CN103039778A - Preparation method of sugarless table sugar - Google Patents
Preparation method of sugarless table sugar Download PDFInfo
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- CN103039778A CN103039778A CN2012105723258A CN201210572325A CN103039778A CN 103039778 A CN103039778 A CN 103039778A CN 2012105723258 A CN2012105723258 A CN 2012105723258A CN 201210572325 A CN201210572325 A CN 201210572325A CN 103039778 A CN103039778 A CN 103039778A
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Abstract
The invention relates to a preparation method of sugarless table sugar. The sugarless table sugar comprises the following components: 0.83-1.17% of sucralose, 48-52% of isomaltitol, 8-10% of erythritol, 35-38% of maltitol and 0.5% of calcium silicate. The preparation method of the sugarless table sugar comprises the following steps: adding isomaltitol, erythritol and 50-70% of maltitol into a multi-dimensional mixer, and mixing to obtain a mixed material; dissolving sucralose and the rest of maltitol into water to obtain a mixed water solution; adding the mixed material into a fluidizing bed of spraying and fluidizing equipment from the lower part of the fluidizing bed, mixing, accelerating spiral flow from the bottom up under a positive pressure, vibrating multiple cloth bags on a porous partition board up and down to beat the mixed material into fine powder; continuously spraying and dispersing the mixed water solution onto the powder inside the fluidizing bed, and drying to obtain table sugar powder; and uniformly mixing the table sugar powder and calcium silicate to obtain finished sugarless table sugar.
Description
Technical field
The present invention relates to a kind of edible sweetening material, be specifically related to a kind of preparation method of Sugarless mensal sugar.
Background technology
In the last few years, raising along with expanding economy and people's lives wealth, obesity, hypertension, diabetes, carious tooth etc. become the height morbidity among the crowd, and the generation of these high morbidities is considered to especially with the sucrose Excessive Intake substantial connection is arranged with eating habit and diet structure.Therefore, people's demand safety and Health, empty calory, do not participate in the non-nutritive dining table sugar of body metabolism.The main feature of sugar-free or low-sugar low-calorie dining-table sugar be exactly safe, consumption is few, sugariness generally is 2 ~ 20 times of sucrose, and use cost is generally all far below sucrose.This dining table sugar generally all selects the very high high sweetener of sugariness as main sweetening material, carries out composite with the not high auxiliary sweetening materials such as glycitols of other sugarinesses and makes.According to different sweet taste demands, people are by carrying out different main sweetening materials and auxiliary sweetening material compound, make the various sweetening materials can Synergistic at the features of the aspects such as sugariness, sweet taste, stability, in the hope of can approach or satisfy the requirement of desirable dining table sugar as far as possible, namely safety non-toxic, that sweet taste is pure is similar to sucrose (this is to be popular generally accepted sweet tastes), low heat value or without calorific value, stable height, unlikely dental caries, reduction cost.
Dining table sugar take Sucralose as main sweetening material in the prior art, can process by method or the spray-dired method of substep of simple blend, the dining table sugar that the simple blend method makes is with low cost, but be difficult to guarantee that main sweetening material Sucralose can be uniformly dispersed, the dissolubility of sugar grain is not good enough.The spray-dired method of substep is that substep is dissolved in main sweetening material and each auxiliary sweetening material in the deionized water in batches, then the method by the wet spray drying is coated on each composition material on the sugared particle by spraying respectively, the dining table sugar product sweetness that this method makes is uniformly dispersed, instant capacity is good, quality is better than the dining table sugar that additive method makes, but its shortcoming is: spray process is large to material loss, the loss of especially main sweetening material is larger, machinery equipment power consumption is too high, and the cost of product is significantly increased.And present Sucralose type dining table sugar product also ubiquity mouthfeel is compared different, poor stability, easily is bonded to the problem of piece with sucrose.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, the better preparation method of Sugarless mensal sugar of a kind of with low cost, mouthfeel and stability is provided, the sugariness of this dining table sugar is 5 ~ 7 times of sucrose sweetness.
