materials of the present invention has reduced the higher antierythrite of cost and the consumption of xylitol, also so that composite sweetener product of the present invention reduced about 10% ~ 15% than the cost of material of other like products.
The present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and carry out disposable spraying by improved spray-fluidized bed apparatus voluntarily and disperse dry, make it to be coated on just mixed mixed material surface, obtained even tiny granular composite sweetener product.Compare with the method for prior art simple blend, the product instant capacity that the present invention obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; Compare the present invention's energy Effective Raise granulation efficiency, the uniformity and the fineness of lifting particle with the prilling process that uses traditional spray equipment; With in the prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy has reduced production cost.
Description of drawings
Fig. 1: the master of spray-fluidized equipment used in the present invention looks schematic diagram;
The A-A of Fig. 2: Fig. 1 is to cross-sectional schematic;
The B-B of Fig. 3: Fig. 1 is to cross-sectional schematic;
The specific embodiment
Composite sweetener of the present invention, its composition is: Sucralose 8.33 ~ 13.33%, antierythrite 30 ~ 33%, oligoisomaltose 43.67 ~ 52.67%, xylitol 9 ~ 10%.
The preparation technology of composite sweetener: 1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 50 ~ 60% are dropped in the Multidimensionblender, progression with 800 ~ 1000rpm mixed 30 ~ 45 minutes, obtained the mixed material of antierythrite, xylitol and oligoisomaltose;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension; Fluid bed is the cylinder column, and the height of fluid bed accounts for 1/2 ~ 2/3 of spray-fluidized device height;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, by the hot blast continuous drying, obtain described composite sweetener again; The wind pushing temperature of fluid bed is at 40 ~ 100 ℃; When the mixed aqueous solution spraying disperseed, the wind pushing temperature of control fluid bed was at 40 ~ 70 ℃, and the wind pushing temperature of control fluid bed is at 70 ~ 100 ℃ during heated-air drying.
Multidimensionblender of the present invention is common commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Spray-fluidized equipment used in the present invention, such as Fig. 1, Fig. 2 and shown in Figure 3, this spray-fluidized equipment comprises columniform fluid bed 1, air-supply arrangement 2, blower unit 3, the plenum chamber 4 that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement 2, the air inducing chamber 5 that is positioned at spray-fluidized equipment top and is connected with blower unit 3, the bottom of plenum chamber 4 and fluid bed 1 is separated by by the flabellum dividing plate 6 that polylith can rotate, between the every flabellum dividing plate 6 interlaced and leave the slit so that wind energy enough by and powder can not pass through, air inducing chamber 5 is separated by by porous barrier 7 with the top of described fluid bed 1, on each hole of described porous barrier cloth bag 8 is installed, the degree of depth of cloth bag 8 can reach 2/3 ~ 1/3 of fluid bed 1 height during stretching, extension; The height of fluidized-bed layer accounts for 1/2 of whole spray-fluidized device height.During this spray-fluidized equipment work, be first the charging aperture 9 of material from fluid bed 1 side lower part to be dropped in the fluid bed 1, drive air-supply arrangement 2 air-supplies and 6 rotations of flabellum dividing plate, the material in the fluid bed 1 then flows with helical the acceleration from bottom to top of malleation; Drive blower unit 3, air quantity by regulating blower unit 3 and wind direction impose the pulse negative pressure to the top of fluid bed 1 and make a plurality of cloth bags 8 up-down vibration (with the shake of level and other directions) on the porous barrier 7, and constantly impact mixed material, this makes the mixed material can be from the omnibearing acquisition momentum of all directions, thereby guarantee that material can mix, form tiny powder.At this moment also can other solution sprays be dispersed on the tiny powder in the fluid bed by a plurality of spray guns 10 on the fluid bed sidewall, make the product of expection.This spraying apparatus can high efficiency enforcement granulation and the problem such as caking can not occur, and institute's particle that obtains is tiny evenly, therefore is fit to very much the preparation of the products such as sweetener.
