CN102805973A - Water filter material, producing process of water filter material and corresponding water filter device - Google Patents
Water filter material, producing process of water filter material and corresponding water filter device Download PDFInfo
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- CN102805973A CN102805973A CN2012103251958A CN201210325195A CN102805973A CN 102805973 A CN102805973 A CN 102805973A CN 2012103251958 A CN2012103251958 A CN 2012103251958A CN 201210325195 A CN201210325195 A CN 201210325195A CN 102805973 A CN102805973 A CN 102805973A
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Abstract
The invention belongs to the technical field of daily life, and particularly relates to a drinking water filter material, a producing process of the filter material, and a corresponding water filter device. The water filter material is formed by powder of a sintering filter component and powder of pottery clay, wherein the filter component at least comprises a substance with positive and negative radicals in water. With the adoption of the technical scheme, PH of purified water can be adjusted to be alkalescent; the water filter material has bacteriostasis and sterilization functions, can release macroelements such as potassium, sodium, calcium, magnesium and phosphorus as well as microelements such as zinc, iron, selenium, copper, strontium, iodine, fluorine and metasilicic acid that are helpful for human bodies, can generate hydroxyl ions and hydronium ions, and can improve the immunity of the human bodies to harmful substances and natural healing ability of the human bodies; and generated anions can be used for reducing water molecular groups, thereby being convenient for the human bodies to absorb water molecules and the microelements.
Description
Technical field
The invention belongs to the daily life technical field, design a kind of drinking water filtering material and preparation technology thereof and corresponding water filtering device especially.
Background technology
Water is Source of life, and the mankind have left water and just can't survive.Along with The development in society and economy and people improve constantly the requirement of living standard, the requirement of drinking water is also improved constantly.But; Contain in the natural water much to person detrimental microorganisms; And along with the continuous development of industry, a large amount of industrial refuses also causes severe contamination to the water source that the mankind depend on for existence, and these water sources that polluted of long-term drinking can cause great injury to human beings'health.
At present, the drinking water of municipal administration supply has all passed through purified treatment, and the processing method of being taked has coarse filtration and counter-infiltration technology of fine filtering usually.The coarse filtration water technology can only carry out simple process to water; Its advantage is to remove large granular impurity, bacterium and the virus in the water; And microorganism, having kept in the water healthy and helpful mineral matter and trace element, the pH value of purifying waste water after the filtration is alkalescent; The shortcoming of coarse filtration technology is to remove impurity such as the chemical pollutant that contains in the water, heavy metal, and the security of water can not get guaranteeing.The advantage of counter-infiltration Fine Filtration Technology is and can carries out fine processing to water; The large granular impurity that contains in the water, bacterium, virus, microorganism and 96% above impurity such as heavy metal can be filtered; The pure safety of water quality, shortcoming are not contain any material in the water basically, particularly can be filtered out simultaneously healthy and helpful mineral matter and trace element; Pure water pH value after the filtration is faintly acid; The pure water that this faintly acid of long-term drinking does not contain mineral matter and trace element can cause the physique acidification, and disappearance mineral matter and trace element can cause damage to the health of health in the health.At present, the municipal tap water is contained more impurity usually, like bleaching powder of remnants etc., just can drink after need boiling; And commercially available pure water adopts the counter-infiltration Fine Filtration Technology to handle more, wherein lacks necessary mineral matter of human body and trace element, can not make the pH value of pure water be alkalescent simultaneously.
A lot of drinking water filtering materials are also arranged in the prior art, though have the function that water purifies, mineralization ability a little less than, and the pH regulating power is poor, can't regulate water pH value to alkalescent.In order to satisfy the demand of people better to healthy water use, just need a kind of functions such as purification, mineralising that both had on the market, can regulate pure water pH value again and be weakly alkaline filtering material, to remedy the deficiency that prior art exists.
Summary of the invention
For solving the problem that exists in the above-mentioned prior art; The purpose of this invention is to provide a kind of have water purification, mineralization function; And can regulate water pH value to weakly alkaline drinking water filtering material and preparation technology thereof with use the water filtering device of said water filtration material.
For realizing above-mentioned purpose, the present invention provides following technical scheme
The water filtration material is formed by the powder that filters component and the powder sintering of kaolin, wherein, comprises chitin in the said filtration component.
