CN109095419B - Carbon dioxide aerosol manufacturing system and process - Google Patents

Carbon dioxide aerosol manufacturing system and process Download PDF

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Publication number
CN109095419B
CN109095419B CN201810645213.8A CN201810645213A CN109095419B CN 109095419 B CN109095419 B CN 109095419B CN 201810645213 A CN201810645213 A CN 201810645213A CN 109095419 B CN109095419 B CN 109095419B
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Prior art keywords
carbon dioxide
gas
pressure
stock solution
filling
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CN109095419A (en
Inventor
孙志勇
王爱军
王璐
朱爱军
徐满康
孙裕梁
楚国涛
陶元
段晶晶
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Shanghai Xixiaier Qidong Daily Chemical Articles Co ltd
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Shanghai Xixiaier Qidong Daily Chemical Articles Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B67OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67CCLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
    • B67C3/00Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
    • B67C3/02Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B67OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67CCLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
    • B67C3/00Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
    • B67C3/02Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
    • B67C3/22Details

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  • Containers And Packaging Bodies Having A Special Means To Remove Contents (AREA)
  • Cosmetics (AREA)
  • Vacuum Packaging (AREA)

Abstract

The invention provides a carbon dioxide aerosol manufacturing process, which is characterized by comprising the following steps: filling carbon dioxide gas into the aluminum tank stock solution filled with the LPG gas in a quantitative and constant pressure manner; wherein the filling pressure of the carbon dioxide is larger than the inner pressure of the aluminum tank stock solution containing LPG gas. The present invention fills gaseous carbon dioxide into a closed pressure-resistant container filled with effective components through special equipment and a process, and makes partial carbon dioxide combine with water in the original solution to form carbonic acid. Meanwhile, carbon dioxide in the gas phase and carbon dioxide in the solution form a gas-liquid balance, so that the purpose that the product can be used for a long time and is effective finally is achieved.