Embodiment 1:
(1) gets in 30 kilograms of antierythrites, 9.2 kilograms of xylitols and 28.85 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 35 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 23.62 kilograms of 8.33 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized equipment of the present invention by the charging aperture of fluid bed side lower part, drive air-supply arrangement and flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, the top of fluid bed imposes the pulse negative pressure by regulating blower unit, make a plurality of cloth bag up-down vibration and multi-faceted shake on the porous barrier, constantly impact mixed material, make it to form tiny uniform sugar alcohol powder;
(4) by a plurality of spray guns on the fluid bed sidewall the continuous spraying of the prepared mixed aqueous solution of step (2) is distributed on the interior sugar alcohol powder of fluid bed, the wind pushing temperature of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the wind pushing temperature of fluid bed between 70 ~ 100 ℃, carry out continuous heated-air drying, last discharging obtains the granular composite sweetener.
Embodiment 2:
(1) gets in 31 kilograms of antierythrites, 9.5 kilograms of xylitols and 28.2 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 35 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 21.3 kilograms of 10 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized equipment of the present invention by the charging aperture of fluid bed side lower part, drive air-supply arrangement and flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, the top of fluid bed imposes the pulse negative pressure by regulating blower unit, make a plurality of cloth bag up-down vibration and multi-faceted shake on the porous barrier, constantly impact mixed material, make it to form tiny uniform sugar alcohol powder;
(4) by a plurality of spray guns on the fluid bed sidewall the continuous spraying of the prepared mixed aqueous solution of step (2) is distributed on the interior sugar alcohol powder of fluid bed, the wind pushing temperature of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the wind pushing temperature of fluid bed between 70 ~ 100 ℃, carry out continuous heated-air drying, last discharging obtains the granular composite sweetener.
Embodiment 3:
(1) gets in 32 kilograms of antierythrites, 9.7 kilograms of xylitols and 26.63 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 40 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 20 kilograms of 11.67 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized equipment of the present invention by the charging aperture of fluid bed side lower part, drive air-supply arrangement and flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, the top of fluid bed imposes the pulse negative pressure by regulating blower unit, make a plurality of cloth bag up-down vibration and multi-faceted shake on the porous barrier, constantly impact mixed material, make it to form tiny uniform sugar alcohol powder;
(4) by a plurality of spray guns on the fluid bed sidewall the continuous spraying of the prepared mixed aqueous solution of step (2) is distributed on the interior sugar alcohol powder of fluid bed, the wind pushing temperature of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the wind pushing temperature of fluid bed between 70 ~ 100 ℃, carry out continuous heated-air drying, last discharging obtains the granular composite sweetener.
Embodiment 4:
(1) gets in 32.5 kilograms of antierythrites, 10 kilograms of xylitols and 24.17 kilograms of inputs of the oligoisomaltose Multidimensionblender, the progression of control Multidimensionblender is 800rpm, mixed 40 minutes, obtain the mixed material of antierythrite, xylitol and oligoisomaltose, granularity is between 80 ~ 130 orders;
(2) 20 kilograms of 13.33 kilograms of Sucraloses, remaining oligoisomaltose are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
(3) mixed material of step (1) gained is put in the spray-fluidized equipment of the present invention by the charging aperture of fluid bed side lower part, drive air-supply arrangement and flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, the top of fluid bed imposes the pulse negative pressure by regulating blower unit, make a plurality of cloth bag up-down vibration and multi-faceted shake on the porous barrier, constantly impact mixed material, make it to form tiny uniform sugar alcohol powder;
(4) by a plurality of spray guns on the fluid bed sidewall the continuous spraying of the prepared mixed aqueous solution of step (2) is distributed on the interior sugar alcohol powder of fluid bed, the wind pushing temperature of control fluid bed is between 40 ~ 70 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the wind pushing temperature of fluid bed between 70 ~ 100 ℃, carry out continuous heated-air drying, last discharging obtains the granular composite sweetener.
The composite sweetener that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
The present invention has controlled the ratio of composite sweetener mesoerythrit and xylitol subtly, when the sugariness multiple of composite sweetener and sucrose is in about 50 ~ 80 times scope, composite sweetener product of the present invention can be applied in the neutral solid beverage that milk tea, soya-bean milk etc. can reconstitute with pulvis well, improves mouthfeel and the local flavor of application; In addition because composition of raw materials of the present invention has reduced the higher antierythrite of cost and the consumption of xylitol, also so that composite sweetener product of the present invention than the cost of other like products about 10% ~ 15%.