Described water filtration material, wherein, said filtration component also comprises at least aly can produce the material with the atomic group of positive and negative electricity in water.
Described water filtration material wherein, also comprises at least a material that can produce hydroxidion or hydrogen ion in the said filtration component, make water form small-micelle water.
Described water filtration material, wherein: the said material that can in water, produce with the atomic group of positive and negative electricity is the medical stone powder, and the said material that can produce hydroxidion or hydrogen ion is a tourmaline powdery thing.
Described water filtration material; Wherein, said water filtration material is that the powder sintering with chitin, wooden fish stone, medical stone, tourmaline, kaolin forms, and the shared percentage by weight of each component is respectively: chitin 20-40%; Wooden fish stone 5-25%; Medical stone 5-25%, tourmaline 15-40%, kaolin 10-15%.
Described water filtration material, wherein, the shared percentage by weight of said each component is: chitin 30%, wooden fish stone 15%, medical stone 15%, tourmaline 30%, kaolin 10%.
Described water filtration material, wherein, the granular size of said chitin, wooden fish stone, medical stone, tourmaline, kaolin powder is the 80-300 order, described water filtration material sinters the spherical of 2-8mm into.
The preparation technology of described water filtration material comprises step:
1), chitin, wooden fish stone, medical stone, tourmaline, kaolin are put into ball mill respectively be crushed to 80-300 purpose powder, for use;
2), be chitin 20-40% according to percentage by weight, wooden fish stone 5-25%, medical stone 5-25%, tourmaline 15-40%, the ratio of kaolin 10-15% is put into mixer with the powder for preparing in the step 1) and stirred, and is for use;
3), to step 2) in add pure water in the compound after stirring, stirring makes it become material-mud, for use;
4), the material-mud for preparing in the step 3) is processed the sphere material of diameter 2-8mm through marble forming machine, oven dry, for use;
5), the sphere material for preparing in the step 4) put into 1000-1200 ℃ high temperature furnace heated roasting 2-3 hour, the cooling of ceasing fire can be come out of the stove and processed finished product.
The percentage by weight of each component is a chitin 30% preparation technology of described water filtration material, wherein: step 2), wooden fish stone 15%, medical stone 15%, tourmaline 30%, kaolin 10%.
Water filtering device comprises the shell with entrance and exit, wherein: above-mentioned water filtration material is set in the said shell.
(3) beneficial effect: technical scheme provided by the invention discloses a kind of water filtration material and preparation technology thereof, corresponding water treatment facilities.When pure water during through water filtration material provided by the present invention; The water filtration material can discharge calcium carbonate in pure water, can increase calcium ion content in the water, regulates the pure water pH value and is alkalescent; Has antibacterial, sterilizing function; Release produces hydroxidion and two kinds of anions of hydrogen ion to trace elements such as the useful potassium of human body, sodium, calcium, magnesium, phosphorus macroelement and zinc, iron, selenium, copper, strontium, iodine, fluorine, metasilicic acids, can improve resistance and the natural curability of human body to harmful substance; Utilize the anion that produces to dwindle water clusters, be convenient to absorption of human body hydrone and trace element.
The specific embodiment
Below in conjunction with preferred embodiment the present invention is explained further details.
Embodiment one
A kind of drinking water filtering material is formed by the powder that filters component and the powder sintering of kaolin, and wherein, said filtration component comprises at least a kind ofly can produce the material with the atomic group of positive and negative electricity in water.
Described water filtration material wherein, also comprises the material that can produce hydroxidion or hydrogen ion in the said filtration component, makes water form small-micelle water.
Described water filtration material, wherein, the said material that can in water, produce with the atomic group of positive and negative electricity is the medical stone powder, the said material that can produce hydroxidion or hydrogen ion is a tourmaline powdery thing.
Described water filtration material, wherein, its component comprises the powder of chitin, wooden fish stone, medical stone, tourmaline, kaolin, the powder of above-mentioned component is processed spherical back by marble forming machine formed by high temperature sintering.
