CN102697938B - Natural hair growth promoting liquid and preparation method thereof - Google Patents
Natural hair growth promoting liquid and preparation method thereof Download PDFInfo
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- CN102697938B CN102697938B CN 201210220365 CN201210220365A CN102697938B CN 102697938 B CN102697938 B CN 102697938B CN 201210220365 CN201210220365 CN 201210220365 CN 201210220365 A CN201210220365 A CN 201210220365A CN 102697938 B CN102697938 B CN 102697938B
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Abstract
The invention relates to a natural hair growth promoting liquid and a preparation method thereof. The liquid is prepared from Semen Nigellae, Fructus Phyllanthi, Semen Melo, Semen Brassicae Junceae, Semen Myristicae, Herba Rutae, and Fructus Zanthoxyli by pulverizing, adding water, extracting volatile oil, adding water or ethanol to residue and extracting to obtain extract, filtering, concentrating, and mixing with the volatile oil. The natural hair growth promoting liquid developed on basis of Uyghur medicinal basic theory has the advantages of natural product for treating alopecia, definitecurative effect, no toxic/side effect and irritation, is especially suitable for seborrheic alopecia, and provides convenience for alopecia patients.
Description
Technical field
The present invention relates to a kind of is the natural hair growth liquor of primary raw material with the Chinese herbal medicine, belongs to the skin-protection product technical field.
Background technology
Alopecia is a kind of common skin disease, can betide the male, also can betide the women, is the common appearance hair problem attractive in appearance that influences, and brings very heavy mental pressure often for when serious the trouble patient.Along with the quickening of the development of society and people's life, working and learning rhythm, the mental pressure that people bear increases the weight of day by day, and the sickness rate of alopecia is also more and more higher among the crowd.The clinical medicine that is used for the treatment of seborrheic alopecia of American-European countries is mainly hormone regulator and biologically regulator at present.Yet, and above medicine exists bigger toxicity and side effect, is not suitable for patient's life-time service.Therefore, the natural product for improving hair-growing tool of exploitation has very important significance in the middle of Chinese medicine, the ethnic drug.
A kind of natural hair growth liquor of the present invention and preparation method thereof is prescription under the guidance of Uygur medicine traditional theory, and is used for the treatment of alopecia, determined curative effect clinically for many years.
Summary of the invention
The object of the invention is, a kind of natural hair growth liquor and preparation method thereof is provided, this hair growth liquor is to be raw material by fennelflower seed, Fructus Phyllanthi, Semen Melo, Semen Sinapis, Semen Myristicae, Folium Symplocoris Caudatae, Pericarpium Zanthoxyli, employing is with raw material pulverizing, add water, extract volatile oil, will remain again that medicinal residues add water or ethanol extraction obtains extract, filter, concentrate the back and be mixed and made into volatile oil.This hair growth liquor serves as to instruct the natural product of having developed effective treatment alopecia disease with the Uygur medicine rationale, and its effect is remarkable, has no side effect and zest, is specially adapted to seborrheic alopecia.
A kind of natural hair growth liquor of the present invention, this hair growth liquor are to be made by parts by weight of raw materials fennelflower seed 1-20 part, Fructus Phyllanthi 1-20 part, Semen Melo 1-20 part, Semen Sinapis 1-12 part, Semen Myristicae 1-12 part, Folium Symplocoris Caudatae 1-12 part, Pericarpium Zanthoxyli 1-8 part.
The preparation method of described a kind of natural hair growth liquor follows these steps to carry out:
A, will screen good fennelflower seed, Fructus Phyllanthi, Semen Melo, Semen Sinapis, Semen Myristicae, Folium Symplocoris Caudatae, Zanthoxyli Bungeani powder and be broken to the 10-30 order, add the water that 4-18 doubly measures, extract volatile oil, extraction time is 20-90 minute, extract 60-100 ℃ of temperature, be cooled to temperature 25-30 ℃, obtain volatile oil;
B, the residue medicinal residues among the step a are added entry or concentration is 30%-95% ethanol, reflux, extract, 1-4 time, each extraction time is 1-3 hour, temperature 60-100 ℃, obtains extract;
C, step b extract is filtered, reclaim solvent, concentrate, the volatile oil that concentrated extract and step a are obtained merges again, mixes that fully volatile oil fully is distributed in the concentrated extract, and the packing sterilization can obtain hair growth liquor.
Residue medicinal residues and water or alcoholic acid solid-liquid ratio are 1 among the step b: 5-1: 20.
The method of the extraction volatile oil among the step a is for boiling lifting manipulation, vapor distillation or CO
2Super critical extraction.
