CN102952478B - Filter adhesive film prepared by mixing neoprene and ethylene propylene diene monomer (EPDM) - Google Patents
Filter adhesive film prepared by mixing neoprene and ethylene propylene diene monomer (EPDM) Download PDFInfo
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- CN102952478B CN102952478B CN2012104164942A CN201210416494A CN102952478B CN 102952478 B CN102952478 B CN 102952478B CN 2012104164942 A CN2012104164942 A CN 2012104164942A CN 201210416494 A CN201210416494 A CN 201210416494A CN 102952478 B CN102952478 B CN 102952478B
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- rubber
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- terpolymer
- mixing
- filter
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- 239000002313 adhesive film Substances 0.000 title claims abstract description 16
- 238000002156 mixing Methods 0.000 title claims abstract description 7
- YACLQRRMGMJLJV-UHFFFAOYSA-N Chloroprene Chemical compound ClC(=C)C=C YACLQRRMGMJLJV-UHFFFAOYSA-N 0.000 title abstract 4
- 229920002943 EPDM rubber Polymers 0.000 title abstract 4
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims abstract description 13
- 239000002956 ash Substances 0.000 claims abstract description 13
- 239000000843 powder Substances 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 8
- PPBRXRYQALVLMV-UHFFFAOYSA-N styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229920002367 Polyisobutene Polymers 0.000 claims abstract description 7
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 7
- -1 ether diol Chemical class 0.000 claims abstract description 4
- 229920001084 poly(chloroprene) Polymers 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- 229920001897 terpolymer Polymers 0.000 claims description 16
- 229920001971 elastomer Polymers 0.000 claims description 13
- 238000010074 rubber mixing Methods 0.000 claims description 11
- FUIQBJHUESBZNU-UHFFFAOYSA-N 2-[(dimethylazaniumyl)methyl]phenolate Chemical compound CN(C)CC1=CC=CC=C1O FUIQBJHUESBZNU-UHFFFAOYSA-N 0.000 claims description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 9
- BJZYYSAMLOBSDY-QMMMGPOBSA-N (2S)-2-butoxybutan-1-ol Chemical compound CCCCO[C@@H](CC)CO BJZYYSAMLOBSDY-QMMMGPOBSA-N 0.000 claims description 6
- 230000003712 anti-aging Effects 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 6
- 230000004048 modification Effects 0.000 claims description 6
- 238000006011 modification reaction Methods 0.000 claims description 6
- 229920002223 polystyrene Polymers 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- IJVRPNIWWODHHA-UHFFFAOYSA-M 2-cyanoprop-2-enoate Chemical compound [O-]C(=O)C(=C)C#N IJVRPNIWWODHHA-UHFFFAOYSA-M 0.000 claims description 3
- VHOQXEIFYTTXJU-UHFFFAOYSA-N 2-methylbuta-1,3-diene;2-methylprop-1-ene Chemical class CC(C)=C.CC(=C)C=C VHOQXEIFYTTXJU-UHFFFAOYSA-N 0.000 claims description 3
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 claims description 3
- WNROFYMDJYEPJX-UHFFFAOYSA-K Aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 3
- TZCXTZWJZNENPQ-UHFFFAOYSA-L Barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 3
- 239000004593 Epoxy Substances 0.000 claims description 3
- KTWOOEGAPBSYNW-UHFFFAOYSA-N Ferrocene Chemical compound [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- 229940014598 TAC Drugs 0.000 claims description 3
- URAYPUMNDPQOKB-UHFFFAOYSA-N Triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 claims description 3
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 3
- 229960000892 attapulgite Drugs 0.000 claims description 3
- 229910052601 baryte Inorganic materials 0.000 claims description 3
- 239000010428 baryte Substances 0.000 claims description 3
- 229920005557 bromobutyl Polymers 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000006229 carbon black Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 239000004927 clay Substances 0.000 claims description 3
- 229910052570 clay Inorganic materials 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- HGQSXVKHVMGQRG-UHFFFAOYSA-N dioctyltin Chemical compound CCCCCCCC[Sn]CCCCCCCC HGQSXVKHVMGQRG-UHFFFAOYSA-N 0.000 claims description 3
- 229910001882 dioxygen Inorganic materials 0.000 claims description 3
- 239000000395 magnesium oxide Substances 0.000 claims description 3
- 239000002105 nanoparticle Substances 0.000 claims description 3
- 230000001264 neutralization Effects 0.000 claims description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims description 3
- 229910052625 palygorskite Inorganic materials 0.000 claims description 3
- JCVQKRGIASEUKR-UHFFFAOYSA-N triethoxy(phenyl)silane Chemical compound CCO[Si](OCC)(OCC)C1=CC=CC=C1 JCVQKRGIASEUKR-UHFFFAOYSA-N 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 235000003140 Panax quinquefolius Nutrition 0.000 claims 1
- 240000005373 Panax quinquefolius Species 0.000 claims 1
- 239000000853 adhesive Substances 0.000 abstract description 4
- 230000001070 adhesive Effects 0.000 abstract description 4
- 230000032683 aging Effects 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- AHDSRXYHVZECER-UHFFFAOYSA-N 2,4,6-tris[(dimethylamino)methyl]phenol Chemical compound CN(C)CC1=CC(CN(C)C)=C(O)C(CN(C)C)=C1 AHDSRXYHVZECER-UHFFFAOYSA-N 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000010292 electrical insulation Methods 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 1
