CN102703199A - Preparation method of cutting fluid for hardware alloy cutter or processed workpiece as hardware alloy - Google Patents
Preparation method of cutting fluid for hardware alloy cutter or processed workpiece as hardware alloy Download PDFInfo
- Publication number
- CN102703199A CN102703199A CN201210177434XA CN201210177434A CN102703199A CN 102703199 A CN102703199 A CN 102703199A CN 201210177434X A CN201210177434X A CN 201210177434XA CN 201210177434 A CN201210177434 A CN 201210177434A CN 102703199 A CN102703199 A CN 102703199A
- Authority
- CN
- China
- Prior art keywords
- percent
- cutting fluid
- methyl
- preparation
- acid ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention discloses a preparation method of a cutting fluid fora hardware alloy cutter or a processed workpiece as a hardware alloy. The preparation method of the cutting fluid comprises the following steps of: adding 5-7 percent of boracic acid and 24-26 percent of 2-amino-2-methyl-1-propanolamine into water; stirring the mixture under the condition of 40-50DEG C to be completely dissolved; cooling the dissolved solution to 25-35DEG C; then adding 3-5 percent of polyoxyethylene octadecyl phosphate, 5-7 percent of polyoxyethylene phenyl phosphate, 2-4 percent of dibutyl phthalate, 6-8 percent of phenol ether phosphate, 2-4 percent of sodium benzoate, 2-4 percent of propanetriol, 0.4-0.6 percent of isothiazolin one, 0.6-0.8 percent of benzotriazol and 0.3-0.5 percent of nonylphenol polyoxyethylene ether one by one and fully stirring; after the substances are completely dissolved, adding 0.6-1.0 percent of methyl silicone oil and then stirring for 60-90 minutes; and finally, adjusting the pH value to 8.5-9.5, wherein various components are counted according to weight percentage and the balance of water is counted according to weight percentage.
Description
Technical field
The present invention relates to the metal cutting processing technique field, relating in particular to a kind of inserted tool or work piece of adopting is the preparation method of the cutting fluid of wimet.
Background technology
Aqueous cutting fluid can be divided into three kinds of soluble oil (emulsion), semi-synthetic cutting fluid (microemulsion) and fully synthetic cutting fluids.Compare with soluble oil and semi-synthetic cutting fluid, fully synthetic cutting fluid does not contain MO, and its each component such as multiple additives such as rust-preventive agent, extreme-pressure anti-friction additive, tensio-active agent, sanitas and skimmer are all water-soluble, and diluent is transparence or translucent.Totally synthesized cutting fluid good cooling results, processing site are cleaned, product performance are stable, are one type of metal working fluids that has wide range of applications.
But contain trolamine in the Totally synthesized cutting fluid usually, trolamine helps cutting fluid to soak into, permeate in mill (cutting) and cut the interface as the important additives of fully synthetic cutting fluid, gives full play to the cleaning of fully synthetic cutting fluid, lubricated and rust inhibition.But, Ammonia additives such as trolamine to the cobalt in the wimet such as WC-Co have the leaching effect (referring to Pat.Brutto.Water hazard.Cutting Tool Engineering, 1996, (12): 50; Referring to Zhang Xiuling, the high skin of bamboo. contain of the harm of trolamine grinding fluid to inserted tool. wimet, 2000,17 (4): 231-232).And cobalt metal is the sticker of wimet such as WC-Co; If when carrying out ground finish at the use inserted tool or to wimet; Cobalt element in the WC-Co wimet is leached; Directly affect on the one hand the performances such as tenacity and shock resistance of wimet, cause the surface of WC-Co hard metal article color fringe to occur on the other hand, directly influence the outward appearance of goods.
Carry out the occasion of ground finish at the use inserted tool or to wimet; For fear of the leaching effect of fully synthetic cutting fluid to the cobalt in the wimet such as tungsten cobalt or titanium cobalt; Domestic scholars replaces trolamine with triethanolamine oleate; Can partly reduce the leaching effect of fully synthetic cutting fluid like this to cobalt in the alloy; But still can not suppress fully cobalt element leaching (referring to Zhang Haoqiang. the inserted tool cobalt element leaches mechanism and countermeasure, Institutes Of Technology Of Hebei's master thesis, 2005).
