CN108066162A - A kind of use in personal care slow-release perfume aerosol and preparation method thereof - Google Patents
A kind of use in personal care slow-release perfume aerosol and preparation method thereof Download PDFInfo
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- CN108066162A CN108066162A CN201810142640.4A CN201810142640A CN108066162A CN 108066162 A CN108066162 A CN 108066162A CN 201810142640 A CN201810142640 A CN 201810142640A CN 108066162 A CN108066162 A CN 108066162A
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- Prior art keywords
- personal care
- release
- preparation
- aerosol
- slow
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/0279—Porous; Hollow
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B61/00—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages
- B65B61/26—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages for marking or coding completed packages
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/22—Details
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Abstract
The present invention relates to aerosol spray technique fields, and in particular to a kind of use in personal care slow-release perfume aerosol and preparation method thereof, the aerosol includes：Solvent, aromatic release fragrant solidifying pearl, fixastive, emollient and propellant.The slow long-acting release fragrance of perfume aerosol energy of the present invention, has excellent stability.
Description
Technical field
The present invention relates to aerosol spray technique fields, and in particular to a kind of use in personal care slow-release perfume aerosol and its system
Preparation Method.
Background technology
Perfume is a kind of liquid for being used for generating pleasant smell, is taken from flowers and plants plant or organic synthesis object.Perfume
Quality except related with perfume ingredient, the selection of solvent and evaporation rate more directly determine the quality of perfume.
Existing perfume products, as solvent, save cost, dissolubility is good, but the presence of ethyl alcohol easily triggers mostly using ethyl alcohol
The problems such as allergy, and ethyl alcohol has extremely strong volatility, it is easy to the aromatic in taking away perfume in volatilization deposits perfume
The persistence of storage and fragrance all has a significant impact.Meanwhile existing perfume preparation process is only the originals such as physical mixed aromatic, solvent
Material, fragrance will scatter and disappear, it is necessary to which Reusability, makes troubles to user in the short time completely after use.In order to obtain
Long-acting perfume, also someone is made into solid perfume to reach this purpose, although relatively long fragrance remaining time can be reached,
But solid perfume contacts directly human skin surface, it may be polluted, and solid perfume is to cure essence absorption
In agent, fragrance is long not as good as the fragrance liquid gracefulness with formula, it is impossible to be experienced well to user.
The Chinese patent application of Publication No. CN103405357B discloses a kind of preparation process of long-acting slow-release perfume, should
Perfume is made of sustained release solvent, citric acid and perfume mixture, mixes in proportion raw material to obtain the final product.The invented technology is simple,
It can significantly improve the duration of fragrance, but the ingredient containing thickening property in the sustained release agent that uses of the invention, easily cause essence
It is scattered uneven, and colloidal solution can be formed under cryogenic.
Therefore, for above-mentioned technical problem, it is necessary to provide a kind of perfume aerosol that can slowly discharge fragrance longer
Agent and preparation method thereof.
The content of the invention
The present invention develops a kind of use in personal care slow-release perfume aerosol, the defects of overcoming the prior art, provides
A kind of use in personal care slow-release perfume aerosol and preparation method thereof.
Technical problem of the present invention is realized by following technical scheme：A kind of use in personal care slow-release perfume aerosol,
Contain solvent, aromatic in the aerosol, release fragrant solidifying pearl, fixastive, emollient and propellant；
Further, the mass ratio (w/w) of each component is as follows in the aerosol：Solvent 10%~20%, aromatic 6~
12%th, fragrant solidifying pearl 0.2~1%, fixastive 0.01~0.1%, emollient 1~5% are released, remaining is propellant；
Further, the mass ratio (w/w) of each component is as follows in the aerosol：Solvent 10%~20%, aromatic 6~
12%th, fragrant solidifying pearl 0.5~1%, fixastive 0.01~0.05%, emollient 3~5% are released, remaining is propellant.
Further, the one kind or two of the solvent in ultra-pure water, phthalic acid ester and cyclosiloxane polymer
Kind or more, preferred cyclosiloxane polymer；
Further, the cyclosiloxane polymer is DX-6031 cyclosiloxane polymer, is bought in Guangzhou chemical industry prosperous greatly
Limited starting material company.
Further, D001-CC large apertures cation exchange resin is purchased from Chemical Plant of Nankai Univ..
