CN102952480B - Filter adhesive film containing nano calcium carbonate - Google Patents
Filter adhesive film containing nano calcium carbonate Download PDFInfo
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- CN102952480B CN102952480B CN2012104164995A CN201210416499A CN102952480B CN 102952480 B CN102952480 B CN 102952480B CN 2012104164995 A CN2012104164995 A CN 2012104164995A CN 201210416499 A CN201210416499 A CN 201210416499A CN 102952480 B CN102952480 B CN 102952480B
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- CN
- China
- Prior art keywords
- calcium carbonate
- adhesive film
- phenol
- filter
- nano
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 19
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 16
- 239000002313 adhesive film Substances 0.000 title claims abstract description 15
- 229960003563 Calcium Carbonate Drugs 0.000 title abstract 3
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims abstract description 13
- 239000002956 ash Substances 0.000 claims abstract description 13
- AHDSRXYHVZECER-UHFFFAOYSA-N 2,4,6-tris[(dimethylamino)methyl]phenol Chemical compound CN(C)CC1=CC(CN(C)C)=C(O)C(CN(C)C)=C1 AHDSRXYHVZECER-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- PPBRXRYQALVLMV-UHFFFAOYSA-N styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229920002367 Polyisobutene Polymers 0.000 claims abstract description 7
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 7
- -1 ether diol Chemical class 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 9
- BJZYYSAMLOBSDY-QMMMGPOBSA-N (2S)-2-butoxybutan-1-ol Chemical compound CCCCO[C@@H](CC)CO BJZYYSAMLOBSDY-QMMMGPOBSA-N 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 229920001971 elastomer Polymers 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 230000004048 modification Effects 0.000 claims description 6
- 238000006011 modification reaction Methods 0.000 claims description 6
- 229920001084 poly(chloroprene) Polymers 0.000 claims description 6
- 229920002223 polystyrene Polymers 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- XLOMVQKBTHCTTD-UHFFFAOYSA-N zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 6
- IJVRPNIWWODHHA-UHFFFAOYSA-M 2-cyanoprop-2-enoate Chemical compound [O-]C(=O)C(=C)C#N IJVRPNIWWODHHA-UHFFFAOYSA-M 0.000 claims description 3
- WNROFYMDJYEPJX-UHFFFAOYSA-K Aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 3
- KTWOOEGAPBSYNW-UHFFFAOYSA-N Ferrocene Chemical compound [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 claims description 3
- 239000006238 High Abrasion Furnace Substances 0.000 claims description 3
- OUBMGJOQLXMSNT-UHFFFAOYSA-N N-isopropyl-N'-phenyl-p-phenylenediamine Chemical compound C1=CC(NC(C)C)=CC=C1NC1=CC=CC=C1 OUBMGJOQLXMSNT-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- 239000005864 Sulphur Substances 0.000 claims description 3
- 229940014598 TAC Drugs 0.000 claims description 3
- KUAZQDVKQLNFPE-UHFFFAOYSA-N Thiram Chemical compound CN(C)C(=S)SSC(=S)N(C)C KUAZQDVKQLNFPE-UHFFFAOYSA-N 0.000 claims description 3
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 claims description 3
- IQPQWNKOIGAROB-UHFFFAOYSA-N [N-]=C=O Chemical compound [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 claims description 3
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 3
- 230000003712 anti-aging Effects 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000006229 carbon black Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 229920003211 cis-1,4-polyisoprene Polymers 0.000 claims description 3
- 239000007822 coupling agent Substances 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910001882 dioxygen Inorganic materials 0.000 claims description 3
- 239000003292 glue Substances 0.000 claims description 3
- UMKARVFXJJITLN-UHFFFAOYSA-N lead;phosphorous acid Chemical compound [Pb].OP(O)O UMKARVFXJJITLN-UHFFFAOYSA-N 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000002105 nanoparticle Substances 0.000 claims description 3
- 230000001264 neutralization Effects 0.000 claims description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 3
- 239000001069 triethyl citrate Substances 0.000 claims description 3
- 235000013769 triethyl citrate Nutrition 0.000 claims description 3
- 238000004073 vulcanization Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000011787 zinc oxide Substances 0.000 claims description 3
- 230000032683 aging Effects 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- YACLQRRMGMJLJV-UHFFFAOYSA-N Chloroprene Chemical compound ClC(=C)C=C YACLQRRMGMJLJV-UHFFFAOYSA-N 0.000 abstract 1
- 238000010292 electrical insulation Methods 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 1
- 229920000909 polytetrahydrofuran Polymers 0.000 abstract 1
- 238000000034 method Methods 0.000 description 6
- 238000001914 filtration Methods 0.000 description 4
- 238000010008 shearing Methods 0.000 description 4
- 239000000428 dust Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 230000003245 working Effects 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000001627 detrimental Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 238000004642 transportation engineering Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Abstract
The present invention discloses filter adhesive film containing nano calcium carbonate, which is prepared from the following raw materials: neoprene CR121, styrene, 2,4,6-tris(dimethylaminomethyl)phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutylene, polytetrahydrofuran ether diol, nano calcium carbonate, modified tree ashes and the like. The filter adhesive film is good in heat resistance, high in shear strength and excellent in electrical insulation and aging resistance. The adhesive film after curing is smooth in surface, and good in toughness and anti-seismic effect.
