CN102669304A - Selenium-enriched tea oil and preparation method thereof - Google Patents
Selenium-enriched tea oil and preparation method thereof Download PDFInfo
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Abstract
The invention discloses selenium-enriched tea oil and a preparation method thereof, relating to the technical field of biological medicines. The selenium-enriched tea oil is made from the following raw materials in percentage by weight: 5-10 wt% of ginseng, 1-5 wt% of peanut, 1-8 wt% of purple sweet potato, 1-5 wt% of garlic, 1-10 wt% of oat and 65-80 wt% of tea seed. The preparation method of the selenium-enriched tea oil comprises the following steps of: preparing the materials, carrying out water extraction, carrying out alcohol extraction, drying, squeezing, carrying out alkaline wash, adsorbing, filtering and extracting, thereby obtaining the selenium-enriched tea oil. The product has the characteristics of selenium enrichment, multiple healthcare effects, and the like. The selenium-enriched tea oil disclosed by the invention is suitable for being eaten by people of all ages, in particular for the middle-aged and aged.
Description
Technical field
The present invention relates to the biological medicine technology field, particularly a kind of preparation method of rich selenium tea oil.
Background technology
Oil tea is the distinctive woody oleiferous plants of China, also is the oil crops that China greatly develops.The comprehensive utilization value of oil tea is very high, contains a lot of high bioactivators, like the active material to the human body beneficial such as vitamin E, Tea Polyphenols, squalene.Selenium is respectfully called " kindling material of life " by domestic and international the world of medicine and nutrition educational circles, enjoys " long-lived element ", " anticancer king ", " heart patron saint " and good reputations such as " natural antidotes "; Selenium is 1/10000000th at the tissue intensive amount, but it has determined the existence of life, is that other materials are irreplaceable to the huge effect of human health; Scarce selenium can directly cause the human immunological competence to descend, and clinical medicine proves, threatens more than 40 kind of disease of human health and life all relevant with the scarce selenium of human body, like cancer, cardiovascular disease, hepatopathy, cataract, pancreas disease, diabetes, genital system diseases etc.In the last few years; Some have occurred and contained the edible oil of selenium element, like Chinese patent (number of patent application is 201010163757.4) " complex intensifying medicine-food two-purpose edible oil and manufacturing approach thereof ", its batching comprises vitamin A, vitamin D, vitamin E, leukotrienes, linoleic acid and selenium; The mass percent of each batching is: vitamin A is 0.3%-0.8%; Vitamin D is 0.000003%-0.000016%, and vitamin E is 0.006%-0.04%, and leukotrienes is 6%-26%; Linoleic acid is 12%-80%, and selenium is 0.0000001%-0.000006%; This product has nutritional oil concurrently and is one with health care oil; Can prevent and treat hypertension, high fat of blood, hyperglycaemia, high cholesterol, cardiovascular and cerebrovascular disease, fatty liver, obesity and senile dementia effectively to a certain extent, simultaneously to a certain extent can enhance memory power.Chinese patent (number of patent application is 200910066402.0) " selenizing 3/6 balance edible oil " and for example, its proportioning is: a-leukotrienes and linoleic ratio are 1: 1～10, and vitamin E is 0～1%, and organic selenium is 0.5～2500 μ g/kg; The aforementioned proportion of this invention has different proportion requirement according to actual needs; Like popular 3/6 balance edible oil; A-leukotrienes: linoleic acid=1: 5～10; Calculate according to taking in 25 gram edible oils for each person every day, should satisfy human body and take in above linoleic acid of 10 grams and the above a-leukotrienes standard of 2 grams every day; Selenizing 3/6 balance edible oil of this invention mainly refers to various all kinds of plant meal oil, comprises that proportionings such as safflower seed oil, siritch, linseed oil, perilla oil, walnut oil, sunflower oil, peanut oil, soya-bean oil, corn oil, cottonseed oil, peanut oil, rapeseed oil, sesame oil, tea oil form; Selenizing 3/6 balance edible oil that this invention is stated can add in vitamin E, fat-soluble tea polyphenol, butylated hydroxy anisole (BHA), 2,6 BHTs (BHT) one or more as protective agent; Selenizing 3/6 balance edible oil of this invention is in 3/6 balance edible oil of different proportion, to add micro-organic selenium, and organic selenium derives from selenide of carragheen, and the selenide of carragheen selenium content is 125mg/g; Selenizing 3/6 balance edible oil of this invention not only provides people's balanced nutrients, mends selenium; And selenium has the effect that keeps grease stability, can overcome many carbon unrighted acid chemical property stable inadequately, meet light and high temperature is prone to take place shortcoming destructive, that be difficult for long preservation.