Further, the aromatic is selected from lemon extract, grapefruit flavours, cream jasmin france, bergamot essence, rhodamine toner
One or more of oil, Cypress ethereal oil, refined jasmine oil and cherry essence mixed liquor, but the invention is not limited in the example above
Scope；
Further, it is described release fragrant solidifying pearl preparation process be：
The preparation of S1, modified gelatin：Configuration quality fraction is 5%~10% aqueous gelatin solution, and room temperature storing 1 is molten when small
50 DEG C of heating water bath dissolvings after swollen, when the nitrine niacin formyl reaction 2 of addition gelatin quality 1/10 is small, mixed liquor quenching,
Vacuum drying to get；
S2, the preparation for releasing fragrant solidifying pearl：Modified gelatin and maltodextrin are taken with 1:2 ratio mixing, it is ultrapure to add in 5 times of volumes
Water, adjust pH to 4.5, naturally precipitation microencapsulated form coagulate pearl to get.
Further, the fixastive be selected from one or both of Moschus, liquid storax, rosalin and vanillic aldehyde with
On, preferred vanillic aldehyde；
Further, the emollient is selected from isopropyl myristate, sorbitan fatty acid ester and stearic acid polyoxy
It is more than one or both of vinyl acetate, preferred isopropyl myristate；
Further, the propellant is selected from difluoromethane, nitrogen, F-11, HFO-1234ze, pharmaceutical grade two
It more than one or both of methyl ether, compressed air, HFA 134a and cosmetics-stage liquefied petroleum gas, preferably makes up
Grade liquefied petroleum gas；
Correspondingly, the present invention also provides a kind of method for preparing above-mentioned aerosol, comprise the following steps：
A the preparation of fragrant solidifying pearl) is released：The preparation of modified gelatin：Configuration quality fraction is 5%~10% aqueous gelatin solution,
50 DEG C of heating water baths dissolvings after swelling when room temperature storing 1 is small, when the nitrine niacin formyl reaction 2 of addition gelatin quality 1/10 is small,
Mixed liquor quenching, be dried in vacuo to get；Modified gelatin and maltodextrin are taken with 1:2 ratio mixing, adds in 5 times of volumes
Ultra-pure water, adjust pH to 4.5, naturally precipitation microencapsulated form coagulate pearl to get；
B) the preparation of agent liquid：The accurate each component substance for weighing formulation content, by solvent, aromatic, fixastive and moisturizing
Agent all adds in mixing kettle and mixes slowly to uniform state；Stirring at low speed mixed raw material, while addition is released fragrant solidifying pearl and is stirred to equal
It is even, stand storage after detection is qualified；
C) product is filling：By step B) during the agent liquid that is prepared poured by bottle placer in tank, sealing, filling is cast
Agent, water-bath detection, tank bottom penetrate code, install nozzle, install outer cover, packaging cartonning to get.
Use in personal care slow-release perfume aerosol disclosed by the invention, which employs, to be released fragrant solidifying pearl aromatic is wrapped up, is inhaled
It receives, gelatin is modified by nitrine niacin formyl, and nitrine niacin formyl substitutes the amino on its side chain, obtains cationic structural, change
Property after cationic structural gelatin and maltodextrin when adding in ultra-pure water in acid condition, due to charge effect, modified gelatin
With maltodextrin molecular skeleton scion grafting, tiny capsules are precipitated in solution naturally, compared to gelatin plus water self-assembling formation with the solid of hole
Gel.Solidifying pearl prepared by this method is hollow tiny capsules, can adsorb aromatic package wherein, maltodextrin is in capsule
It can also play the role of swelling volume in forming process, the tiny capsules to be formed is enable to adsorb more aromatic, glue obtained
Capsule watchcase has elasticity, and spraying will not crush immediately to human skin and garment surface, when it rubs with clothes, limbs
Solidifying pearl rupture, releases the aromatic included, achievees the purpose that long-acting, slow release fragrance.
Compared with prior art, advantageous effect of the present invention is：
(1) perfume aerosol provided by the invention not spirituosity, it is non-stimulated to skin using flexible polymer as solvent
Property, it is safe, it can long-time service；
(2) it is with the addition of in perfume aerosol provided by the invention and releases fragrant solidifying pearl, is hollow microcapsule, is wrapped in fragrance
Agent can rupture to discharge fragrance with human action, achieve the purpose that long-acting, slow release fragrance；
(3) perfume aerosol provided by the invention is packed using tank body, enough preserves perfume more lasting, while using more
Add conveniently, be more easy to grasp dosage, be not easy to pollute.
Specific embodiment
The present invention is illustrated below by embodiment, following non-limiting embodiments are the preferred embodiments of the present invention,
In the case without departing from the scope of the present invention, the variation of the present embodiment is various.