- 239000000945 filler Substances 0.000 abstract 1
- 229920000909 polytetrahydrofuran Polymers 0.000 abstract 1
- 238000000034 method Methods 0.000 description 6
- 239000002131 composite material Substances 0.000 description 5
- 238000010008 shearing Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000003245 working Effects 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000002905 metal composite material Substances 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 238000004642 transportation engineering Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Abstract
The present invention discloses filter adhesive film prepared by mixing neoprene and EPDM, which is prepared from the following raw materials: neoprene CR121, styrene, 2,4,6-tris(dimethylaminomethyl)phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutylene, polytetrahydrofuran ether diol, modified tree ashes and the like. Through mixing neoprene and EPDM and adding compound powder as a filler, the filter adhesive film is good in heat resistance and high in adhesive strength, and excellent in electrical insulation and aging resistance. The adhesive film after curing is smooth in surface, good in toughness and good in anti-seismic effect.
Description
Technical field
The present invention relates to the purifier apparatus field, be exactly a kind of chloroprene rubber and terpolymer EP rubber mixing and adhesive film for filter.
Background technology
The selection of filter paper and complete processing, filter paper adhesion process are two crucial qualifying points in the purifier Production Flow Chart.Some producer, in order to reduce production costs, purchases more cheap underproof filter paper and tackiness agent, or the bonding time is short, brush coating is very few or inhomogeneous etc., all can cause filtration efficiency defective, thereby affect the work-ing life of purifier.
Especially for air filter, its tackiness agent that uses with epoxy resin as main raw material, the tackiness agent of the type is fluid binder, must fully stir before using, adopt again the methods such as pickling process, spraying method, spread coating, rolling method, transfer method to operate, therefore comparatively complicated on technique, be prone to adhesive distribution inhomogeneous and cause the phenomenon such as waste; And tackiness agent is very crisp, not shock-resistant after solidifying, and is easy to damage in following process, transportation and installation process, causes purifier short work-ing life.
In addition, develop rapidly along with rubber industry, rubber composite is widely used, in rubber and metal composite goods, the quality of tackiness agent is the key of composite product quality, along with increasing and the expansion of Application Areas of composite product kind, more and more harsher to the requirement of adhesive techniques.The technology such as traditional chlorinated rubber method, isocyanic ester method can not meet new requirement, need new tackiness agent to improve the quality of rubber composite product.
Traditional rubber cement can not meet new requirement, is badly in need of the better rubber adhesive of performance and improves the quality of purifier.
Summary of the invention
The object of the present invention is to provide a kind of chloroprene rubber with higher consolidation strength and toughness and terpolymer EP rubber mixing and adhesive film for filter.
Above-mentioned purpose realizes by following scheme:
a kind of chloroprene rubber and terpolymer EP rubber mixing and adhesive film for filter, it is characterized in that: it is that raw material by following weight parts makes: chloroprene rubber CR121 130-133, vinylbenzene 15-20, 2,4,6-three (dimethylamino methyl) phenol 1-2, polyvinyl alcohol 8-12, the N-2-(aminoethyl)-3-aminopropyl trimethoxysilane 2-3, polyisobutene 2-3, PTMG 2-3, terpolymer EP rubber 5-8, brominated butyl rubber BBK-232 8-12, Vanay 3-5, epoxy oleum lini 2-5, glycerol glycerinate 2-5, magnesium oxide 2-5, Imarcaptoacetate dioctyltin 1-2, attapulgite 15-20, nano barite powder 20-25, bauxitic clay powder 20-25, carbon black N339 10-15, 3-aminopropyl trimethoxysilane 1-2, irgasfos 168 1-2, phenyl triethoxysilane 1-2, silane coupling agent KH570 1-2, anti-aging agent ODA 1-2, anti-aging agent RD 1-2, 2-thiol group benzimidazolyl 1-2, accelerant CZ 1-2, accelerator CBS 0.5-1.5, ferrocene 1-2, modification trees ashes 1.3-2.1,
The preparation method of described modification trees ashes is:
(1), be the dioxygen bubble of 15-20% after 2-3 hour with the trees ashes with concentration, then with deionized water wash to neutral, oven dry;
(2), add 2 of the nano-sized carbon that is equivalent to its weight 2-3%, 1-2% in the trees ashes, 4, the α-cyanoacrylate of 6-three (dimethylamino methyl) phenol, 2-3%, the linking agent TAC of 1-2%, the aluminium hydroxide of 3-5%, after stirring 20-30 minute under 4500-4800 rev/min, ovendry power is broken into ultrafine powder and get final product.