Said chitin be a kind of from the shell of crustaceans such as shrimp shell, crab shell, shell, extract powder; Have restraining and sterilizing bacteria, antitumor, the effect that improves body immunity and liver detoxification; And contain calcium carbonate in the chitin, can increase calcium ion in the water.In the said water filtration material of present embodiment, add chitinous composition, the calcium ion that can carry out sterilizing and provide human body to need water quality.And researcher of the present invention finds that in research process chitin has the ability of pH value in the very strong adjusting water, and the pH value that can regulate pure water is alkalescent, and the weakly alkaline water of long-term drinking is of value to the health of human body.
Said wooden fish stone be a kind of be the powder that raw material is produced with the wooden fish ore; The composition of wooden fish ore is a limonite, and except iron oxide, other impurity often is phosphate; Also has a spot of metasilicate; And more than ten kind of trace elements to the human body beneficial such as strontium, molybdenum, lithium, zinc, selenium, having the metabolism of regulating human body, softening blood vessel prevents the function of artery sclerosis.In the said water filtration material of present embodiment, add wooden fish stone composition, can increase human body trace elements necessary and mineral matter in the water, make pure water after the filtration reach the standard of high quality mineral water.
Said medical stone is a kind of powder of being processed by the subvolcano rock ore, contains more than 20 kind of potassium, sodium, calcium, magnesium, phosphorus macroelement and zinc, iron, selenium, copper, strontium, iodine, fluorine, metasilicic acid etc. to the health healthy trace elements with household.Medical stone is porous, and adsorption capacity is very strong, can absorbing pathogenic bacteria and bacterium, and be good wholefood antistaling and antiseptic agent and refrigeration deodorant.When medical stone is used for water treatment, can the bleaching powder in the water and impurity, organic matter, the bacterium of mixing etc. be adsorbed, decompose, and supply with in the water with mineral matter and multiple human body trace elements necessary.And medical stone can make a large amount of atomic group that has positive and negative electricity of generation in the water, thereby can adsorbed water middle reaches ion.In the said water filtration material of present embodiment, add the medical stone composition, the trace element and mineral matter in increasing water, can also adsorb the impurity such as bleaching powder in the municipal tap water.
Said tourmaline be a kind of be the powder that raw material is produced with the Tourmaline ore, its Main Ingredients and Appearance is a borosilicate.Tourmaline can be regulated the pH value and the electric conductivity of water; Make water deflection alkalescent; Can produce two kinds of anions of hydroxidion and hydrogen ion, make water form small-micelle water, compare with common macromolecular mass water; Get into human body cell more easily and be absorbed, and make that the water penetration of said water filtration material is better.Functional activation water through tourmaline is handled is compared with light water; The trace element and the mineral matter that can have higher concentration; Like calcium, iron, zinc, selenium etc.; Thereby human body brought into play better physiology and medical care effect, long-term drinking just can improve resistance and the natural curability of human body to harmful substance through the tourmaline treated water.
Said kaolin is that a kind of aleuritic texture clay of forming with kaolinite, montmorillonite, quartz, feldspar is the powder that raw material is produced, can with other material mixing tool that fires pottery.
The said water filtration material that present embodiment provided; Its crucial part is that the mix and match of said chitin, wooden fish stone, medical stone, tourmaline, kaolin uses; Can either restraining and sterilizing bacteria, regulate the pH value to alkalescent; Macroelement and trace element be can discharge again, hydroxidion and hydrogen ion also produced simultaneously to promote human body to trace elements absorbed to the human body beneficial.
Described water filtration material, preferably, the granular size of said chitin, wooden fish stone, medical stone, tourmaline, kaolin is 200 orders.
Described water filtration material, preferably, the percentage by weight of the component that is wherein contained is: chitin 30%, wooden fish stone 15%, medical stone 15%, tourmaline 30%, kaolin 10%.Water filtration material according to this proportional arrangement one-tenth; All be up to state standards bottle (bucket) the dress sanitary standard for drinking water of GB19298-2003 defined of the various indexs of the water after filtering; A plurality of indexs obviously are superior to the technical indicator of existing pure water, and the concrete parameter of partial test project is as shown in the table.