Therefore, cutting fluid of the prior art is inappropriate for and adopts inserted tool processing, or is inappropriate for wimet is carried out cut.
Summary of the invention
The objective of the invention is to propose a kind of inserted tool or work piece of adopting is the preparation method of the cutting fluid of wimet; The cutting fluid of employing method preparation is suitable for the cut that adopts inserted tool to carry out, also is suitable for the cut that work piece relates to wimet.
For reaching this purpose, the present invention adopts following technical scheme:
A kind of inserted tool or work piece of adopting is the preparation method of the cutting fluid of wimet, and said cutting fluid is made up of following component by weight percentage: 2-amino-2-methyl-1-propanol amine 24-26%, boric acid 5-7%; T 46155 octadecyl SULPHOSUCCINIC ACID ESTER 3-5%, T 46155 phenyl phosphate ester 5-7%, phenolic ether SULPHOSUCCINIC ACID ESTER 6-8%; Witcizer 300 2-4%, Sodium Benzoate 2-4%, USP Kosher 2-4%; Different plug azoles quinoline ketone 0.4-0.6%, benzotriazole 0.6-0.8%, polyoxyethylene nonylphenol 0.3-0.5%; Methyl-silicone oil 0.6-1.0%, the deionized water surplus; The preparation method of said cutting fluid comprises the steps: boric acid, 2-amino-2-methyl-1-propanol amine are added in the entry; Stir under the 40-50 ℃ of condition and make its dissolving fully; Be cooled to 25-35 ℃; Add T 46155 octadecyl SULPHOSUCCINIC ACID ESTER, T 46155 phenyl phosphate ester, Witcizer 300, phenolic ether SULPHOSUCCINIC ACID ESTER, Sodium Benzoate, USP Kosher then item by item, different plug azoles quinoline ketone, benzotriazole, polyoxyethylene nonylphenol fully stir, and treat that the above-mentioned substance dissolving adds methyl-silicone oil in the back fully; Restir 60-90 minute, at last pH value is adjusted to 8.5-9.5 and get final product.
Composition mechanism of the present invention is: do not adopt trolamine, but adopts 2-amino-2-methyl-1-propanol amine to suppress separating out of cobalt, and on this basis; Various additives such as composite boric acid, T 46155 octadecyl SULPHOSUCCINIC ACID ESTER, T 46155 phenyl phosphate ester, phenolic ether SULPHOSUCCINIC ACID ESTER, Witcizer 300 adopt Sodium Benzoate as antirust composition, at an amount of composite other additive; And on a large amount of experiment basis, confirmed the adding proportion of each component; Make to reach synergistic action effect between the each component, make cutting fluid and suppress the effect that cobalt separates out that it is desired lubricated also to have common cutting fluid concurrently except having; Antirust, cooling and cleanup action.
Compared with prior art the present invention has following outstanding advantage and beneficial effect:
1) cutting fluid of the inventive method preparation can prevent that cobalt from separating out, and is applicable to the cut that adopts inserted tool to carry out, and also is suitable for the cut that work piece relates to wimet.
2) cutting fluid of the inventive method preparation is lubricated, antirust in use, and cooling and cleaning performance are outstanding, satisfy user demand fully.
3) the cutting fluid environmental protection of the inventive method preparation, preparation technology is simple, and cost is low, long service life.