Described a kind of chloroprene rubber and terpolymer EP rubber mixing and adhesive film for filter, it is characterized in that: the preparation method is: join by weight chloroprene rubber CR121 in vinylbenzene, be heated to 100-110 ℃, stir 10-15 minute, add by weight again 2,4,6-three (dimethylamino methyl) phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutene, PTMG, stir reaction 1-2 hour; Add by weight again all the other raw materials, mixing to desired thickness, be trimmed to finally desired size and get final product.
Beneficial effect of the present invention is: the present invention is mixing by chloroprene rubber and terpolymer EP rubber, add composite powder as weighting agent, make heat resistance of the present invention good, have good electrical insulating property and ageing resistance when shearing resistance is high, and this adhesive film solidifies that rear surface is smooth, good toughness, anti seismic efficiency are good.
Embodiment
a kind of chloroprene rubber and terpolymer EP rubber mixing and adhesive film for filter, it is that raw material by following weight parts (kg) makes: chloroprene rubber CR121 133, vinylbenzene 20, 2, 4, 6-three (dimethylamino methyl) phenol 2, polyvinyl alcohol 12, the N-2-(aminoethyl)-3-aminopropyl trimethoxysilane 3, polyisobutene 2, PTMG 3, terpolymer EP rubber 5, brominated butyl rubber BBK-232 12, Vanay 3, epoxy oleum lini 5, glycerol glycerinate 2, magnesium oxide 5, Imarcaptoacetate dioctyltin 2, attapulgite 20, nano barite powder 25, bauxitic clay powder 25, carbon black N339 15, 3-aminopropyl trimethoxysilane 2, irgasfos 168 2, phenyl triethoxysilane 1, silane coupling agent KH570 2, anti-aging agent ODA 2, anti-aging agent RD 2, 2-thiol group benzimidazolyl 1, accelerant CZ 2, accelerator CBS 1.5, ferrocene 2, modification trees ashes 2.1,
The preparation method of described modification trees ashes is:
(1), be 15% dioxygen bubble after 3 hours with the trees ashes with concentration, then with deionized water wash to neutral, oven dry;
(2), add in the trees ashes nano-sized carbon that is equivalent to its weight 2%, 1% 2,4,6-three (dimethylamino methyl) phenol, 2% α-cyanoacrylate, 1% linking agent TAC, 4% aluminium hydroxide, after stirring 25 minutes under 4800 rev/mins, ovendry power is broken into ultrafine powder and get final product.
Described a kind of chloroprene rubber and terpolymer EP rubber mixing and adhesive film for filter, the preparation method is: join by weight chloroprene rubber CR121 in vinylbenzene, be heated to 105 ℃, stirred 15 minutes, add by weight again 2,4,6-three (dimethylamino methyl) phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutene, PTMG, stir reaction 1-2 hour; Add by weight again all the other raw materials, mixing to desired thickness, be trimmed to finally desired size and get final product.
Chloroprene rubber of the present invention and terpolymer EP rubber mixing and adhesive film for filter have higher shearing resistance and toughness, after using, the normal temperature shearing resistance can reach 260 kilograms every square centimeter of 250-, the shearing resistance of 150 ℃ can reach 100-110 kilograms every square centimeter, and uneven pulling intensity can reach every square centimeter of 50-53 kilogram.
During use, film of the present invention is stained with filter paper of filter and end cap,, then in the sulfuration of heating, keeps sealed state, dust can not occur flow through in gap.Can greatly improve the bond strength of its toughness and rubber and filter paper, durable in use.