1~3 use in personal care slow-release perfume aerosol component of the embodiment of the present invention and its proportioning (part)
Preparation method：
A the preparation of fragrant solidifying pearl) is released：
The preparation of S1, modified gelatin：Configuration quality fraction is 5% aqueous gelatin solution, when room temperature storing 1 is small 50 after swelling
The dissolving of DEG C heating water bath, add in gelatin quality 1/10 nitrine niacin formyl reaction 2 it is small when, mixed liquor quenching, vacuum is done
It is dry to get；
S2, the preparation for releasing fragrant solidifying pearl：Modified gelatin and maltodextrin are taken with 1:2 ratio mixing, it is ultrapure to add in 5 times of volumes
Water, adjust pH to 4.5, naturally precipitation microencapsulated form coagulate pearl to get；
B) the preparation of agent liquid：The accurate each component substance for weighing formulation content, by solvent, aromatic, fixastive and moisturizing
Agent all adds in mixing kettle and mixes slowly to uniform state；Stirring at low speed mixed raw material, while addition is released fragrant solidifying pearl and is stirred to equal
It is even, stand storage after detection is qualified；
C) product is filling：By step B) during the agent liquid that is prepared poured by bottle placer in tank, sealing, filling is cast
Agent, water-bath detection, tank bottom penetrate code, install nozzle, install outer cover, packaging cartonning to get.
1 use in personal care slow-release perfume aerosol of comparative example
Difference with embodiment 1 is step A) it releases fragrant solidifying pearl and is made by modified gelatin, other are the same as embodiment 1.
2 use in personal care slow-release perfume aerosol of comparative example
Difference with embodiment 1 is step A) it releases fragrant solidifying pearl and is made by maltodextrin, other are the same as embodiment 1.
Test example 1, release rate experiment
The rate of release of 1-3 of the embodiment of the present invention and comparative example 1-2 perfume being prepared is tested, is calculated public
Formula：(ct2-ct1)/ct1× 100% (wherein c expression fragrance concentrations, t2And t1Represent current and last minute point), as a result
It is as shown in the table.
1 result of the test of table
From table 1 it follows that perfume lasting fragrance made from 1-3 of the embodiment of the present invention and release slowly it is uniform, each
The release of period fragrance is uniform, and lingering fragrance is also left after 2 days, and the interior energy when preceding 24 is small of comparative example 1 and 2 keeps more stable fragrance
Rate of release, but when 24-40 is small between fragrance rate of release start significantly to decline, and less than 48 it is small when fragrance just release
Finish.
The above content is the preferred embodiment of the present invention, it is impossible to assert that the specific implementation of the present invention is only limited to these and says
It is bright, it should be pointed out that：For those of ordinary skill in the art, without departing from the principle of the present invention, can also do
Go out several improvements and modifications, these improvements and modifications also should be regarded as protection scope of the present invention.
Claims (9)
1. a kind of use in personal care slow-release perfume aerosol, it is characterised in that：The mass ratio (w/w) of each component in the aerosol
It is as follows：Solvent 10%~20%, aromatic 6~12% release fragrant solidifying pearl 0.2~1%, fixastive 0.01~0.1%, emollient 1
~5% and the propellant of surplus.
2. use in personal care slow-release perfume aerosol according to claim 1, it is characterised in that：Each group in the aerosol
The mass ratio (w/w) divided is as follows：Solvent 10%~20%, aromatic 6~12% release fragrant solidifying pearl 0.5~1%, fixastive 0.01
~0.05%, emollient 3~5% and the propellant of surplus.
3. use in personal care slow-release perfume aerosol according to claim 1, it is characterised in that：The solvent is selected from super
It is more than one or both of pure water, phthalic acid ester and cyclosiloxane polymer.
4. use in personal care slow-release perfume aerosol according to claim 1, it is characterised in that：The aromatic is selected from
Lemon extract, grapefruit flavours, cream jasmin france, bergamot essence, Rosa Damascana, Cypress ethereal oil, refined jasmine oil and cherry essence
One or more of.
5. use in personal care slow-release perfume aerosol according to claim 1, it is characterised in that：The perfume of releasing coagulates pearl
Preparation process is：
The preparation of S1, modified gelatin：Configuration quality fraction is 5%~10% aqueous gelatin solution, when room temperature storing 1 is small after swelling
50 DEG C of heating water bath dissolvings, when the nitrine niacin formyl reaction 2 of addition gelatin quality 1/10 is small, mixed liquor quenching, vacuum
It is dry to get；
S2, the preparation for releasing fragrant solidifying pearl：Modified gelatin and maltodextrin are taken with 1:2 ratio mixing, adds in 5 times of volume ultra-pure waters,
Adjust pH to 4.5, naturally precipitation microencapsulated form coagulate pearl to get.