A kind of natural hair growth liquor of the present invention and preparation method thereof according to theoretical its action characteristic of Uygur medicine is: the excessive oils and fats of dissolving scalp top layer secretion, the pore that mediation is stopped up.Regulate the epidermis dermis layer that raw property is contained partially, the original gentle attribute of conditioning scalp top layer skin corium.The conditioning smegma is improved the sebaceous gland metabolism.Improve the skin corium blood circulation, recover the alimentation power of hair follicle.Improve scalp top layer skin corium, hair is taken the photograph power, alimentation power, hair plastic force.This hair growth liquor was treated 56 routine seborrheic alopecia patients through 3 years, twice of every day, each 5-10ml, be applied to alopecia place, through 3-5 month treatment, mean treatment 120 days, comparison and detection after 200 times of Electronic Speculum are to scalp Vascular Ultrasonography wavefront, scalp top layer softness, relaxed state, skin corium smegma amount.Volume, temporo, occipital artery blood flow cross-reference is more equal, takes place to change significantly.The efficacy evaluation result: recovery from illness (27 example), hair regrows, and begins to be the fine hair shape, gradually chap blackening and recover normal.Produce effects (22 example), hair bears more than 70%, the little Huang of hair.Effectively (4 example) hair 30% bears the thin Huang of hair.Invalid (3 example) hair does not bear, total effective rate 94.6%, and do not see any toxic and side effects and the irritated phenomenon of non-stimulated nothing during the treatment.
The specific embodiment
Embodiment 1
To screen good 4 parts of 1 part of 1 part in 3 parts of 5 parts of 1 part of fennelflower seed, Fructus Phyllanthis, Semen Melos, Semen Sinapis, Semen Myristicae, Folium Symplocoris Caudataes, Pericarpium Zanthoxyli by weight and be crushed to 10 orders for 1 part, the water that adds 10 times of amounts, adopt conventional vapor distillation to extract volatile oil, extraction time is 45 minutes, extract 60 ℃ of temperature, be cooled to 25 ℃ of temperature, obtain volatile oil;
Residual medicine dreg is added entry, feed liquid ratio 1: 5, reflux, extract, 2 times, each extraction time is 2 hours, 60 ℃ of temperature obtain extract;
Extract is filtered, reclaim solvent, concentrate, concentrated extract and volatile oil are merged again, mix that fully volatile oil fully is distributed in the concentrated extract, the packing sterilization can obtain hair growth liquor.
Embodiment 2
To screen good 1 part of 3 parts of 5 parts in 1 part of 1 part of 5 parts of fennelflower seeds, Fructus Phyllanthi, Semen Melo, Semen Sinapis, Semen Myristicaes, Folium Symplocoris Caudatae, Pericarpium Zanthoxyli by weight and be crushed to 30 orders for 3 parts, the water that adds 4 times of amounts, adopt conventional vapor distillation to extract volatile oil, extraction time is 40 minutes, extract 80 ℃ of temperature, be cooled to 28 ℃ of temperature, obtain volatile oil;
Residual medicine dreg is added entry, and solid-liquid ratio is 1: 10, reflux, extract, 3 times, and each extraction time is 1 hour, 80 ℃ of temperature obtain extract;
Extract is filtered, reclaim solvent, concentrate, concentrated extract and volatile oil are merged again, mix that fully volatile oil fully is distributed in the concentrated extract, the packing sterilization can obtain hair growth liquor.
Embodiment 3
To screen good 5 parts of 5 parts of 3 parts in 9 parts of 8 parts of 10 parts of fennelflower seeds, Fructus Phyllanthis, Semen Melos, Semen Sinapis, Semen Myristicaes, Folium Symplocoris Caudataes, Pericarpium Zanthoxyli by weight and be crushed to 20 orders for 4 parts, the water that adds 15 times of amounts, adopt the conventional lifting manipulation of boiling to extract volatile oil, extraction time is 60 minutes, extract 90 ℃ of temperature, be cooled to 30 ℃ of temperature, obtain volatile oil;
It is 30% ethanol that residual medicine dreg is added concentration, feed liquid ratio 1: 14, and reflux, extract, 2 times, each extraction time is 1.5 hours, 90 ℃ of temperature obtain extract;
Extract is filtered, reclaim solvent, concentrate, concentrated extract and volatile oil are merged again, mix that fully volatile oil fully is distributed in the concentrated extract, the packing sterilization can obtain hair growth liquor.
