CN102871868B - Massage mask-facial cleanser combination - Google Patents
Massage mask-facial cleanser combination Download PDFInfo
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- CN102871868B CN102871868B CN201210178072.6A CN201210178072A CN102871868B CN 102871868 B CN102871868 B CN 102871868B CN 201210178072 A CN201210178072 A CN 201210178072A CN 102871868 B CN102871868 B CN 102871868B
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- massage pack
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Abstract
The invention relates to a massage mask-facial cleanser combination which is characterized in that spreadability of foam is good, the foam is easy to wash away, the use feel is good and the foam is of good quality even at low temperature. The combination contains 92-97 weight percent water-solubility aerosol stoste and 3-8 weight percent liquefied petroleum gas; carbon dioxide is pressurized to 0.4-0.7MPa at a temperature of 25 degrees; and the water-solubility aerosol stoste contains 1-5 weight percent higher alcohol formed by docosyl alcohol and cetanol, 3-8 weight percent higher aliphatic acid formed by the docosyl alcohol and stearic acid, and 1-4 weight percent nonionic surfactant formed by Phytosterols and cithrol.
Description
Technical field
The present invention relates to massage face-washing composition, more specifically, the present invention relates to the massage pack face-washing composition that can spray with blister.
Background technology
As foam-form face-washing material, patent documentation 1 has proposed the material of washing one's face by the alveolar substance exquisiteness forming containing aqueous solution, liquefied petroleum gas, the carbon dioxide of anion surfactant.Patent documentation 2,3, has proposed the blister facial film material that contains the polyhydric alcohol such as a large amount of Polyethylene Glycol or glycerol.
Patent documentation 1: No. 2010-94476, Japanese Patent Application
Patent documentation 2: clear No. 61-158909 of Japanese Patent Application
Patent documentation 3: No. 2005-2030, TOHKEMY
But, for patent documentation 1, although because alveolar substance is fine and smooth and it is good to sprawl, be suitable as foaming mousse cleanser, so because alveolar substance is soft unsatisfactory with material as massage.For the technology of patent documentation 2 and 3, although owing to containing the polyhydric alcohol such as more than 50% Polyethylene Glycol or glycerol, good to the adhesion of skin, be not easy but then to wash off, need to use large water gaging.
Summary of the invention
The inventor conducts in-depth research in order to address the above problem.Found that a kind of massage pack face-washing composition, said composition contains water solublity aerosol stock solution 92-97 % by weight and liquefied petroleum gas 3-8 % by weight, and at 25 ℃, be pressurized to 0.4-0.7MPa with carbon dioxide, wherein water solublity aerosol stock solution contains the higher alcohol 1-5 % by weight consisting of behenyl alcohol and hexadecanol, the higher fatty acids 3-8 % by weight that behenic acid and stearic acid form, the non-ionic surface active agent 1-4 % by weight that polyoxyethylene sterol and cithrol form, this massage pack compositions can be injected into blister, spreadability to skin is good, and can simply wash off, thereby completed the present invention.
That is to say, the invention provides following massage pack face-washing composition.
1. a massage pack face-washing composition, said composition contains water solublity aerosol stock solution 92-97 % by weight and liquefied petroleum gas 3-8 % by weight, and at 25 ℃, be pressurized to 0.4-0.7MPa with carbon dioxide, wherein water solublity aerosol stock solution contains the non-ionic surface active agent 1-4 % by weight that higher fatty acids 3-8 % by weight, polyoxyethylene sterol and cithrol that the higher alcohol 1-5 % by weight, behenic acid and the stearic acid that consist of behenyl alcohol and hexadecanol form form.
2. a massage pack face-washing composition, wherein, the proportioning of aforementioned behenyl alcohol and hexadecanol is 80: 20-60: 40
3. a massage pack face-washing composition, wherein, aforementioned behenic acid and stearic proportioning are 80: 20-60: 40.
4. the massage pack face-washing composition as described in 1, wherein, the proportioning of polyoxyethylene sterol and cithrol is 20: 80-40: 60.
Below massage pack face-washing composition of the present invention is specifically described.