Description

Carbon dioxide aerosol manufacturing system and process
Technical Field
The invention relates to the field of cosmetic filling, in particular to a carbon dioxide aerosol manufacturing system and a carbon dioxide aerosol manufacturing process.
Background
The main reason is that carbonic acid molecules are easily decomposed into carbon dioxide and water, the carbon dioxide molecules are small and are very easy to be absorbed through skin, carbon dioxide absorbed through skin can enter capillary vessels, and the carbon dioxide entering the capillary vessels can obviously promote blood circulation of the capillary vessels and increase blood flow. In addition, part of oxygen in the blood is replaced by carbon dioxide entering capillary vessels and then enters the surface layer of the skin, and the oxygen can achieve the effect of increasing the oxidation resistance of the skin by promoting the activation of cells.
However, no cosmetics containing carbonic acid exist in the current Chinese market, and the main reason is that carbonic acid is an unstable system and is seriously influenced by the environmental temperature, the higher the temperature is, the lower the density of carbon dioxide is, and the lower the environmental temperature is, the higher the density of carbon dioxide is, so that under the common process conditions, the filling amount of carbon dioxide is difficult to control, the filling amount of products is relatively unstable every time, and if the consistency of carbon dioxide filling of all products cannot be ensured, the quality difference of the products is overlarge.
Disclosure of Invention
The present invention aims at overcoming the said defect and filling gaseous carbon dioxide quantitatively into sealed pressure container with filled effective component to combine partial carbon dioxide with water in the original solution to form carbonic acid. Meanwhile, carbon dioxide in the gas phase and carbon dioxide in the solution form a gas-liquid balance, so that the product can be used for a long time and is effective finally.
The invention provides a carbon dioxide aerosol manufacturing system for manufacturing a cosmetic containing carbonic acid, which is characterized in that:
the cosmetic stock solution sequentially passes through an aluminum can stock solution filling unit, an LPG gas filling unit, a carbon dioxide gas filling unit and a sealing/packaging unit to realize the manufacture of aerosol;
the aluminum can stock solution filling unit comprises an aluminum can stock solution filling machine for filling and sealing the cosmetic stock solution;
the LPG gas filling unit comprises LPG injecting equipment for injecting LPG gas into an aluminum tank containing cosmetic stock solution;
the carbon dioxide gas filling unit comprises carbon dioxide flushing equipment, and carbon dioxide gas is quantitatively pressed into an aluminum tank containing LPG gas under the condition of constant temperature;
the water bath unit performs water bath leak detection on the aluminum tank;
the above-mentioned closing and packaging unit performs closing and packaging of the aluminum can.
Further, the invention provides a carbon dioxide aerosol manufacturing system, which also has the following characteristics: namely, the carbon dioxide flushing and injecting unit comprises carbon dioxide flushing and injecting equipment and a flushing and injecting channel;
wherein, the carbon dioxide flushing equipment comprises a carbon dioxide gas tank and a pressure reducing valve;
the first port of the pressure reducing valve is communicated with the air supply end of the carbon dioxide gas tank;
the second port of the pressure reducing valve is communicated with the injection channel, and a constant temperature device is arranged on the second port of the pressure reducing valve.
Further, the invention provides a carbon dioxide aerosol manufacturing system, which also has the following characteristics: that is, the filling pressure of the carbon dioxide is higher than the internal pressure of the aluminum tank containing LPG gas.
Further, the invention provides a carbon dioxide aerosol manufacturing system, which also has the following characteristics: namely, the pressure in the aluminum tank after injecting LPG gas is 0.4-0.5 MPa.
Further, the invention provides a carbon dioxide aerosol manufacturing system, which also has the following characteristics: namely, the flushing pressure of the carbon dioxide gas is 3 to 5 times of the pressure in the aluminum can.
Further, the invention provides a carbon dioxide aerosol manufacturing system, which also has the following characteristics: namely, a weighing device is arranged between the aluminum tank stock solution filling unit and the LPG gas filling unit;
and/or
A weighing device is arranged between the LPG gas filling unit and the carbon dioxide gas filling unit;
and/or
A weighing device is provided between the carbon dioxide gas filling unit and the closing/packaging unit.
So that the weight of the product can be controlled at various stages or at designated stages.
Further, the invention provides a carbon dioxide aerosol manufacturing system, which also has the following characteristics: that is, the above-mentioned closing/packaging unit includes an automatic nozzle adding machine, an automatic capping machine, and a packaging machine.
In addition, the invention also provides a manufacturing process of the carbon dioxide aerosol, which is characterized by comprising the following steps: filling carbon dioxide gas into the aluminum tank stock solution filled with the LPG gas in a quantitative and constant pressure manner;
wherein the filling pressure of the carbon dioxide is higher than the inner pressure of the aluminum tank stock solution containing LPG gas.
Further, the above carbon dioxide aerosol manufacturing process also has the following characteristics: namely, the outputted carbon dioxide gas is subjected to constant temperature treatment.
The invention has the following functions and effects:
the present invention fills gaseous carbon dioxide into a closed pressure-resistant container filled with effective components through special equipment and a process, and makes partial carbon dioxide combine with water in the original solution to form carbonic acid. Meanwhile, carbon dioxide in the gas phase and carbon dioxide in the solution form a gas-liquid balance, so that the purpose that the product can be used for a long time and is effective finally is achieved.
The invention solves the problems that the prior carbon dioxide cannot ensure the stability of the filling amount of the carbon dioxide when being filled into a pressure-containing sealed container (filled with LPG gas), and the using effect of the product cannot be ensured because the content of carbonic acid generated by each bottle of the product is inconsistent, and the CO is additionally provided with a constant temperature heater2The gas density changes due to the change of the environmental temperature, so that the consistency of the filling amount can be controlled by controlling the flow and the flow rate; meanwhile, the phenomenon of temperature reduction and ice accumulation of the pressure reducing valve caused by long-time mass gas delivery can be prevented, and the normal work of an adjusting mechanism of the adjusting valve is ensured, so that the constant temperature of the filled carbon dioxide is ensured, the specific gravity of all the carbon dioxide is consistent, and the safety of the product can be ensured.
Regarding the amount of carbon dioxide gas to be injected, the amount of carbon dioxide gas to be injected is controlled by the injection flow rate and the injection time, and the amount of carbon dioxide gas to be injected is preferably such that the pressure in the tube body after the injection is completed reaches 0.5 to 1Mpa, and under the pressure condition, the cosmetic stock solution and the carbon dioxide gas can be fully mixed and simultaneously reach a gas-liquid equilibrium state.
Drawings
Fig. 1 is a schematic view of a carbon dioxide aerosol production system according to an embodiment.
Detailed Description
As shown in fig. 1, the cosmetic stock solution is subjected to aluminum tank stock solution filling, LPG gas filling, carbon dioxide gas filling and online weighing, then is sent into water bath leakage detection equipment for leakage detection, rejected unqualified products are added with an injection head through an automatic nozzle adding machine, and then enters a packaging production line for outer packaging coating through an automatic capping machine.
In the process of filling carbon dioxide gas, as LPG gas is filled in the product, the product has certain pressure (0.4-0.5MPa) and simultaneously the filling amount of carbon dioxide is ensured, and the CO is filled in a high-pressure volume mode of more than 0.5MPa, so that CO is filled2The gas is quantitatively filled into the product containing pressure to make CO2The gas forms carbonic acid (CO) with water in the product2+H2O=H2CO3)。
To ensure gas stability and controllability of the charge during this flushing, CO2The gas in the steel cylinder passes through the pressure reducing valve at the output pressure of 5.0MPa to control the output gas pressure to be about 1.8MPa, and the constant temperature heater is additionally arranged at the outlet of the pressure reducing valve, so that CO is generated2The output proportion/density of constant, no longer receive ambient temperature or output temperature's influence, the relief pressure valve cooling that prevents simultaneously that a large amount of conveying gas from arousing for a long time from long-time long-pending ice, and then the governing valve adjustment mechanism who leads to loses effect, has still solved gas conveying's potential safety hazard problem. Precision), the filling precision of the carbon dioxide of the product is ensured.