| Interventions Requested | Standard value | Measured value | Interventions Requested | Standard value | Measured value |
| Colourity, (degree) | ≤10 | <1 | Turbidity, (degree) | ≤3 | 0.70 |
| Total plate count, (cfu/mL) | ≤50 | 5 | Yeast, (cfu/mL) | ≤10 | <1 |
| Mould, (cfu/mL) | ≤10 | <1 | pH | ? | 7.35 |
| Calcium, (mg/kg) | ? | 1.12 | Magnesium, (mg/kg) | ? | 0.20 |
| Potassium, (mg/kg) | ? | 0.95 | Zinc, (mg/kg) | ? | <0.05 |
| Strontium, (mg/kg) | ? | <0.05 | Iron, (mg/kg) | ? | <0.05 |
| Iodine, (mg/kg) | ? | 57.0 | Metasilicic acid, (mg/L) | ? | 2.7 |
Embodiment two
A kind of water filtration material is compared with embodiment one, and its difference is:
Described water filtration material, preferably, the granular size of said chitin, wooden fish stone, medical stone, tourmaline, kaolin is 80 orders.
Described water filtration material, preferably, the percentage by weight of the component that is wherein contained is: chitin 20%, wooden fish stone 25%, medical stone 25%, tourmaline 15%, kaolin 15%.Water filtration material according to this proportional arrangement one-tenth; All be up to state standards bottle (bucket) the dress sanitary standard for drinking water of GB19298-2003 defined of the various indexs of the water after filtering; A plurality of indexs obviously are superior to the technical indicator of existing pure water, and the concrete parameter of partial test project is as shown in the table.
| Interventions Requested | Standard value | Measured value | Interventions Requested | Standard value | Measured value |
| Colourity, (degree) | ≤10 | <2 | Turbidity, (degree) | ≤3 | 0.90 |
| Total plate count, (cfu/mL) | ≤50 | 6 | Yeast, (cfu/mL) | ≤10 | <2 |
| Mould, (cfu/mL) | ≤10 | <1.5 | pH | ? | 7.15 |
| Calcium, (mg/kg) | ? | 1.5 | Magnesium, (mg/kg) | ? | 0.25 |
| Potassium, (mg/kg) | ? | 0.95 | Zinc, (mg/kg) | ? | <0.05 |
| Strontium, (mg/kg) | ? | <0.06 | Iron, (mg/kg) | ? | <0.05 |
| Iodine, (mg/kg) | ? | 59.0 | Metasilicic acid, (mg/L) | ? | 2.8 |
Embodiment three
A kind of water filtration material is compared with embodiment one, and its difference is:
Described water filtration material, preferably, the granular size of said chitin, wooden fish stone, medical stone, tourmaline, kaolin is 300 orders.
Described water filtration material, preferably, the percentage by weight of the component that is wherein contained is: chitin 40%, wooden fish stone 5%, medical stone 5%, tourmaline 40%, kaolin 10%.Water filtration material according to this proportional arrangement one-tenth; All be up to state standards bottle (bucket) the dress sanitary standard for drinking water of GB19298-2003 defined of the various indexs of the water after filtering; A plurality of indexs obviously are superior to the technical indicator of existing pure water, and the concrete parameter of partial test project is as shown in the table.
| Interventions Requested | Standard value | Measured value | Interventions Requested | Standard value | Measured value |
| Colourity, (degree) | ≤10 | <2 | Turbidity, (degree) | ≤3 | 0.80 |
| Total plate count, (cfu/mL) | ≤50 | 7 | Yeast, (cfu/mL) | ≤10 | <1.5 |
| Mould, (cfu/mL) | ≤10 | <3 | pH | ? | 7.65 |
| Calcium, (mg/kg) | ? | 1.03 | Magnesium, (mg/kg) | ? | 0.10 |
| Potassium, (mg/kg) | ? | 0.35 | Zinc, (mg/kg) | ? | <0.05 |
| Strontium, (mg/kg) | ? | <0.04 | Iron, (mg/kg) | ? | <0.06 |
| Iodine, (mg/kg) | ? | 51.0 | Metasilicic acid, (mg/L) | ? | 2.3 |
Embodiment four
A kind of preparation technology of water filtration material is used to prepare the water filtration material described in the embodiment one to three, comprises the steps:
1, the powder of chitin, wooden fish stone, medical stone, tourmaline, kaolin is put into ball mill respectively and be crushed to more than 200 orders, for use;
2, be chitin 30% according to percentage by weight, wooden fish stone 15%, medical stone 15%, tourmaline 30%, the ratio of kaolin 10% is put into mixer with the powder of preparation in the step 1 and stirred, and is for use;
3, add pure water in the compound after in step 2, stirring, stirring makes it become material-mud, for use;
4, the material-mud of preparation in the step 3 is processed the sphere material of diameter 5mm through marble forming machine, oven dry, for use;
5, the sphere material of preparation in the step 4 is put into the roasting 2.5 hours of heating of 1100 ℃ of high temperature furnaces, the cooling of ceasing fire can be come out of the stove and processed finished product.