Purpose of the present invention is achieved through the following technical solutions:
A kind of preparation method of Sugarless mensal sugar, dining table sugar comprises following percentage by weight composition: Sucralose 0.83 ~ 1.17%, isomalt 48 ~ 52%, antierythrite 8 ~ 10%, maltitol 35 ~ 38%, calcium silicates 0.5%; Its preparation method comprises following processing step:
1. isomalt, antierythrite and the maltitol that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 40 minutes with the progression of 600 ~ 1000rpm, obtain the mixed material of isomalt, antierythrite and maltitol;
2. the maltitol with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and maltitol;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, again by the hot blast continuous drying, obtain the dining table sugar powder;
5. add calcium silicates in the dining table sugar powder that 4. obtains to step, mix, discharging, pack namely gets described Sugarless mensal sugar.
Further, the preparation method of above-mentioned a kind of Sugarless mensal sugar, the fluid bed of described spray-fluidized equipment is the cylinder column, the height of fluid bed accounts for 1/2 ~ 2/3 of spray-fluidized device height.
Further, the preparation method of above-mentioned a kind of Sugarless mensal sugar, step 4. in, the wind pushing temperature of fluid bed is at 50 ~ 105 ℃; When the mixed aqueous solution spraying disperseed, the wind pushing temperature of control fluid bed was at 50 ~ 80 ℃, and the wind pushing temperature of control fluid bed is at 80 ~ 105 ℃ during heated-air drying.
The substantive distinguishing features that technical solution of the present invention is outstanding and significant progressive being mainly reflected in:
Composition of raw materials of the present invention is reasonable, and mouthfeel, instant capacity are good, and because adopted special voluntarily improved spraying apparatus and in composition of raw materials, added specified quantitative calcium silicates and so that powder is not easy to be bonded to piece.
The present invention carries out tentatively mixing in the part glycitols raw material input Multidimensionblender with dining table sugar first, then main sweetening material and remaining other raw materials are dissolved into mixed aqueous solution, and carry out disposable spraying by improved spray-fluidized bed apparatus voluntarily and disperse dry, make it to be coated on just mixed mixed material surface, add again the calcium silicates mixing, obtained even tiny granular dining table sugar product.Compare with the method for prior art simple blend, the product instant capacity that the present invention obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; Compare the present invention's energy Effective Raise granulation efficiency, the uniformity and the fineness of lifting particle with the prilling process that uses traditional spray equipment; With in the prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy has reduced production cost.
Description of drawings
Fig. 1: the master of spray-fluidized equipment used in the present invention looks schematic diagram;
The A-A of Fig. 2: Fig. 1 is to cross-sectional schematic;
The B-B of Fig. 3: Fig. 1 is to cross-sectional schematic;
The specific embodiment
Sugarless mensal sugar of the present invention, its composition is: Sucralose 0.83 ~ 1.17%, isomalt 48 ~ 52%, antierythrite 8 ~ 10%, maltitol 35 ~ 38%, calcium silicates 0.5%.
The preparation technology of this Sugarless mensal sugar: 1. isomalt, antierythrite and the maltitol that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, progression with 600 ~ 1000rpm mixed 20 ~ 40 minutes, obtained the mixed material of isomalt, antierythrite and maltitol;
2. the maltitol with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and maltitol;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension; Fluid bed is the cylinder column, and the height of fluid bed accounts for 1/2 ~ 2/3 of spray-fluidized device height;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, again by the hot blast continuous drying, obtain the dining table sugar powder; The wind pushing temperature of fluid bed is at 50 ~ 105 ℃; When the mixed aqueous solution spraying disperseed, the wind pushing temperature of control fluid bed was at 50 ~ 80 ℃, and the wind pushing temperature of control fluid bed is at 80 ~ 105 ℃ during heated-air drying;
5. add calcium silicates in the dining table sugar powder that 4. obtains to step, mix, discharging, pack namely gets described Sugarless mensal sugar product.