Summary of the invention
Technical problem to be solved by this invention provides and a kind ofly contains the more edible oil of selenium element, and its preparation method is provided.
The technical scheme that the present invention taked is a kind of rich selenium tea oil of invention, is to be formed by following feedstock production by weight percentage:
The purple potato 1-8 of genseng 5-10 peanut 1-5
Garlic 1-5 oat 1-10 tea seed 65-80.
The technical scheme of its optimization is to be formed by following feedstock production by weight percentage:
Genseng 8 peanuts 3 purple potatos 5
Garlic 3 oats 6 tea seeds 75.
Meanwhile, a kind of preparation method of rich selenium tea oil is provided also, its technical process is following:
A, get the raw materials ready: get genseng, peanut, purple potato, garlic, oat, tea seed by weight percentage, subsequent use respectively;
B, water are carried: subsequent use genseng, purple potato, garlic, oat are dropped in the lixiviate jar, added used genseng, purple potato, garlic, oat gross weight 4-6 purified water doubly, boil extraction, the time is 1.0-2.0h, filters, and collects recrement, and is subsequent use;
C, alcohol extracting: subsequent use recrement is mixed with peanut, add the edible ethanol of recrement and peanut gross weight 4-8 50-95% (volumetric concentration) doubly, soak down at 30-70 ℃, the time is 1.0-2.5h, filters; In recrement, add with the doubly edible ethanol extraction of the 50-95% (volumetric concentration) of amount, the time is 1.0-1.5h, filters, and collects the material slag after extracting, and is subsequent use again;
D, oven dry: subsequent use material slag 40-60 ℃ of oven dry down, is become the dry material slag, subsequent use;
E, squeezing: subsequent use dry material slag is mixed with the tea seed, press through colding pressing and handle (usually below 60 ℃, best temperature is 4-10 ℃), collect the coarse tea oil that squeezes out, subsequent use;
F, alkali cleaning: with subsequent use coarse tea oil, putting into concentration is in the aqueous alkali of 0.5-1.2%, coarse tea oil 2-4 times weight, stirs, and leaves standstill (time is at 0.5-2.5h), separates, and collects the upper strata oil solution, becomes alkali cleaning tea oil, subsequent use;
G, absorption: subsequent use alkali cleaning tea oil is put into the lixiviate jar, add the neutral active carbon that accounts for alkali cleaning tea oil weight 10-15%, fully stir, filter, 3 times repeatedly, collect fluid, become absorption tea oil, subsequent use;
H, filtration: subsequent use absorption tea oil is filtered (crossing the 100-200 mesh filter screen), remove active carbon and other impurity particle, collect the fluid after filtering, become filtration tea oil, subsequent use;
I, extraction: subsequent use filtration tea oil through supercritical fluid extraction (spe medium is a carbon dioxide), is collected the fluid of extraction, promptly get rich selenium tea oil, in the rich selenium tea oil of per 100 grams, selenium content >=100 μ g.
Aqueous alkali described in the f step is a kind of in sodium hydrate aqueous solution or aqueous sodium carbonate or the sodium bicarbonate aqueous solution, or two kinds or three kinds of mixed solutions, and when adopting two kinds or three kinds of mixed solutions, the consumption of each component can be single-candidate or other ratio.