Claims (3)
- a chloroprene rubber and terpolymer EP rubber mixing and adhesive film for filter, it is characterized in that: it is that raw material by following weight parts makes: chloroprene rubber CR121 130-133, vinylbenzene 15-20, 2,4,6-three (dimethylamino methyl) phenol 1-2, polyvinyl alcohol 8-12, the N-2-(aminoethyl)-3-aminopropyl trimethoxysilane 2-3, polyisobutene 2-3, PTMG 2-3, terpolymer EP rubber 5-8, brominated butyl rubber BBK-232 8-12, Vanay 3-5, epoxy oleum lini 2-5, glycerol glycerinate 2-5, magnesium oxide 2-5, Imarcaptoacetate dioctyltin 1-2, attapulgite 15-20, nano barite powder 20-25, bauxitic clay powder 20-25, carbon black N339 10-15, 3-aminopropyl trimethoxysilane 1-2, irgasfos 168 1-2, phenyl triethoxysilane 1-2, silane coupling agent KH570 1-2, anti-aging agent ODA 1-2, anti-aging agent RD 1-2, 2-thiol group benzimidazolyl 1-2, accelerant CZ 1-2, accelerator CBS 0.5-1.5, ferrocene 1-2, modification trees ashes 1.3-2.1,The preparation method of described modification trees ashes is:(1), be the dioxygen bubble of 15-20% after 2-3 hour with the trees ashes with concentration, then with deionized water wash to neutral, oven dry;(2), add 2 of the nano-sized carbon that is equivalent to its weight 2-3%, 1-2% in the trees ashes, 4, the α-cyanoacrylate of 6-three (dimethylamino methyl) phenol, 2-3%, the linking agent TAC of 1-2%, the aluminium hydroxide of 3-5%, after stirring 20-30 minute under 4500-4800 rev/min, ovendry power is broken into ultrafine powder and get final product.
- A kind of chloroprene rubber according to claim 1 and terpolymer EP rubber mixing and adhesive film for filter, it is characterized in that: the preparation method is: join by weight chloroprene rubber CR121 in vinylbenzene, be heated to 100-110 ℃, stir 10-15 minute, add by weight 2 again, 4,6-three (dimethylamino methyl) phenol, polyvinyl alcohol, N-2-(aminoethyl)-3-aminopropyl trimethoxysilane, polyisobutene, PTMG, stir reaction 1-2 hour; Add by weight again all the other raw materials, mixing to desired thickness, be trimmed to finally desired size and get final product.
- A kind of chloroprene rubber according to claim 1 and terpolymer EP rubber mixing and adhesive film for filter, it is characterized in that: described terpolymer EP rubber is German bright Sheng 5962.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104164942A CN102952478B (en) | 2012-10-27 | 2012-10-27 | Filter adhesive film prepared by mixing neoprene and ethylene propylene diene monomer (EPDM) |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104164942A CN102952478B (en) | 2012-10-27 | 2012-10-27 | Filter adhesive film prepared by mixing neoprene and ethylene propylene diene monomer (EPDM) |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102952478A CN102952478A (en) | 2013-03-06 |
| CN102952478B true CN102952478B (en) | 2013-11-13 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012104164942A Active CN102952478B (en) | 2012-10-27 | 2012-10-27 | Filter adhesive film prepared by mixing neoprene and ethylene propylene diene monomer (EPDM) |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103601991A (en) * | 2013-10-28 | 2014-02-26 | 安徽东方金河精密机械制造有限公司 | Novel environment protective sealing ring for capacitor and preparation method thereof |
| CN104086902B (en) * | 2014-07-02 | 2016-04-27 | 合肥市再德高分子材料有限公司 | A kind of automobile high-temperature resistant rubber sealing-ring |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101033298A (en) * | 2006-03-09 | 2007-09-12 | 廊坊开发区深思博远新材料技术有限公司 | Coiled material with environmental protection function and use thereof |
| CN102229785A (en) * | 2011-05-13 | 2011-11-02 | 秦琪航 | Adhesive film for filter |
| CN102277105A (en) * | 2011-08-10 | 2011-12-14 | 佛山市豹王滤芯制造有限公司 | High-temperature resistant adhesive for filter cleaner of automobile |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7589145B2 (en) * | 2004-04-15 | 2009-09-15 | Exxonmobil Chemical Patents Inc. | Syndiotactic rich polyolefins |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101033298A (en) * | 2006-03-09 | 2007-09-12 | 廊坊开发区深思博远新材料技术有限公司 | Coiled material with environmental protection function and use thereof |
| CN102229785A (en) * | 2011-05-13 | 2011-11-02 | 秦琪航 | Adhesive film for filter |
| CN102277105A (en) * | 2011-08-10 | 2011-12-14 | 佛山市豹王滤芯制造有限公司 | High-temperature resistant adhesive for filter cleaner of automobile |
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| CN102952478A (en) | 2013-03-06 |
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Owner name: ANHUI PHOENIX INTERNATIONAL CO., LTD. Free format text: FORMER NAME: BENGBU FENGHUANG FILTERS CO., LTD. |
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Address after: 233000 Mount Huangshan Road, Bengbu high tech Zone, Anhui, No. 8028 Patentee after: ANHUI PHOENIX FILTER CO., LTD. Address before: 233000 Mount Huangshan Road, Bengbu high tech Zone, Anhui, No. 8028 Patentee before: Bengbu Fenghuang Filters Co., Ltd. |