Embodiment
Embodiment one
A kind of inserted tool or work piece of adopting is the preparation method of the cutting fluid of wimet, and said cutting fluid is made up of following component by weight percentage: 2-amino-2-methyl-1-propanol amine 24%, boric acid 7%; T 46155 octadecyl SULPHOSUCCINIC ACID ESTER 3%, T 46155 phenyl phosphate ester 7%, phenolic ether SULPHOSUCCINIC ACID ESTER 6%; Witcizer 300 4%, Sodium Benzoate 2%, USP Kosher 4%; Different plug azoles quinoline ketone 0.4%, benzotriazole 0.8%, polyoxyethylene nonylphenol 0.3%; Methyl-silicone oil 1.0%, the deionized water surplus; The preparation method of said cutting fluid comprises the steps: boric acid, 2-amino-2-methyl-1-propanol amine are added in the entry; Stir under 40 ℃ of conditions and make its dissolving fully; Be cooled to 35 ℃; Add T 46155 octadecyl SULPHOSUCCINIC ACID ESTER, T 46155 phenyl phosphate ester, Witcizer 300, phenolic ether SULPHOSUCCINIC ACID ESTER, Sodium Benzoate, USP Kosher then item by item, different plug azoles quinoline ketone, benzotriazole, polyoxyethylene nonylphenol fully stir, and treat that the above-mentioned substance dissolving adds methyl-silicone oil in the back fully; Restir 60 minutes is adjusted to 9.5 with pH value at last and is got final product.
Embodiment two
A kind of inserted tool or work piece of adopting is the preparation method of the cutting fluid of wimet, and said cutting fluid is made up of following component by weight percentage: 2-amino-2-methyl-1-propanol amine 26%, boric acid 5%; T 46155 octadecyl SULPHOSUCCINIC ACID ESTER 5%, T 46155 phenyl phosphate ester 5%, phenolic ether SULPHOSUCCINIC ACID ESTER 8%; Witcizer 300 2%, Sodium Benzoate 4%, USP Kosher 2%; Different plug azoles quinoline ketone 0.6%, benzotriazole 0.6%, polyoxyethylene nonylphenol 0.5%; Methyl-silicone oil 0.6%, the deionized water surplus; The preparation method of said cutting fluid comprises the steps: boric acid, 2-amino-2-methyl-1-propanol amine are added in the entry; Stir under 50 ℃ of conditions and make its dissolving fully; Be cooled to 25 ℃; Add T 46155 octadecyl SULPHOSUCCINIC ACID ESTER, T 46155 phenyl phosphate ester, Witcizer 300, phenolic ether SULPHOSUCCINIC ACID ESTER, Sodium Benzoate, USP Kosher then item by item, different plug azoles quinoline ketone, benzotriazole, polyoxyethylene nonylphenol fully stir, and treat that the above-mentioned substance dissolving adds methyl-silicone oil in the back fully; Restir 90 minutes is adjusted to 8.5 with pH value at last and is got final product.
Embodiment three
A kind of inserted tool or work piece of adopting is the preparation method of the cutting fluid of wimet, and said cutting fluid is made up of following component by weight percentage: 2-amino-2-methyl-1-propanol amine 25%, boric acid 6%; T 46155 octadecyl SULPHOSUCCINIC ACID ESTER 4%, T 46155 phenyl phosphate ester 6%, phenolic ether SULPHOSUCCINIC ACID ESTER 7%; Witcizer 300 3%, Sodium Benzoate 3%, USP Kosher 3%; Different plug azoles quinoline ketone 0.5%, benzotriazole 0.7%, polyoxyethylene nonylphenol 0.4%; Methyl-silicone oil 0.8%, the deionized water surplus; The preparation method of said cutting fluid comprises the steps: boric acid, 2-amino-2-methyl-1-propanol amine are added in the entry; Stir under 45 ℃ of conditions and make its dissolving fully; Be cooled to 30 ℃; Add T 46155 octadecyl SULPHOSUCCINIC ACID ESTER, T 46155 phenyl phosphate ester, Witcizer 300, phenolic ether SULPHOSUCCINIC ACID ESTER, Sodium Benzoate, USP Kosher then item by item, different plug azoles quinoline ketone, benzotriazole, polyoxyethylene nonylphenol fully stir, and treat that the above-mentioned substance dissolving adds methyl-silicone oil in the back fully; Restir 75 minutes is adjusted to 9.0 with pH value at last and is got final product.