Rich selenium tea oil of the present invention; Adopt tea seed (Camellia oleifera Abel), genseng (Panax ginseng C. A. Mey.), peanut (Arachis hypogaea), purple potato (Solanum tuberosum), garlic (Allium sativum L.) and oat (Bromus japonicus Thunb.) as raw material; Contain a large amount of monounsaturated fatty acids, unrighted acid in the tea seed; Be rich in vitamin E; Also contain squalene and Flavonoid substances, anticancer, anti-inflammatory are had splendid effect.Contain multiple panaxoside and vitamin (Vitamine) B in the genseng
1, Cobastab
2, Cobastab
12, vitamin C; 20 various trace elements such as nicotinic acid (Nicotinic acid), folic acid (Folic acid), pantothenic acid, biotin (Biotin) and nicotinic acid amide and copper, zinc, iron, manganese.Peanut contains protein 25%～36%, and fat content can reach 40%, also contains abundant Cobastab in the peanut
2.PP, A, D, E, calcium and iron etc.Purple potato is rich in selenium element and anthocyanidin.Garlic contains calcium, phosphorus, iron and vitamin C
3, also contain trace elements such as thiamine, riboflavin, niacin, allicin, citral and selenium and germanium.Oat contains mineral matters such as vitamin E, leukotrienes and copper, calcium, phosphorus, iron, zinc, selenium and magnesium.Through preliminary treatment to various raw materials, make its contained organic selenium be easy to liposoluble, and then handle the tea oil that obtains with the tea seed, be rich in organic selenium, in the rich selenium tea oil of per 100 grams, selenium content >=100 μ g; Simultaneously,, kept the most of active bio matter in the tea oil, thereby the rich selenium tea oil that adopts the present invention to prepare contains more selenium element owing to adopt cold pressing.
In addition, the rich selenium tea oil of the present invention's preparation also contains multiple high-activity biological active material and various trace elements such as a large amount of monounsaturated fatty acids, unrighted acid and vitamin E, Tea Polyphenols, flavonoids, so, have plurality of health care functions.
Following table is that the composition of rich selenium tea oil of the present invention detects data:
(content is the nutrient content of 100 gram edible parts)
Can find out from last table data, rich selenium tea oil of the present invention, not only the content of its unrighted acid and monounsaturated fatty acids is very high, and, also contain abundant selenium element and many trace elements to the human body beneficial.
The specific embodiment
Below in conjunction with embodiment, the present invention is done further explanation.Following explanation is the mode to give an example, but protection scope of the present invention is not limited thereto.
The preparation technology of rich selenium tea oil of the present invention is following:
A, get the raw materials ready: get 8 parts of gensengs, 3 parts of peanuts, 5 parts of purple potatos, 3 parts in garlic, 6 parts of oats, 75 parts of tea seeds by weight, add up to 100 parts, subsequent use respectively;
B, water are carried: subsequent use genseng, purple potato, garlic, oat are dropped in the lixiviate jar, add the purified water of 5 times of used gensengs, purple potato, garlic, oat gross weight, boil extraction, the time is 1.5h, filters, and collects recrement, and is subsequent use;
C, alcohol extracting: subsequent use recrement is mixed with peanut, add the edible ethanol of recrement and 6 times of peanut gross weights, volumetric concentration 75%, soak down at 50 ℃, the time is 2.0h, filters; In recrement, add with the doubly edible ethanol extraction of amount, volumetric concentration 75%, the time is 1.2h, filters, and collects the material slag after extracting, and is subsequent use again;
D, oven dry: subsequent use material slag 50 ℃ of oven dry down, is become the dry material slag, subsequent use;
E, squeezing: subsequent use dry material slag is mixed with the tea seed, press through colding pressing and handle (this example adopts 10 ℃), collect the coarse tea oil that squeezes out, subsequent use;
F, alkali cleaning: with subsequent use coarse tea oil, put in the sodium hydrate aqueous solution of concentration 1.0%, three times of coarse tea oil weight, stir, leave standstill (time 1.5h), separate, collect the upper strata oil solution, become alkali cleaning tea oil, subsequent use;
G, absorption: subsequent use alkali cleaning tea oil is put into the lixiviate jar, add the neutral active carbon that accounts for alkali cleaning tea oil weight 12%, fully stir, filter, 3 times repeatedly, collect fluid, become absorption tea oil, subsequent use;
H, filtration: subsequent use absorption tea oil is filtered (crossing the 100-200 mesh filter screen), remove active carbon and other impurity particle, collect the fluid after filtering, become filtration tea oil, subsequent use;
I, extraction: with subsequent use filtration tea oil through supercritical fluid extraction (spe medium adopts carbon dioxide, t=374.3 ℃, p=22.05 MPa); Collect the fluid of extraction, promptly get rich selenium tea oil of the present invention, at this moment; In the rich selenium tea oil of per 100 grams, selenium content >=100 μ g.
Rich selenium tea oil of the present invention, the people that are fit to each ages are edible, and it is edible especially to be fit to the elderly.