The higher alcohol using in the present invention, can enumerate behenyl alcohol and hexadecanol.Can mix and use these two kinds of alcohol, use level is the 1-5 % by weight of aqueous aerosol solution, is preferably 2-4 % by weight.Proportioning is 80: 20-60: 40, be preferably 70: 30-65: 35.When the proportioning of hexadecanol is less than 20%, steeped softly, be difficult to obtain massage effect, in addition, if proportioning surpasses 40%, steep really up to the mark, unsatisfactory as massage pack use material.
The higher fatty acids using in the present invention, can enumerate behenic acid and stearic acid.Can mix and use these two kinds of acid, the use level in water solublity aerosol solution is 3-8 % by weight, is preferably 4-6 % by weight.Proportioning is 80: 20-60: 40, be preferably 70: 30-65: 35.When stearic use level is less than 20%, steeped softly, be difficult to obtain massage effect, in addition, if proportioning surpasses 40%, steep really up to the mark, unsatisfactory as massage use material.
The non-ionic surface active agent using in the present invention, can enumerate polyoxyethylene sterol and cithrol.More specifically, as polyoxyethylene sterol, can enumerate PEG-5 soyasterol, PEG-10 soyasterol, PEG-20 soyasterol, PEG-30 soyasterol, particularly preferably PEG-10 soyasterol.In addition, as cithrol, can enumerate polyethylene glycol laurate, Myrj 45, polyoxyethylene oleate, polyoxyethylene distearate, polyoxyethylene diisopstearate, particularly preferably Myrj 45.Can mix two kinds in these, use level is preferably the aerocolloidal 1-4 % by weight of water solublity, more preferably 2-3 % by weight.Proportioning is 20: 80-40: 60, be preferably 30: 70-35: 65.When the use level of polyoxyethylene sterol is less than 20%, it is large that foaming becomes, unsatisfactory with material as massage pack, in addition, if surpass 40%, steep really up to the markly, as massage pack, uses material unsatisfactory.
Liquefied petroleum gas in the present invention, can enumerate such as propane, normal butane, iso-butane, isopentane etc., wherein the mixture of preferably propane, normal butane, iso-butane.Preferred content is 3-8 % by weight, more preferably 4-6 % by weight.If content is less than 3 % by weight, alveolar substance variation, in addition, if surpass 8 % by weight, foams and becomes large, can not form fine and smooth bubble.
Even if coordinating the object of carbon dioxide in the present invention is to use as the auxiliary agent that also can spray content when low temperature, because the dissolubility with respect to aqueous stock solution is excellent, thereby preferably.Preferably its content is to be pressurized to 0.4-0.7MPa at 25 ℃, is more preferably pressurized to 0.5-0.6MPa.If be less than 0.4MPa at 25 ℃, when low temperature, sometimes can not be injected into finally, in addition, if surpass 0.7MPa, spray intensity excessive, undesirable in the use.
The pH of water solublity aerosol stock solution of the present invention is preferably 4.0-7.0, more preferably 5.0-6.5.If pH is less than 4.0, likely corrode aerocolloidal canister, if surpass 7.0, pH, approach alkalescence, skin is produced and stimulated.
In massage pack face-washing composition of the present invention, except above-mentioned necessary component, other conventional ingredients that use in can also suitably coordinating cosmetics in the scope of not damaging effect of the present invention, such as wetting agent, antiseptic, pH adjusting agent, viscosity modifier, antioxidant, freshener, antibacterial, essence, pigment etc.
The specific embodiment
Below, the embodiment of massage pack face-washing composition of the present invention is described, but the present invention is not limited to these embodiment.
Embodiment 1-2 and comparative example 1-5
Composition modulation massage face-washing composition according to shown in following table 1, is filled into respectively in aluminum aerosol container.According to the hardness of following evaluation methodology evaluation (1) bubble, the spreadability of (2) bubble, (3) are the property washed off easily, bubble hardness during (4) low temperature.Its evaluation result is as shown in table 1.Unit in embodiment and comparative example is % by weight.