Claims (1)
- One kind to adopt inserted tool or work piece be the preparation method of the cutting fluid of wimet, it is characterized in that said cutting fluid is made up of following component by weight percentage: 2-amino-2-methyl-1-propanol amine 24-26%; Boric acid 5-7%, T 46155 octadecyl SULPHOSUCCINIC ACID ESTER 3-5%, T 46155 phenyl phosphate ester 5-7%; Phenolic ether SULPHOSUCCINIC ACID ESTER 6-8%, Witcizer 300 2-4%, Sodium Benzoate 2-4%; USP Kosher 2-4%, different plug azoles quinoline ketone 0.4-0.6%, benzotriazole 0.6-0.8%; Polyoxyethylene nonylphenol 0.3-0.5%, methyl-silicone oil 0.6-1.0%, deionized water surplus; The preparation method of said cutting fluid comprises the steps: boric acid, 2-amino-2-methyl-1-propanol amine are added in the entry; Stir under the 40-50 ℃ of condition and make its dissolving fully; Be cooled to 25-35 ℃; Add T 46155 octadecyl SULPHOSUCCINIC ACID ESTER, T 46155 phenyl phosphate ester, Witcizer 300, phenolic ether SULPHOSUCCINIC ACID ESTER, Sodium Benzoate, USP Kosher then item by item, different plug azoles quinoline ketone, benzotriazole, polyoxyethylene nonylphenol fully stir, and treat that the above-mentioned substance dissolving adds methyl-silicone oil in the back fully; Restir 60-90 minute, at last pH value is adjusted to 8.5-9.5 and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210177434.XA CN102703199B (en) | 2012-05-31 | 2012-05-31 | Preparation method of cutting fluid for hardware alloy cutter or processed workpiece as hardware alloy |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210177434.XA CN102703199B (en) | 2012-05-31 | 2012-05-31 | Preparation method of cutting fluid for hardware alloy cutter or processed workpiece as hardware alloy |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102703199A true CN102703199A (en) | 2012-10-03 |
| CN102703199B CN102703199B (en) | 2015-04-15 |
Family
ID=46896259
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210177434.XA Expired - Fee Related CN102703199B (en) | 2012-05-31 | 2012-05-31 | Preparation method of cutting fluid for hardware alloy cutter or processed workpiece as hardware alloy |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102703199B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102977357A (en) * | 2012-10-30 | 2013-03-20 | 上海源育节能环保科技有限公司 | Polyoxyethane ether-based glycerol phosphite polymer, preparation method for same and near-dry cutting fluid prepared from same for gear machining |
| CN105238533A (en) * | 2015-09-16 | 2016-01-13 | 东莞市伟思化学科技有限公司 | Steel total-synthesis metal processing fluid and preparation method thereof |
| CN106190480A (en) * | 2016-07-13 | 2016-12-07 | 天长市润达金属防锈助剂有限公司 | A kind of anti-rust metal cutting fluid of high lubricating property |
| CN106244295A (en) * | 2016-07-13 | 2016-12-21 | 天长市润达金属防锈助剂有限公司 | A kind of extreme boundary lubrication metalworking fluid |
| CN115700274A (en) * | 2022-11-28 | 2023-02-07 | 广东红日星实业有限公司 | Cutting fluid and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6383991B1 (en) * | 1998-04-03 | 2002-05-07 | Kao Corporation | Cutting oil composition |
| CN101230305A (en) * | 2007-12-29 | 2008-07-30 | 广州机械科学研究院 | Totally synthesized cutting fluid adapted for cobalt-containing alloy material and preparation method thereof |
| CN102311860A (en) * | 2011-04-26 | 2012-01-11 | 东莞市安美润滑科技有限公司 | Water-based cutting fluid used for processing neodymium-iron-boron material slices and application method thereof |
-
2012
- 2012-05-31 CN CN201210177434.XA patent/CN102703199B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6383991B1 (en) * | 1998-04-03 | 2002-05-07 | Kao Corporation | Cutting oil composition |