6. use in personal care slow-release perfume aerosol according to claim 1, it is characterised in that：The fixastive is selected from
It is more than one or both of Moschus, liquid storax, rosalin and vanillic aldehyde.
7. use in personal care slow-release perfume aerosol according to claim 1, it is characterised in that：The emollient is selected from
It is more than one or both of isopropyl myristate, sorbitan fatty acid ester and polyoxyethylene stearic acid ester.
8. use in personal care slow-release perfume aerosol according to claim 1, it is characterised in that：The propellant is selected from
Difluoromethane, nitrogen, F-11, HFO-1234ze, medical grade dimethyl ether, compressed air, 1,1,1,2- tetrafluoroethane
With it is more than one or both of cosmetics-stage liquefied petroleum gas.
9. a kind of method prepared according to any use in personal care slow-release perfume aerosol of claim 1~9, special
Sign is：Comprise the following steps：
A the preparation of fragrant solidifying pearl) is released：The preparation of modified gelatin：Configuration quality fraction be 5%~10% aqueous gelatin solution, room temperature
Put 1 it is small when swelling after the dissolving of 50 DEG C of heating water baths, add in gelatin quality 1/10 nitrine niacin formyl reaction 2 it is small when, mixing
Liquid quenching, vacuum drying；Modified gelatin and maltodextrin are taken with 1:2 ratio mixing, adds in 5 times of volume ultra-pure waters, adjusts
Save pH to 4.5, naturally precipitation microencapsulated form coagulate pearl to get；
B) the preparation of agent liquid：The accurate each component substance for weighing formulation content is complete by solvent, aromatic, fixastive and emollient
Portion adds in mixing kettle and mixes slowly to uniform state；Stirring at low speed mixed raw material, while addition is released fragrant solidifying pearl and is stirred until homogeneous, and examines
Storage is stood after surveying qualification；
C) product is filling：By step B) during the agent liquid that is prepared poured by bottle placer in tank, sealing fills propellant, water
Bath detection, tank bottom penetrate code, install nozzle, install outer cover, packaging cartonning to get.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810142640.4A CN108066162A (en) | 2018-02-11 | 2018-02-11 | A kind of use in personal care slow-release perfume aerosol and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810142640.4A CN108066162A (en) | 2018-02-11 | 2018-02-11 | A kind of use in personal care slow-release perfume aerosol and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108066162A true CN108066162A (en) | 2018-05-25 |
Family
ID=62155153
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810142640.4A Pending CN108066162A (en) | 2018-02-11 | 2018-02-11 | A kind of use in personal care slow-release perfume aerosol and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN108066162A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109095419A (en) * | 2018-06-21 | 2018-12-28 | 上海西西艾尔启东日用化学品有限公司 | A kind of carbon dioxide-containing mist agent manufacture system and technique |
| CN111434356A (en) * | 2019-01-11 | 2020-07-21 | 广东阜和实业有限公司 | Slow-release air freshener and preparation method thereof |
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| CN102002441A (en) * | 2010-12-08 | 2011-04-06 | 倪美华 | Plant balm for improving physical and mental harmonious degree and preparation method thereof |
| CN102488624A (en) * | 2011-12-13 | 2012-06-13 | 中山市天图精细化工有限公司 | Petroleum jelly aerosol compositions for personal care |
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2018
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| CN101296710A (en) * | 2005-11-01 | 2008-10-29 | 雷克特本克斯尔(英国)有限公司 | Aerosol composition and method |
| CN102002441A (en) * | 2010-12-08 | 2011-04-06 | 倪美华 | Plant balm for improving physical and mental harmonious degree and preparation method thereof |
| CN102488624A (en) * | 2011-12-13 | 2012-06-13 | 中山市天图精细化工有限公司 | Petroleum jelly aerosol compositions for personal care |
| CN102698307A (en) * | 2012-06-20 | 2012-10-03 | 桑达化工（南通）有限公司 | Air refreshing aerosol |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109095419A (en) * | 2018-06-21 | 2018-12-28 | 上海西西艾尔启东日用化学品有限公司 | A kind of carbon dioxide-containing mist agent manufacture system and technique |
| CN111434356A (en) * | 2019-01-11 | 2020-07-21 | 广东阜和实业有限公司 | Slow-release air freshener and preparation method thereof |
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Application publication date: 20180525 |
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