Table 1
| Embodiment 1 | Embodiment 2 | Comparative example 1 | Comparative example 2 | Comparative example 3 | |
| Behenyl alcohol | 2 | 1.6 | 2 | 4 | 2 |
| Hexadecanol | 1 | 0.4 | 0.2 | 2 | 1 |
| Stearic acid | 1.5 | 1.2 | 1.5 | 1.5 | 0.5 |
| Behenic acid | 3 | 4.8 | 3 | 3 | 3 |
| PEG-10 soyasterol | 1 | 0.4 | 1 | 1 | 1 |
| Stearic acid PEG-25 | 2 | 1.6 | 2 | 2 | 2 |
| Potassium hydroxide | 0.5 | 0.6 | 0.5 | 0.5 | 0.5 |
| Water | 89 | 89.4 | 89.8 | 86 | 90 |
| Liquefied petroleum gas | 5 | 4 | 5 | 5 | 5 |
| With carbon dioxide pressurization (MPa) | 0.6 | 0.5 | 0.6 | 0.6 | 0.6 |
| (1) result | ○ | ○ | △ | × | △ |
| (2) result | ○ | ○ | △ | × | △ |
| (3) result | ○ | ○ | ○ | △ | △ |
| (4) result | ○ | ○ | △ | △ | △ |
| Comparative example 4 | Comparative example 5 | Comparative example 6 | Comparative example 7 | Comparative example 8 | |
| Behenyl alcohol | 2 | 2 | 2 | 2 | 2 |
| Hexadecanol | 1 | 1 | 1 | 1 | 1 |
| Stearic acid | 5 | 1.5 | 1.5 | 1.5 | 1.5 |
| Behenic acid | 3.5 | 3 | 3 | 3 | 3 |
| PEG-10 soyasterol | 1 | 0.5 | 2.5 | 1 | 1 |
| Stearic acid PEG-25 | 2 | 2.5 | 2.5 | 2 | 2 |
| Potassium hydroxide | 0.5 | 0.5 | 0.5 | 0.5 | 0.5 |
| Water | 86 | 89 | 87 | 89 | 89 |
| Liquefied petroleum gas | 5 | 5 | 5 | 2 | 5 |
| With carbon dioxide pressurization (MPa) | 0.6 | 0.6 | 0.6 | 0.6 | 0.2 |
| (1) result | × | △ | × | △ | × |
| (2) result | × | △ | △ | × | △ |
| (3) result | × | ○ | × | ○ | ○ |
| (4) result | × | △ | △ | △ | × |
Evaluation methodology:
The wash one's face key property evaluation experimental of material of massage pack carries out as follows: uses 10 experimenters to carry out actual massage pack and wash one's face, the spreadability of then evaluating the hardness of bubble, steeping when whole face is sprawled, the easiness of washing off.By the following minute standard of each getting, calculated, average mark is zero more than 2.1 being evaluated as, and average mark is evaluated as △ at 1.1-2.0, average mark being evaluated as below 1.0 *.Test temperature is the room temperature of 25 ± 2 ℃.In addition, also evaluated the blister state (range estimation) under 5 ℃ of low temperature.
(1) hardness of bubble
3: good
2: general
1: undesirable (crossing soft or really up to the mark)
(2) spreadability of bubble
3: good
2: general
1: undesirable
(3) the easy property washed off
3: good
2: general
1: undesirable
(4) the bubble hardness of test chamber temperature at 5 ℃
3: good
2: general
1: undesirable
Massage pack face-washing composition of the present invention is bubble spreadability the and easily property washed off use sense is good, even also good massage pack face-washing composition of alveolar substance at low temperatures.
Claims (16)
1. a massage pack face-washing composition, said composition contains water solublity aerosol stock solution 92-97 % by weight and liquefied petroleum gas 3-8 % by weight, and at 25 ℃, be pressurized to 0.4-0.7MPa with carbon dioxide, wherein water solublity aerosol stock solution contains the non-ionic surface active agent 1-4 % by weight that higher fatty acids 3-8 % by weight, polyoxyethylene sterol and cithrol that the higher alcohol 1-5 % by weight, behenic acid and the stearic acid that consist of behenyl alcohol and hexadecanol form form; The proportioning of described behenyl alcohol and hexadecanol is 80:20-60:40; Described behenic acid and stearic proportioning are 80:20-60:40; The proportioning of described polyoxyethylene sterol and cithrol is 20:80-40:60.
2. massage pack face-washing composition as claimed in claim 1, wherein, the proportioning of described behenyl alcohol and hexadecanol is 70:30-65:35.
3. massage pack face-washing composition as claimed in claim 1, wherein, described behenic acid and stearic proportioning are 70:30-65:35.
4. massage pack face-washing composition as claimed in claim 1, wherein, the proportioning of described polyoxyethylene sterol and cithrol is 30:70-35:65.