| CN101230305A (en) * | 2007-12-29 | 2008-07-30 | 广州机械科学研究院 | Totally synthesized cutting fluid adapted for cobalt-containing alloy material and preparation method thereof |
| CN102311860A (en) * | 2011-04-26 | 2012-01-11 | 东莞市安美润滑科技有限公司 | Water-based cutting fluid used for processing neodymium-iron-boron material slices and application method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102977357A (en) * | 2012-10-30 | 2013-03-20 | 上海源育节能环保科技有限公司 | Polyoxyethane ether-based glycerol phosphite polymer, preparation method for same and near-dry cutting fluid prepared from same for gear machining |
| CN105238533A (en) * | 2015-09-16 | 2016-01-13 | 东莞市伟思化学科技有限公司 | Steel total-synthesis metal processing fluid and preparation method thereof |
| CN106190480A (en) * | 2016-07-13 | 2016-12-07 | 天长市润达金属防锈助剂有限公司 | A kind of anti-rust metal cutting fluid of high lubricating property |
| CN106244295A (en) * | 2016-07-13 | 2016-12-21 | 天长市润达金属防锈助剂有限公司 | A kind of extreme boundary lubrication metalworking fluid |
| CN115700274A (en) * | 2022-11-28 | 2023-02-07 | 广东红日星实业有限公司 | Cutting fluid and preparation method and application thereof |
| CN115700274B (en) * | 2022-11-28 | 2024-03-26 | 广东红日星实业有限公司 | Cutting fluid and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102703199B (en) | 2015-04-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101560430B (en) | Fully synthetic cutting fluid | |
| CN102703199A (en) | Preparation method of cutting fluid for hardware alloy cutter or processed workpiece as hardware alloy | |
| CN105482888A (en) | Complete synthesis cutting fluid capable of meeting machining requirements of multiple materials | |
| CN102559352A (en) | Self-emulsified total synthesis cutting solution | |
| CN104403774A (en) | Water-based cutting fluid and preparation method thereof | |
| CN102787006A (en) | Extreme-pressure metalworking liquid and its preparation method | |
| CN106350189A (en) | Special synthesized cutting fluid with ultra-high lubricating property for black metal and preparation method of special synthesized cutting fluid | |
| CN104193774B (en) | Tall oil acid diacetyl amide borate and preparation method thereof | |
| CN103555396A (en) | Water-based cutting fluid | |
| CN104962937A (en) | Environment-friendly rust-proof cleaning agent and preparation method thereof | |
| CN104327933A (en) | Environmental-protection lubricating water-based cutting fluid | |
| CN102757854B (en) | A kind of inserted tool or work piece of adopting is the cutting fluid of Wimet | |
| CN105612247B (en) | Water-soluble cutting oil agent stoste composition, cutting fluid composition and cutting working method | |
| CN102787010B (en) | Metal water-based stamping liquid and preparation method thereof | |
| CN103992865A (en) | Anti-freezing flame-retardation drawing oil | |
| CN104277898A (en) | Fully synthetic cutting fluid | |
| CN103740454B (en) | Fully synthetic copper and copper alloy workpiece cutting fluid | |
| CN102703188A (en) | Environment-friendly microemulsion cutting fluid without corrosion to machine tools | |
| CN107418693B (en) | Aluminum alloy cutting fluid and preparation method thereof | |
| CN105482871A (en) | Corrosion inhibitor for metal cutting fluids | |
| CN103666726A (en) | Water-based rust-proof cutting fluid and preparation method thereof | |
| CN103451000A (en) | Completely-synthesized cutting fluid for automobile brake disc and preparation method thereof | |
| CN102766519A (en) | Cutting fluid for after-cutting processing of neodymium iron boron | |
| JP2011074186A (en) | Water-soluble metal processing oil | |
| CN105713710A (en) | Improved water-based synthetic cutting fluid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150415 Termination date: 20200531 |