Multidimensionblender of the present invention is common commercial 200 feather weight Multidimensionblenders, rotating speed level journey is 200 ~ 1800rpm, barrel is two taper, middle column, and during work, this Multidimensionblender can make the material in the barrel collide, pulverize and mix from a plurality of angles.
Spray-fluidized equipment used in the present invention, such as Fig. 1, Fig. 2 and shown in Figure 3, this spray-fluidized equipment comprises columniform fluid bed 1, air-supply arrangement 2, blower unit 3, the plenum chamber 4 that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement 2, the air inducing chamber 5 that is positioned at spray-fluidized equipment top and is connected with blower unit 3, the bottom of plenum chamber 4 and fluid bed 1 is separated by by the flabellum dividing plate 6 that polylith can rotate, between the every flabellum dividing plate 6 interlaced and leave the slit so that wind energy enough by and powder can not pass through, air inducing chamber 5 is separated by by porous barrier 7 with the top of described fluid bed 1, on each hole of described porous barrier cloth bag 8 is installed, the degree of depth of cloth bag 8 can reach 2/3 ~ 1/3 of fluid bed 1 height during stretching, extension; The height of fluidized-bed layer accounts for 1/2 of whole spray-fluidized device height.During this spray-fluidized equipment work, be first the charging aperture 9 of material from fluid bed 1 side lower part to be dropped in the fluid bed 1, drive air-supply arrangement 2 air-supplies and 6 rotations of flabellum dividing plate, the material in the fluid bed 1 then flows with helical the acceleration from bottom to top of malleation; Drive blower unit 3, air quantity by regulating blower unit 3 and wind direction impose the pulse negative pressure to the top of fluid bed 1 and make a plurality of cloth bags 8 up-down vibration (with the shake of level and other directions) on the porous barrier 7, and constantly impact mixed material, this makes the mixed material can be from the omnibearing acquisition momentum of all directions, thereby guarantee that material can mix, form tiny powder.At this moment also can other solution sprays be dispersed on the tiny powder in the fluid bed by a plurality of spray guns 10 on the fluid bed sidewall, make the product of expection.This spraying apparatus can high efficiency enforcement granulation and be not prone to the problem such as caking, and institute's particle that obtains is tiny evenly, therefore is fit to very much the preparation of the products such as sweetener, dining table sugar.
Embodiment 1:
(1) gets in 51 kilograms of isomalts, 10 kilograms of antierythrites, 22.5 kilograms of inputs of the maltitol Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 30 minutes, obtain the mixed material of isomalt, antierythrite and maltitol, granularity is between 80 ~ 130 orders;
(2) 15.17 kilograms of 0.83 kilogram of Sucraloses, remaining maltitol are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and maltitol;
(3) mixed material of step (1) gained is put in the spray-fluidized equipment of the present invention by the charging aperture of fluid bed side lower part, drive air-supply arrangement and flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, the top of fluid bed imposes the pulse negative pressure by regulating blower unit, make a plurality of cloth bag up-down vibration and multi-faceted shake on the porous barrier, constantly impact mixed material, make it to form tiny uniform powder;
(4) by a plurality of spray guns on the fluid bed sidewall the continuous spraying of the prepared mixed aqueous solution of step (2) is distributed on the interior sugar alcohol powder of fluid bed, the wind pushing temperature of control fluid bed is between 50 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the wind pushing temperature of fluid bed between 80 ~ 105 ℃, carry out continuous heated-air drying, obtain the dining table sugar powder;
(5) the dining table sugar powder that step (4) is obtained drops in the Multidimensionblender with 0.5 kilogram of calcium silicates, and 1000rpm mixed after ten minutes, and discharging, pack namely obtain the Sugarless mensal sugar product of present embodiment.