Embodiment 4
To screen good 12 parts of 12 parts of 12 parts in 20 parts of 20 parts of 20 parts of fennelflower seeds, Fructus Phyllanthis, Semen Melos, Semen Sinapis, Semen Myristicaes, Folium Symplocoris Caudataes, Pericarpium Zanthoxyli by weight and be crushed to 30 orders for 8 parts, the water that adds 18 times of amounts, adopt CO2 supercritical extraction volatile oil, extraction time is 90 minutes, extract 100 ℃ of temperature, be cooled to 30 ℃ of temperature, obtain volatile oil;
It is 90% ethanol that residual medicine dreg is added concentration, feed liquid ratio 1: 8, and reflux, extract, 4 times, each extraction time is 2 hours, 100 ℃ of temperature obtain extract;
Extract is filtered, reclaim solvent, concentrate, concentrated extract and volatile oil are merged again, mix that fully volatile oil fully is distributed in the concentrated extract, the packing sterilization can obtain hair growth liquor.
Embodiment 5
To screen good 11 parts of 9 parts of 10 parts in 16 parts of 18 parts of 15 parts of fennelflower seeds, Fructus Phyllanthis, Semen Melos, Semen Sinapis, Semen Myristicaes, Folium Symplocoris Caudataes, Pericarpium Zanthoxyli by weight and be crushed to 20 orders for 6 parts, adopt CO
2Supercritical extraction volatile oil, extraction time is 30 minutes, extracts 60 ℃ of temperature, is cooled to 25 ℃ of temperature, obtains volatile oil;
To go on foot residual medicine dreg adding concentration is 50% ethanol, feed liquid ratio 1: 15, and reflux, extract, 2 times, each extraction time is 3 hours, 60 ℃ of temperature obtain extract;
Extract is filtered, reclaim solvent, concentrate, concentrated extract and volatile oil are merged again, mix that fully volatile oil fully is distributed in the concentrated extract, the packing sterilization can obtain hair growth liquor.
Embodiment 6
To screen good 6 parts of 8 parts of 12 parts in 7 parts of 15 parts of 12 parts of fennelflower seeds, Fructus Phyllanthis, Semen Melos, Semen Sinapis, Semen Myristicaes, Folium Symplocoris Caudataes, Pericarpium Zanthoxyli by weight and be crushed to 10 orders for 8 parts, adopt CO2 supercritical extraction volatile oil, extraction time is 20 minutes, extract 65 ℃ of temperature, be cooled to 30 ℃ of temperature, obtain volatile oil;
It is 95% ethanol that residual medicine dreg is added concentration, feed liquid ratio 1: 20, and reflux, extract, 4 times, each extraction time is 1 hour, 60 ℃ of temperature obtain extract;
Extract is filtered, reclaim solvent, concentrate, concentrated extract and volatile oil are merged again, mix that fully volatile oil fully is distributed in the concentrated extract, the packing sterilization can obtain hair growth liquor.
A kind of natural hair growth liquor of the present invention is between in December, 2008-2010 year December 12 months, press the Hamilton classification and select the male patient of I to V level, hair growth liquor treatment seborrheic alopecia (androgenetic) 56 examples of the special treatment of utilization seborrheic alopecia have obtained good effect.
Clinical data:
(1) 16-45 one full year of life man patient.
(2) clinical diagnosis is seborrheic alopecia (androgenetic)
(3) can press doctor's advice partner treatment person.
Therapeutic Method:
The hair growth liquor of the special treatment of external seborrheic alopecia, every day twice, each 5-10ml is applied to alopecia place, and 30 days is a course of treatment.
Criterion of therapeutical effect:
According to alopecia number every day, alopecia result (type, general layout, stage) scalp result (state, density) hair result (state, diameter), the New Development growing state is assessed.
Patient Lee XX, 24 years old, occupation: the advertisement practitioner, the every index before the treatment is:
The result:
Ouyang XX, the man, 28 years old, the professional manager:
The result:
Conclusion: recovery from illness, hair grows again, and fat secretion is normal, and the unit are hair density improves, hair blackening chap, the alopecia result is relatively preceding with use, and three indexs recover normal.
Horse XX, 26 years old, the individual operator, the diagnostic result before the treatment:
Result after four courses of treatment:
Old XX, 32 years old, telecommunications worker, the diagnostic result before the treatment:
Result after three course of therapy:
Conclusion: the effect produce effects, hair bears more than 70%, and little Huang, and the scalp fat secretion is normal, and the unit are hair density significantly improves; The alopecia result is relatively preceding with use, three remarkable recoveries that taken stopgap measures.
Buy XX, 30 years old, the man, the industrial and commercial administration personnel, the diagnostic result before the treatment:
Result after three course of therapy:
Ah XX, the man, 35 years old, the practitioner of public institution:
Result after three course of therapy:
Conclusion: effective, hair 30% bears, and more yellow, and it is normal that the scalp fat secretion recovers, and the unit are hair density slightly improves, and relatively, slightly changes before alopecia result and the use.