Preparation method of the present invention drops into the auxiliary sweetening material of the part of composite sweetener in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and carry out disposable spraying by improved spray-fluidized bed apparatus voluntarily and disperse dry, make it to be coated on just mixed mixed material surface, obtained even tiny granular composite sweetener product.Compare with the method for prior art simple blend, the product instant capacity that the present invention obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; Compare the present invention's energy Effective Raise granulation efficiency, the uniformity and the fineness of lifting particle with the prilling process that uses traditional spray equipment; With in the prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy, reduced production cost (about 60 ~ 80 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of composite sweetener of the present invention can be adjusted by the consumption of Sucralose according to actual needs, and the present invention is fit to the sugar-free composite sweetener of 50～80 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. a sugar-free composite sweetener that is applicable to neutral solid beverage is characterized in that comprising following percentage by weight composition: Sucralose 8.33 ~ 13.33%, antierythrite 30 ~ 33%, oligoisomaltose 43.67 ~ 52.67%, xylitol 9 ~ 10%; Its preparation method comprises following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 50 ~ 60% are dropped in the Multidimensionblender, mixed 30 ~ 45 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of antierythrite, xylitol and oligoisomaltose;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, by the hot blast continuous drying, obtain described sugar-free composite sweetener again.
2. a kind of preparation method who is applicable to the sugar-free composite sweetener of neutral solid beverage claimed in claim 1 is characterized in that comprising following processing step:
1. antierythrite, xylitol and the oligoisomaltose that accounts for total amount 50 ~ 60% are dropped in the Multidimensionblender, mixed 30 ~ 45 minutes with the progression of 800 ~ 1000rpm, obtain the mixed material of antierythrite, xylitol and oligoisomaltose;
2. the oligoisomaltose with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and oligoisomaltose;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, by the hot blast continuous drying, obtain described sugar-free composite sweetener again.
3. a kind of preparation method who is applicable to the sugar-free composite sweetener of neutral solid beverage according to claim 2, it is characterized in that: the fluid bed of described spray-fluidized equipment is the cylinder column, and the height of fluid bed accounts for 1/2 ~ 2/3 of spray-fluidized device height.
4. a kind of preparation method who is applicable to the sugar-free composite sweetener of neutral solid beverage according to claim 2 is characterized in that: step 4. in, the wind pushing temperature of fluid bed is at 40 ~ 100 ℃.
5. a kind of preparation method who is applicable to the sugar-free composite sweetener of neutral solid beverage according to claim 4, it is characterized in that: step 4. in, when the mixed aqueous solution spraying disperses, the wind pushing temperature of control fluid bed is at 40 ~ 70 ℃, and the wind pushing temperature of control fluid bed is at 70 ~ 100 ℃ during heated-air drying.
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| CN1672567A (en) * | 2004-03-24 | 2005-09-28 | 江西省农学会 | Sweetener |
| CN201337897Y (en) * | 2008-12-05 | 2009-11-04 | 株洲千金药业股份有限公司 | Spray drying granulator |
| CN101897426A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Granular composite sugar-free sweetener and preparation method thereof |
| CN102429204A (en) * | 2011-12-09 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Fluffy granular compound sugar-free sweetening agent and preparation method thereof |
| CN102440369A (en) * | 2011-12-09 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Fluffy powdery composite sugar-free sweetener and preparation method thereof |
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2012
- 2012-11-30 CN CN2012105013865A patent/CN102960704A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1672567A (en) * | 2004-03-24 | 2005-09-28 | 江西省农学会 | Sweetener |
| CN201337897Y (en) * | 2008-12-05 | 2009-11-04 | 株洲千金药业股份有限公司 | Spray drying granulator |
| CN101897426A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Granular composite sugar-free sweetener and preparation method thereof |
| CN102429204A (en) * | 2011-12-09 | 2012-05-02 | 苏州工业园区尚融科技有限公司 | Fluffy granular compound sugar-free sweetening agent and preparation method thereof |
| CN102440369A (en) * | 2011-12-09 | 2012-05-09 | 苏州工业园区尚融科技有限公司 | Fluffy powdery composite sugar-free sweetener and preparation method thereof |
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Application publication date: 20130313 |