Claims (9)

1. A carbon dioxide aerosol production system for producing a cosmetic containing carbonic acid, characterized in that:
the cosmetic stock solution sequentially passes through an aluminum tank stock solution filling unit, an LPG gas filling unit, a carbon dioxide gas filling unit, a water bath unit and a sealing and packaging unit to realize the manufacture of the aerosol;
the aluminum can stock solution filling unit comprises an aluminum can stock solution filling machine for filling and sealing the cosmetic stock solution;
the LPG gas filling unit comprises LPG injecting equipment, and LPG gas is injected into an aluminum tank containing a cosmetic stock solution;
the carbon dioxide gas filling unit comprises carbon dioxide flushing equipment, and carbon dioxide gas is quantitatively pressed into an aluminum tank containing LPG gas under the condition of constant temperature;
the water bath unit performs water bath leak detection on the aluminum tank;
the sealing and packaging unit is used for sealing and packaging the aluminum can;
in the process of quantitatively pressing the carbon dioxide gas into the aluminum tank containing the LPG gas under the condition of constant temperature, the output carbon dioxide gas is subjected to constant temperature treatment to ensure that CO is generated2The output specific gravity/density of (a) is constant.
2. A carbon dioxide aerosol manufacturing system according to claim 1, wherein:
the carbon dioxide gas filling unit comprises carbon dioxide flushing and injecting equipment and a flushing and injecting channel;
wherein the carbon dioxide flushing device comprises a carbon dioxide gas tank and a pressure reducing valve;
the first port of the pressure reducing valve is communicated with the air supply end of the carbon dioxide gas tank;
and a second port of the pressure reducing valve is communicated with the injection channel, and a constant temperature device is arranged on the second port of the pressure reducing valve.
3. A carbon dioxide aerosol manufacturing system according to claim 1, wherein:
the pressure in the aluminum tank after the LPG gas is injected is 0.4-0.5 MPa.
4. A carbon dioxide aerosol manufacturing system according to claim 1, wherein:
the carbon dioxide filling pressure is greater than the internal pressure of the aluminium tank containing LPG gas.
5. A carbon dioxide aerosol manufacturing system according to claim 1, wherein:
the flushing pressure of the carbon dioxide gas is 3-5 times of the pressure in the aluminum tank.
6. A carbon dioxide aerosol manufacturing system according to claim 1, wherein:
a weighing device is arranged between the aluminum tank stock solution filling unit and the LPG gas filling unit;
and/or
A weighing device is arranged between the LPG gas filling unit and the carbon dioxide gas filling unit;
and/or
A weighing device is arranged between the carbon dioxide gas filling unit and the closing and packaging unit.
7. A carbon dioxide aerosol manufacturing system according to claim 1, wherein:
the sealing and packaging unit comprises an automatic nozzle adding machine, an automatic capping machine and a packaging machine.
8. A manufacturing process for the carbon dioxide aerosol manufacturing system according to any one of claims 1 to 7, characterized in that: filling carbon dioxide gas into the aluminum tank stock solution filled with the LPG gas in a quantitative and constant pressure manner;
wherein the filling pressure of the carbon dioxide is larger than the inner pressure of the aluminum tank stock solution containing LPG gas.
9. The process of manufacturing a carbon dioxide aerosol manufacturing system according to claim 8, wherein:
and carrying out constant temperature treatment on the output carbon dioxide gas.
CN201810645213.8A 2018-06-21 2018-06-21 Carbon dioxide aerosol manufacturing system and process Active CN109095419B (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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CN109095419B true CN109095419B (en) 2021-04-20

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Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8921337D0 (en) * 1989-09-21 1989-11-08 Glaxo Group Ltd Method and apparatus
US5535790A (en) * 1994-06-24 1996-07-16 Hirz; Donald J. Pressurized can filling apparatus
JP2013023493A (en) * 2011-07-15 2013-02-04 Nisshin Kagaku Kk Composition for facial massage pack cleanser
JP2017125004A (en) * 2015-05-29 2017-07-20 花王株式会社 Aerosol Cosmetic
KR20170035293A (en) * 2015-09-22 2017-03-30 (주)투어멀린나노텍 A buble equip
JP6738141B2 (en) * 2015-11-24 2020-08-12 株式会社マンダム Aerosol cosmetics
JP6605983B2 (en) * 2016-02-16 2019-11-13 花王株式会社 Aerosol skin treatment
KR101880057B1 (en) * 2016-05-10 2018-07-19 (주)화니핀코리아 Hair care cosmetic composition containing Chojeong carbonated water for hair loss prevention
JP2017114915A (en) * 2017-03-30 2017-06-29 花王株式会社 Aerosol cosmetics
CN107510621B (en) * 2017-10-10 2019-09-20 珀莱雅化妆品股份有限公司 It is a kind of for makeup removing without Water blown aerosol
CN108066162A (en) * 2018-02-11 2018-05-25 中山市天图精细化工有限公司 A kind of use in personal care slow-release perfume aerosol and preparation method thereof

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