Description
Technical field
The present invention relates to the purifier apparatus field, is exactly a kind of adhesive film for filter that contains nano-calcium carbonate.
Background technology
Purifier is by the filtering to detrimental impurity originally, engine can be worked under various operating modes, and can reach rated wear.When the underproof product of filtration efficiency is used, can not can cause the engine premature wear of motor vehicle by the harmful dust impurity of engine is carried out to effective filtering, reduce work-ing life, the harm engine even leads to a disaster.
Adhesion process in production is not grasped, or the poor quality of tackiness agent own, thereby make between the filter paper of purifier and end cap, can not keep sealed state to make dust from gap, flowing through, thereby cause the purifier quality defective.The selection of filter paper and complete processing, filter paper adhesion process are two crucial qualifying points in the purifier Production Flow Chart.Some producer, in order to reduce production costs, purchases more cheap underproof filter paper and tackiness agent, or the bonding time is short, brush coating is very few or inhomogeneous etc., all can cause filtration efficiency defective.
Especially for air filter, its tackiness agent used with epoxy resin as main raw material, the tackiness agent of the type is fluid binder, before using, must fully stir, adopt again the methods such as pickling process, spraying method, spread coating, rolling method, transfer method to operate, therefore comparatively complicated on technique, be prone to adhesive distribution inhomogeneous and cause the phenomenon such as waste; And tackiness agent is very crisp, not shock-resistant after solidifying, in following process, transportation and installation process, be easy to damage, cause purifier short work-ing life.
Traditional rubber cement can not meet new requirement, is badly in need of the quality that the better rubber adhesive of performance improves purifier.
Summary of the invention
The object of the present invention is to provide a kind of adhesive film for filter that contains nano-calcium carbonate with higher consolidation strength and toughness.
Above-mentioned purpose realizes by following scheme:
A kind of adhesive film for filter that contains nano-calcium carbonate, it is characterized in that: it is that raw material by following weight parts makes: chloroprene rubber CR121 135-140, vinylbenzene 15-18, 2, 4, 6-tri-(dimethylamino methyl) phenol 1-2, polyvinyl alcohol 8-10, the N-2-(aminoethyl)-3-aminopropyl trimethoxysilane 2-3, polyisobutene 2-3, PTMG 2-3, cis-1, 4-polyisoprene rubber 5-10, isocyanate glue 5-10, triethyl citrate 2-5, epoxyoleic acid butyl ester 3-5, dibasic lead phosphite 1-2, sulphur 1.0-1.5, zinc oxide 1-2, Zinic stearas 3-4, anti-aging agent RD 1-2, antioxidant 4010NA 1-2, high abrasion furnace carbon black N330 62-65, titanate coupling agent TMC-TTS1-2, irgasfos 168 1-2, Silane coupling agent KH550 1-2, nano-calcium carbonate 25-35, Vulcanization accelerator TMTD 1-2, acceterator TE TD1-2, ferrocene 1-2, modification trees ashes 1-2,
The preparation method of described modification trees ashes is:
(1), by the trees ashes, be the dioxygen bubble of 15-20% after 2-3 hour by concentration, then with deionized water wash to neutral, dry;
(2), in the trees ashes, add 2 of the nano-sized carbon that is equivalent to its weight 2-3%, 1-2%, 4, the α-cyanoacrylate of 6-tri-(dimethylamino methyl) phenol, 2-3%, the linking agent TAC of 1-2%, the aluminium hydroxide of 3-5%, after under 4500-4800 rev/min, stirring 20-30 minute, ovendry power is broken into ultrafine powder and get final product.