Embodiment 2:
(1) gets in 51 kilograms of isomalts, 9.5 kilograms of antierythrites, 23.6 kilograms of inputs of the maltitol Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 30 minutes, obtain the mixed material of isomalt, antierythrite and maltitol, granularity is between 80 ~ 130 orders;
(2) 14.4 kilograms of 1 kilogram of Sucraloses, remaining maltitol are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and maltitol;
(3) mixed material of step (1) gained is put in the spray-fluidized equipment of the present invention by the charging aperture of fluid bed side lower part, drive air-supply arrangement and flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, the top of fluid bed imposes the pulse negative pressure by regulating blower unit, make a plurality of cloth bag up-down vibration and multi-faceted shake on the porous barrier, constantly impact mixed material, make it to form tiny uniform powder;
(4) by a plurality of spray guns on the fluid bed sidewall the continuous spraying of the prepared mixed aqueous solution of step (2) is distributed on the interior sugar alcohol powder of fluid bed, the wind pushing temperature of control fluid bed is between 50 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the wind pushing temperature of fluid bed between 80 ~ 105 ℃, carry out continuous heated-air drying, obtain the dining table sugar powder;
(5) the dining table sugar powder that step (4) is obtained drops in the Multidimensionblender with 0.5 kilogram of calcium silicates, and 1000rpm mixed after ten minutes, and discharging, pack namely obtain the Sugarless mensal sugar product of present embodiment.
Embodiment 3:
(1) gets in 51.2 kilograms of isomalts, 9.5 kilograms of antierythrites, 23 kilograms of inputs of the maltitol Multidimensionblender, the progression of control Multidimensionblender is 1000rpm, mixed 30 minutes, obtain the mixed material of isomalt, antierythrite and maltitol, granularity is between 80 ~ 130 orders;
(2) 14.63 kilograms of 1.17 kilograms of Sucraloses, remaining maltitol are mixed with deionized water, the intensification stirring and dissolving obtains the mixed aqueous solution of Sucralose and maltitol;
(3) mixed material of step (1) gained is put in the spray-fluidized equipment of the present invention by the charging aperture of fluid bed side lower part, drive air-supply arrangement and flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, the top of fluid bed imposes the pulse negative pressure by regulating blower unit, make a plurality of cloth bag up-down vibration and multi-faceted shake on the porous barrier, constantly impact mixed material, make it to form tiny uniform powder;
(4) by a plurality of spray guns on the fluid bed sidewall the continuous spraying of the prepared mixed aqueous solution of step (2) is distributed on the interior sugar alcohol powder of fluid bed, the wind pushing temperature of control fluid bed is between 50 ~ 80 ℃, when spraying finishes substantially after 30 ~ 40 minutes, control again the wind pushing temperature of fluid bed between 80 ~ 105 ℃, carry out continuous heated-air drying, obtain the dining table sugar powder;
(5) the dining table sugar powder that step (4) is obtained drops in the Multidimensionblender with 0.5 kilogram of calcium silicates, and 1000rpm mixed after ten minutes, and discharging, pack namely obtain the Sugarless mensal sugar product of present embodiment.
The Sugarless mensal sugar that adopts technical solution of the present invention to obtain, its main performance index sees Table 1.
Table 1
Sugarless mensal sugar of the present invention has and do not have smell, even white, and is soluble in water, uses very easily characteristics.Products taste is good, and molten speed, the sugariness uniformity, stability are all very good, are difficult for being bonded to piece, belong to the high quality of products in the like product.Dining table sugar product of the present invention was stored 3 years at normal temperatures, the phenomenons such as rotten and sugariness reduction do not occurred, stability is very superior.
The present invention drops into the auxiliary sweetening material of the part in the dining table sugar raw material in the Multidimensionblender first and carries out tentatively mixing, then main sweetening material and remaining auxiliary sweetening material are dissolved into mixed aqueous solution, and carry out disposable spraying by improved spray-fluidized bed apparatus voluntarily and disperse dry, make it to be coated on just mixed mixed material surface, obtained even tiny dining table sugar powder, by making this powder continue to mix with calcium silicates, obtained the Sugarless mensal sugar finished product of good dispersion, prevented from caking.Compare with the method for prior art simple blend, the product instant capacity that the present invention obtains, sugariness dispersiveness etc. have significantly lifting, have good quality; Compare the present invention's energy Effective Raise granulation efficiency, the uniformity and the fineness of lifting particle with the prilling process that uses traditional spray equipment; With in the prior art in batches spray-dired method compare, can greatly shorten the process-cycle again, the amount of saving energy, reduced production cost (about 70 ~ 90 minutes of product manufacturing cycle of the present invention, and about 2 ~ 3 hours of the manufacturing cycle of spray drying process in batches, and the present invention just the mixed power consumption that uses Multidimensionblender be approximately fluidized bed with spraying electricity consumption of equipment amount 1/24).