Embodiment five
A kind of preparation technology of water filtration material is used to prepare the water filtration material described in the embodiment one to three, comprises the steps:
1, the powder of chitin, wooden fish stone, medical stone, tourmaline, kaolin is put into ball mill respectively and be crushed to more than 80 orders, for use;
2, be chitin 20% according to percentage by weight, wooden fish stone 25%, medical stone 25%, tourmaline 15%, the ratio of kaolin 15% is put into mixer with the powder of preparation in the step 1 and stirred, and is for use;
3, add pure water in the compound after in step 2, stirring, stirring makes it become material-mud, for use;
4, the material-mud of preparation in the step 3 is processed the sphere material of diameter 2mm through marble forming machine, oven dry, for use;
5, the sphere material of preparation in the step 4 is put into the roasting 3 hours of heating of 1000 ℃ of high temperature furnaces, the cooling of ceasing fire can be come out of the stove and processed finished product.
Embodiment six
A kind of preparation technology of water filtration material is used to prepare the water filtration material described in the embodiment one to three, comprises the steps:
1, the powder of chitin, wooden fish stone, medical stone, tourmaline, kaolin is put into ball mill respectively and be crushed to more than 300 orders, for use;
2, be chitin 40% according to percentage by weight, wooden fish stone 5%, medical stone 5%, tourmaline 40%, the ratio of kaolin 10% is put into mixer with the powder of preparation in the step 1 and stirred, and is for use;
3, add pure water in the compound after in step 2, stirring, stirring makes it become material-mud, for use;
4, the material-mud of preparation in the step 3 is processed the sphere material of diameter 8mm through marble forming machine, oven dry, for use;
5, the sphere material of preparation in the step 4 is put into the roasting 2 hours of heating of 1200 ℃ of high temperature furnaces, the cooling of ceasing fire can be come out of the stove and processed finished product.
Embodiment seven
A kind of water filtering device comprises shell, inlet porting and outlet on the said shell, and key is, is provided with in the said shell like embodiment one, two, the water filtration material described in three.
Above content is the explanation to preferred embodiment of the present invention, can help those skilled in the art to understand technical scheme of the present invention more fully.But these embodiment only illustrate, and can not assert that the specific embodiment of the present invention only limits to the explanation of these embodiment.Under the present invention, the those of ordinary skill of technical field, under the prerequisite that does not break away from the present invention's design, can also make some simple deductions and conversion, all should be regarded as belonging to protection scope of the present invention.
Claims (10)
1. the water filtration material is formed by the powder that filters component and the powder sintering of kaolin, it is characterized in that, comprises chitin in the said filtration component.
2. water filtration material according to claim 1 is characterized in that, said filtration component also comprises at least aly can produce the material with the atomic group of positive and negative electricity in water.
3. water filtration material according to claim 1 is characterized in that, also comprises at least a material that can produce hydroxidion or hydrogen ion in the said filtration component, makes water form small-micelle water.
4. according to each described water filtration material of claim 1-3; It is characterized in that: the said material that can in water, produce with the atomic group of positive and negative electricity is the medical stone powder, and the said material that can produce hydroxidion or hydrogen ion is a tourmaline powdery thing.
5. water filtration material according to claim 4; It is characterized in that said water filtration material is that the powder sintering with chitin, wooden fish stone, medical stone, tourmaline, kaolin forms, the shared percentage by weight of each component is respectively: chitin 20-40%; Wooden fish stone 5-25%; Medical stone 5-25%, tourmaline 15-40%, kaolin 10-15%.
6. water filtration material according to claim 4 is characterized in that, the shared percentage by weight of said each component is: chitin 30%, wooden fish stone 15%, medical stone 15%, tourmaline 30%, kaolin 10%.
7. water filtration material according to claim 4 is characterized in that, the granular size of said chitin, wooden fish stone, medical stone, tourmaline, kaolin powder is the 80-300 order, and described water filtration material sinters the spherical of 2-8mm into.