Described a kind of adhesive film for filter that contains nano-calcium carbonate, it is characterized in that: the preparation method is: join by weight chloroprene rubber CR121 in vinylbenzene, be heated to 100-110 ℃, stir 10-15 minute, add by weight again 2,4,6-tri-(dimethylamino methyl) phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutene, PTMG, stir reaction 1-2 hour; Add by weight again all the other raw materials, mixing to desired thickness, finally be trimmed to desired size and get final product.
Beneficial effect of the present invention is: heat resistance of the present invention is good, shearing resistance has good electrical insulating property and ageing resistance in the time of high, and this adhesive film solidifies that rear surface is smooth, good toughness, anti seismic efficiency are good.
Embodiment
A kind of adhesive film for filter that contains nano-calcium carbonate, it is that raw material by following weight parts (kg) makes: chloroprene rubber CR121 140, vinylbenzene 18, 2, 4, 6-tri-(dimethylamino methyl) phenol 2, polyvinyl alcohol 10, the N-2-(aminoethyl)-3-aminopropyl trimethoxysilane 3, polyisobutene 3, PTMG 3, cis-1, 4-polyisoprene rubber 5, isocyanate glue 8, triethyl citrate 3, epoxyoleic acid butyl ester 4, dibasic lead phosphite 2, sulphur 1, zinc oxide 2, Zinic stearas 3, anti-aging agent RD 1, antioxidant 4010NA 2, high abrasion furnace carbon black N330 65, titanate coupling agent TMC-TTS2, irgasfos 168 1.5, Silane coupling agent KH550 1.5, nano-calcium carbonate 30, Vulcanization accelerator TMTD 1, acceterator TE TD1, ferrocene 1, modification trees ashes 2,
The preparation method of described modification trees ashes is:
(1), by the trees ashes, be 15% dioxygen bubble after 3 hours by concentration, then with deionized water wash to neutral, dry;
(2), in the trees ashes, add the nano-sized carbon that is equivalent to its weight 2%, 1% 2,4,6-tri-(dimethylamino methyl) phenol, 2% α-cyanoacrylate, 1% linking agent TAC, 4% aluminium hydroxide, after under 4800 rev/mins, stirring 25 minutes, ovendry power is broken into ultrafine powder and get final product.
Described a kind of adhesive film for filter that contains nano-calcium carbonate, the preparation method is: join by weight chloroprene rubber CR121 in vinylbenzene, be heated to 105 ℃, stirred 15 minutes, add by weight again 2,4,6-tri-(dimethylamino methyl) phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutene, PTMG, stir reaction 1-2 hour; Add by weight again all the other raw materials, mixing to desired thickness, finally be trimmed to desired size and get final product.
The adhesive film for filter that the present invention contains nano-calcium carbonate has higher shearing resistance and toughness, after using, the normal temperature shearing resistance can reach every square centimeter of 256-281 kilogram, the shearing resistance of 150 ℃ can reach every square centimeter of 108-120 kilogram, and uneven pulling intensity can reach every square centimeter of 51-54 kilogram.During use, film of the present invention is stained with to filter paper of filter and end cap, then in the sulfuration of heating, keeps sealed state, dust can not occur from gap, flowing through.Can greatly improve the bond strength of its toughness and rubber and filter paper, durable in use.