Zhao XX, the man, 38 years old, self-employed entrepreneur:
Result after three course of therapy:
Lee XX, the man, 47 years old, the supermarket storekeeper:
Result after three course of therapy:
Conclusion: invalid, hair does not bear, and hair density is only arranged, and small variation takes place for the change of oiliness scalp and diameter of hair.
Claims (4)
1. a natural hair growth liquor is characterized in that this hair growth liquor is to be made by parts by weight of raw materials fennelflower seed 1-20 part, Fructus Phyllanthi 1-20 part, Semen Melo 1-20 part, Semen Sinapis 1-12 part, Semen Myristicae 1-12 part, Folium Symplocoris Caudatae 1-12 part, Pericarpium Zanthoxyli 1-8 part.
2. the preparation method of a kind of natural hair growth liquor according to claim 1 is characterized in that following these steps to carrying out:
A, will screen good fennelflower seed, Fructus Phyllanthi, Semen Melo, Semen Sinapis, Semen Myristicae, Folium Symplocoris Caudatae, Zanthoxyli Bungeani powder and be broken to the 10-30 order, add the water that 4-18 doubly measures, extract volatile oil, extraction time is 20-90 minute, extract 60-100 ℃ of temperature, be cooled to temperature 25-30 ℃, obtain volatile oil;
B, the residue medicinal residues among the step a are added entry or concentration is 30%-95% ethanol, reflux, extract, 1-4 time, each extraction time is 1-3 hour, temperature 60-100 ℃, obtains extract;
C, step b extract is filtered, reclaim solvent, concentrate, the volatile oil that concentrated extract and step a are obtained merges again, mixes that fully volatile oil fully is distributed in the concentrated extract, and the packing sterilization can obtain hair growth liquor.
3. method according to claim 2 is characterized in that remaining medicinal residues and water or alcoholic acid solid-liquid ratio among the step b is 1: 5-1: 20.
4. method according to claim 2, the method that it is characterized in that the extraction volatile oil among the step a is for boiling lifting manipulation, vapor distillation or CO
2Super critical extraction.
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| CN102697938B true CN102697938B (en) | 2013-07-31 |
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| CN115414424B (en) * | 2022-04-15 | 2024-03-22 | 西藏自治区藏医院(西藏自治区藏医药研究院) | Phyllanthus emblica spray for preventing and treating alopecia and promoting hair growth and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1121411A (en) * | 1994-10-22 | 1996-05-01 | 中国科学院新疆化学所 | Natural gums hair-caring styling mousse |
| EP2156822A1 (en) * | 2008-08-19 | 2010-02-24 | Imad Znagui | Plant composition for external use on hair and oily preparation comprising such a composition |
| CN102166339A (en) * | 2011-04-01 | 2011-08-31 | 乌鲁木齐彩乃姆日用化妆品有限公司 | Uyghur galenical preparation for hair growing and nourishing and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004002237A (en) * | 2002-05-31 | 2004-01-08 | Noriko Yagi | Anti-aging herb |
| WO2004084848A1 (en) * | 2003-03-27 | 2004-10-07 | Mitsui Chemicals, Inc. | Hair growth stimulant and hair growth stimulating composition |
| KR101133785B1 (en) * | 2009-07-13 | 2012-04-13 | 주식회사 남양 | Composition for Preventing Hair Loss and Promoting Hair Growth Containing Scultellaria baicallensis and Method of Preparing the Same |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1121411A (en) * | 1994-10-22 | 1996-05-01 | 中国科学院新疆化学所 | Natural gums hair-caring styling mousse |
| EP2156822A1 (en) * | 2008-08-19 | 2010-02-24 | Imad Znagui | Plant composition for external use on hair and oily preparation comprising such a composition |
| CN102166339A (en) * | 2011-04-01 | 2011-08-31 | 乌鲁木齐彩乃姆日用化妆品有限公司 | Uyghur galenical preparation for hair growing and nourishing and preparation method thereof |
Non-Patent Citations (6)
| Title |
|---|
| JP特开2004-2237A 2004.01.08 |
| 吐汗• |
| 张瑞等.新疆特色药食两用植物黑种草籽活性成分粗提物抗氧化作用研究.《食品工业》.2011,(第3期),第14-16页，尤其是第14页第2段. |
| 新疆特色药食两用植物黑种草籽活性成分粗提物抗氧化作用研究;张瑞等;《食品工业》;20111231(第3期);第14-16页，尤其是第14页第2段 * |
| 维药头发油治疗脱发;吐汗•阿布都热扎克等;《中国民族医药杂志》;20080731(第7期);第74页，尤其是摘要 * |
| 阿布都热扎克等.维药头发油治疗脱发.《中国民族医药杂志》.2008,(第7期),第74页，尤其是摘要. |
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