8. the preparation technology of the described water filtration material of claim 1 comprises step:
1), chitin, wooden fish stone, medical stone, tourmaline, kaolin are put into ball mill respectively be crushed to 80-300 purpose powder, for use;
2), be chitin 20-40% according to percentage by weight, wooden fish stone 5-25%, medical stone 5-25%, tourmaline 15-40%, the ratio of kaolin 10-15% is put into mixer with the powder for preparing in the step 1) and stirred, and is for use;
3), to step 2) in add pure water in the compound after stirring, stirring makes it become material-mud, for use;
4), the material-mud for preparing in the step 3) is processed the sphere material of diameter 2-8mm through marble forming machine, oven dry, for use;
5), the sphere material for preparing in the step 4) put into 1000-1200 ℃ high temperature furnace heated roasting 2-3 hour, the cooling of ceasing fire can be come out of the stove and processed finished product.
9. preparation technology according to claim 8 is characterized in that: step 2) described in the percentage by weight of each component be chitin 30%, wooden fish stone 15%, medical stone 15%, tourmaline 30%, kaolin 10%.
10. water filtering device comprises the shell with entrance and exit, it is characterized in that: the water filtration material described in the claim 1 is set in the said shell.
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| CN102898120A (en) * | 2012-10-29 | 2013-01-30 | 北京天天一泉环保科技有限公司 | Water filter material and preparation process thereof as well as corresponding water filter device |
| CN105253981A (en) * | 2015-11-04 | 2016-01-20 | 郭学军 | Mineral filter element and manufacture method thereof |
| CN106495249A (en) * | 2016-11-30 | 2017-03-15 | 广州市瑞硒康生物科技有限公司 | A kind of preparation method of selenium-rich water |
| CN107311289A (en) * | 2017-08-17 | 2017-11-03 | 付全贵 | A kind of preparation technology of zinc-rich strontium drinking water |
| CN107311290A (en) * | 2017-08-17 | 2017-11-03 | 付全贵 | A kind of preparation technology of rich trace elements drinking water |
| CN108975573A (en) * | 2018-08-10 | 2018-12-11 | 安徽碧云湖食品科技发展有限公司 | A kind of preparation method of small-micelle water |
| CN110436557A (en) * | 2019-07-29 | 2019-11-12 | 平武县颐生泉生物科技开发有限公司 | A kind of preparation method of mountain spring water |
| CN111807603A (en) * | 2020-07-21 | 2020-10-23 | 供生堂健康管理有限公司 | Drinking water treatment method and device |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102898120A (en) * | 2012-10-29 | 2013-01-30 | 北京天天一泉环保科技有限公司 | Water filter material and preparation process thereof as well as corresponding water filter device |
| CN105253981A (en) * | 2015-11-04 | 2016-01-20 | 郭学军 | Mineral filter element and manufacture method thereof |
| CN105253981B (en) * | 2015-11-04 | 2018-09-07 | 郭学军 | A kind of minerals filter core and its manufacturing method |
| CN106495249A (en) * | 2016-11-30 | 2017-03-15 | 广州市瑞硒康生物科技有限公司 | A kind of preparation method of selenium-rich water |
| CN107311289A (en) * | 2017-08-17 | 2017-11-03 | 付全贵 | A kind of preparation technology of zinc-rich strontium drinking water |
| CN107311290A (en) * | 2017-08-17 | 2017-11-03 | 付全贵 | A kind of preparation technology of rich trace elements drinking water |
| CN107311290B (en) * | 2017-08-17 | 2020-11-06 | 付全贵 | Preparation process of drinking water rich in trace elements |
| CN107311289B (en) * | 2017-08-17 | 2020-11-06 | 付全贵 | Preparation process of zinc-strontium-rich drinking water |
| CN108975573A (en) * | 2018-08-10 | 2018-12-11 | 安徽碧云湖食品科技发展有限公司 | A kind of preparation method of small-micelle water |
| CN110436557A (en) * | 2019-07-29 | 2019-11-12 | 平武县颐生泉生物科技开发有限公司 | A kind of preparation method of mountain spring water |
| CN111807603A (en) * | 2020-07-21 | 2020-10-23 | 供生堂健康管理有限公司 | Drinking water treatment method and device |
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Application publication date: 20121205 |