Claims (2)
1. adhesive film for filter that contains nano-calcium carbonate, it is characterized in that: it is that raw material by following weight parts makes: chloroprene rubber CR121 135-140, vinylbenzene 15-18, 2, 4, 6-tri-(dimethylamino methyl) phenol 1-2, polyvinyl alcohol 8-10, the N-2-(aminoethyl)-3-aminopropyl trimethoxysilane 2-3, polyisobutene 2-3, PTMG 2-3, cis-1, 4-polyisoprene rubber 5-10, isocyanate glue 5-10, triethyl citrate 2-5, epoxyoleic acid butyl ester 3-5, dibasic lead phosphite 1-2, sulphur 1.0-1.5, zinc oxide 1-2, Zinic stearas 3-4, anti-aging agent RD 1-2, antioxidant 4010NA 1-2, high abrasion furnace carbon black N330 62-65, titanate coupling agent TMC-TTS 1-2, irgasfos 168 1-2, Silane coupling agent KH550 1-2, nano-calcium carbonate 25-35, Vulcanization accelerator TMTD 1-2, acceterator TE TD 1-2, ferrocene 1-2, modification trees ashes 1-2,
The preparation method of described modification trees ashes is:
(1), by the trees ashes, be the dioxygen bubble of 15-20% after 2-3 hour by concentration, then with deionized water wash to neutral, dry;
(2), in the trees ashes, add 2 of the nano-sized carbon that is equivalent to its weight 2-3%, 1-2%, 4, the α-cyanoacrylate of 6-tri-(dimethylamino methyl) phenol, 2-3%, the linking agent TAC of 1-2%, the aluminium hydroxide of 3-5%, after under 4500-4800 rev/min, stirring 20-30 minute, ovendry power is broken into ultrafine powder and get final product.
2. a kind of adhesive film for filter that contains nano-calcium carbonate according to claim 1, it is characterized in that: the preparation method is: join by weight chloroprene rubber CR121 in vinylbenzene, be heated to 100-110 ℃, stir 10-15 minute, add by weight again 2,4,6-tri-(dimethylamino methyl) phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutene, PTMG, stir reaction 1-2 hour; Add by weight again all the other raw materials, mixing to desired thickness, finally be trimmed to desired size and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104164995A CN102952480B (en) | 2012-10-27 | 2012-10-27 | Filter adhesive film containing nano calcium carbonate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104164995A CN102952480B (en) | 2012-10-27 | 2012-10-27 | Filter adhesive film containing nano calcium carbonate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102952480A CN102952480A (en) | 2013-03-06 |
| CN102952480B true CN102952480B (en) | 2013-11-27 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012104164995A Active CN102952480B (en) | 2012-10-27 | 2012-10-27 | Filter adhesive film containing nano calcium carbonate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102952480B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106281114A (en) * | 2016-08-05 | 2017-01-04 | 蚌埠威尔特滤清器有限公司 | A kind of gasoline filter anticorrosion high-strength adhesive |
| CN106189929A (en) * | 2016-08-05 | 2016-12-07 | 蚌埠威尔特滤清器有限公司 | A kind of gasoline filter Thief zone binding agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101337179A (en) * | 2008-06-25 | 2009-01-07 | 浙江工业大学 | Method for extracting black carbon absorption material using plant ash as raw material |
| CN102504722A (en) * | 2011-11-21 | 2012-06-20 | 天长市通天化工有限责任公司 | Diatomite chloroprene type sealant |
| CN102504723A (en) * | 2011-11-21 | 2012-06-20 | 天长市通天化工有限责任公司 | Sericite neoprene sealant |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011011924A (en) * | 2009-06-30 | 2011-01-20 | Maruo Calcium Co Ltd | Calcium carbonate based filler for resin, covered with amorphous calcium phosphate and resin composition obtained by blending the filler |
-
2012
- 2012-10-27 CN CN2012104164995A patent/CN102952480B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101337179A (en) * | 2008-06-25 | 2009-01-07 | 浙江工业大学 | Method for extracting black carbon absorption material using plant ash as raw material |
| CN102504722A (en) * | 2011-11-21 | 2012-06-20 | 天长市通天化工有限责任公司 | Diatomite chloroprene type sealant |
| CN102504723A (en) * | 2011-11-21 | 2012-06-20 | 天长市通天化工有限责任公司 | Sericite neoprene sealant |
Non-Patent Citations (1)
| Title |
|---|
| JP特开2011-11924A 2011.01.20 |
Also Published As
| Publication number | Publication date |
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| CN102952480A (en) | 2013-03-06 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
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Owner name: ANHUI PHOENIX INTERNATIONAL CO., LTD. Free format text: FORMER NAME: BENGBU FENGHUANG FILTERS CO., LTD. |
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| CP01 | Change in the name or title of a patent holder |
Address after: 233000 Mount Huangshan Road, Bengbu high tech Zone, Anhui, No. 8028 Patentee after: ANHUI PHOENIX FILTER CO., LTD. Address before: 233000 Mount Huangshan Road, Bengbu high tech Zone, Anhui, No. 8028 Patentee before: Bengbu Fenghuang Filters Co., Ltd. |