The sugariness degree of modification of Sugarless mensal sugar of the present invention can be adjusted by the consumption of Sucralose according to actual needs, and the present invention is fit to the dining table sugar product of 5 ~ 7 times of sucrose sweetness of preparation usually.
What need to understand is: the above only is preferred embodiment of the present invention; for those skilled in the art; under the prerequisite that does not break away from the principle of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (4)
1. the preparation method of a Sugarless mensal sugar, it is characterized in that: the Sugarless mensal steamed bun stuffed with sugar contains following percentage by weight composition: Sucralose 0.83 ~ 1.17%, isomalt 48 ~ 52%, antierythrite 8 ~ 10%, maltitol 35 ~ 38%, calcium silicates 0.5%; Its preparation method comprises following processing step:
1. isomalt, antierythrite and the maltitol that accounts for total amount 50 ~ 70% are dropped in the Multidimensionblender, mixed 20 ~ 40 minutes with the progression of 600 ~ 1000rpm, obtain the mixed material of isomalt, antierythrite and maltitol;
2. the maltitol with Sucralose and surplus is dissolved in the water, obtains the mixed aqueous solution of Sucralose and maltitol;
3. with step 1. the mixed material of gained put in the spray-fluidized equipment, spray-fluidized equipment comprises fluid bed, air-supply arrangement, blower unit, the plenum chamber that is positioned at the spray-fluidized device bottom and is connected with air-supply arrangement, the air inducing chamber that is positioned at spray-fluidized equipment top and is connected with blower unit, the bottom of plenum chamber and fluid bed is separated by by the flabellum dividing plate that polylith can rotate, interlaced and leave the slit between the every flabellum dividing plate, the top of air inducing chamber and fluid bed is separated by by porous barrier, on each hole of porous barrier cloth bag is installed, the degree of depth of cloth bag can reach 2/3 ~ 1/3 of fluidized bed height during stretching, extension;
Mixed material drops in the fluid bed of described spray-fluidized equipment from the bottom of fluid bed, drive air-supply arrangement air-supply and the rotation of flabellum dividing plate, make mixed material accelerate from bottom to top helical flow with malleation, drive simultaneously blower unit, air quantity by regulating blower unit and wind direction impose the pulse negative pressure to the top of described fluid bed and make a plurality of cloth bag up-down vibration on the described porous barrier and impact mixed material, make mixed material form tiny powder;
4. the multiple spot spray gun by the fluid bed sidewall with step 2. prepared mixed aqueous solution continuously spraying be distributed on the powder in the fluid bed, again by the hot blast continuous drying, obtain the dining table sugar powder;
5. add calcium silicates in the dining table sugar powder that 4. obtains to step, mix, discharging, pack namely gets described Sugarless mensal sugar.
2. the preparation method of a kind of Sugarless mensal sugar according to claim 1, it is characterized in that: the fluid bed of described spray-fluidized equipment is the cylinder column, and the height of fluid bed accounts for 1/2 ~ 2/3 of spray-fluidized device height.
3. the preparation method of a kind of Sugarless mensal sugar according to claim 1 is characterized in that: step 4. in, the wind pushing temperature of fluid bed is at 50 ~ 105 ℃.
4. the preparation method of a kind of Sugarless mensal sugar according to claim 3, it is characterized in that: step 4. in, when the mixed aqueous solution spraying disperseed, the wind pushing temperature of control fluid bed was at 50 ~ 80 ℃, and the wind pushing temperature of control fluid bed is at 80 ~ 105 ℃ during heated-air drying.
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Application publication date: 20130417 |