5. massage pack face-washing composition as claimed in claim 1, wherein, water solublity aerosol stock solution contains the higher alcohol 2-4 % by weight consisting of behenyl alcohol and hexadecanol.
6. massage pack face-washing composition as claimed in claim 1, wherein, it is 4-6 % by weight that water solublity aerosol stock solution contains the higher fatty acids that behenic acid and stearic acid form.
7. massage pack face-washing composition as claimed in claim 1, wherein, described polyoxyethylene sterol is selected from PEG-5 soyasterol, PEG-10 soyasterol, PEG-20 soyasterol, PEG-30 soyasterol.
8. massage pack face-washing composition as claimed in claim 7, described polyoxyethylene sterol is PEG-10 soyasterol.
9. massage pack face-washing composition as claimed in claim 1, wherein, described cithrol is selected from polyethylene glycol laurate, Myrj 45, polyoxyethylene oleate, polyoxyethylene distearate, polyoxyethylene diisopstearate.
10. massage pack face-washing composition as claimed in claim 9, wherein, described cithrol is selected from Myrj 45.
11. massage pack face-washing compositions as claimed in claim 1, wherein, the non-ionic surface active agent 2-3 % by weight that described water solublity aerosol stock solution contains polyoxyethylene sterol and cithrol formation.
12. massage pack face-washing compositions as claimed in claim 1, wherein, described liquefied petroleum gas is selected from propane, normal butane, iso-butane, isopentane or its mixture.
13. massage pack face-washing compositions as claimed in claim 1, wherein, compositions contains liquefied petroleum gas 4-6 % by weight.
14. massage pack face-washing compositions as claimed in claim 1, wherein, described compositions is pressurized to 0.5-0.6MPa with carbon dioxide at 25 ℃.
15. massage pack face-washing compositions as claimed in claim 1, wherein, the pH of water solublity aerosol stock solution is 4.0-7.0.
16. massage pack face-washing compositions as claimed in claim 15, wherein, the pH of water solublity aerosol stock solution is 5.0-6.5.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2011169634A JP2013023493A (en) | 2011-07-15 | 2011-07-15 | Composition for facial massage pack cleanser |
| JP2011-169634 | 2011-07-15 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102871868A CN102871868A (en) | 2013-01-16 |
| CN102871868B true CN102871868B (en) | 2014-04-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210178072.6A Active CN102871868B (en) | 2011-07-15 | 2012-05-24 | Massage mask-facial cleanser combination |
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| Country | Link |
|---|---|
| JP (1) | JP2013023493A (en) |
| CN (1) | CN102871868B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102394637B1 (en) * | 2015-09-30 | 2022-05-09 | (주)아모레퍼시픽 | Aerosol type composition for preventing hair loss or promoting hair growth |
| JP6645814B2 (en) * | 2015-11-24 | 2020-02-14 | 株式会社マンダム | Foam skin cleanser |
| WO2018221420A1 (en) * | 2017-05-30 | 2018-12-06 | 株式会社マンダム | Foamed skin cleanser |
| CN109095419B (en) * | 2018-06-21 | 2021-04-20 | 上海西西艾尔启东日用化学品有限公司 | Carbon dioxide aerosol manufacturing system and process |
| JP7427742B2 (en) * | 2021-10-29 | 2024-02-05 | 株式会社長寿乃里 | Composition for skin pack and method for using the same |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101554356A (en) * | 2008-04-11 | 2009-10-14 | 花王株式会社 | A spumous skin coating agent |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10144061A1 (en) * | 2001-09-07 | 2003-04-17 | Beiersdorf Ag | Self-foaming or foam-like preparations with inorganic gel formers, organic hydrocolloids and particulate hydrophobic and / or hydrophobized and / or oil-absorbing solid substances |
| US20080031908A1 (en) * | 2006-07-25 | 2008-02-07 | L'oreal | Oily cosmetic composition in aerosol form |
-
2011
- 2011-07-15 JP JP2011169634A patent/JP2013023493A/en not_active Withdrawn
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- 2012-05-24 CN CN201210178072.6A patent/CN102871868B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101554356A (en) * | 2008-04-11 | 2009-10-14 | 花王株式会社 | A spumous skin coating agent |
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| Publication number | Publication date |
|---|---|
| JP2013023493A (en) | 2013-02-04 |
| CN102871868A (en) | 2013-01-16 |
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