Claims (4)
1. rich selenium tea oil is characterized in that it being to be formed by following feedstock production by weight percentage:
The purple potato 1-8 of genseng 5-10 peanut 1-5
Garlic 1-5 oat 1-10 tea seed 65-80.
2. rich selenium tea oil according to claim 1 is characterized in that it being to be formed by following feedstock production by weight percentage:
Genseng 8 peanuts 3 purple potatos 5
Garlic 3 oats 6 tea seeds 75.
3. the preparation method of a rich according to claim 1 or claim 2 selenium tea oil is characterized in that technical process is following:
A, get the raw materials ready: get genseng, peanut, purple potato, garlic, oat, tea seed by weight percentage, subsequent use respectively;
B, water are carried: subsequent use genseng, purple potato, garlic, oat are dropped in the lixiviate jar, added used genseng, purple potato, garlic, oat gross weight 4-6 purified water doubly, boil extraction, the time is 1.0-2.0h, filters, and collects recrement, and is subsequent use;
C, alcohol extracting: subsequent use recrement is mixed with peanut, add the edible ethanol of recrement and peanut gross weight 4-8 50-95% doubly, soak down at 30-70 ℃, the time is 1.0-2.5h, filters; In recrement, add with the doubly edible ethanol extraction of the 50-95% of amount, the time is 1.0-1.5h, filters, and collects the material slag after extracting, and is subsequent use again;
D, oven dry: subsequent use material slag 40-60 ℃ of oven dry down, is become the dry material slag, subsequent use;
E, squeezing: subsequent use dry material slag is mixed with the tea seed, press through colding pressing and handle, collect the coarse tea oil that squeezes out, subsequent use;
F, alkali cleaning: with subsequent use coarse tea oil, putting into concentration is in the aqueous alkali of 0.5-1.2%, coarse tea oil 2-4 times weight, stirs, and leaves standstill, separates, and collects the upper strata oil solution, becomes alkali cleaning tea oil, subsequent use;
G, absorption: subsequent use alkali cleaning tea oil is put into the lixiviate jar, add the neutral active carbon that accounts for alkali cleaning tea oil weight 10-15%, fully stir, filter, 3 times repeatedly, collect fluid, become absorption tea oil, subsequent use;
H, filtration: subsequent use absorption tea oil is filtered, remove active carbon and other impurity particle, collect the fluid after filtering, become filtration tea oil, subsequent use;
I, extraction: subsequent use filtration tea oil through supercritical extract, is collected the fluid of extraction, promptly get rich selenium tea oil.
4. according to the preparation method of the said rich selenium tea oil of claim 3, it is characterized in that: the aqueous alkali described in the f step is a kind of in sodium hydrate aqueous solution or aqueous sodium carbonate or the sodium bicarbonate aqueous solution, or two kinds or three kinds of mixed solutions.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103060080A (en) * | 2013-01-06 | 2013-04-24 | 湖南金浩茶油股份有限公司 | Preparation method of blood-fat-reducing camellia oil |
| CN103283870A (en) * | 2013-06-27 | 2013-09-11 | 管天球 | Tea oil for preventing and treating constipation |
| CN103636815A (en) * | 2013-11-21 | 2014-03-19 | 青岛佰众化工技术有限公司 | High-grade health care edible oil with characteristic of long term storage |
| CN103636816A (en) * | 2013-12-06 | 2014-03-19 | 太和县庄老汉杂粮有限公司 | Sesame oil with functions of blood pressure lowering and health caring |
| CN104839720A (en) * | 2015-05-31 | 2015-08-19 | 安庆市孝柱食品科技有限公司 | Tea oil oral liquid |
| CN105767232A (en) * | 2016-04-05 | 2016-07-20 | 长沙理工大学 | Selenium-rich health grease and preparation method thereof |
| CN106035756A (en) * | 2016-08-16 | 2016-10-26 | 安徽康生源生态农业有限公司 | Selenium-enriched tea oil and preparation technology thereof |
| CN106509159A (en) * | 2016-10-12 | 2017-03-22 | 贵州省黎平县黔香园油脂有限公司 | Preparation method of camellia oil for middle-aged and elderly people |
| CN107227200A (en) * | 2017-07-20 | 2017-10-03 | 贵州黔香园油脂有限公司 | A kind of selenium-rich tea oil of suitable mid-aged population |
| CN107279319A (en) * | 2017-07-19 | 2017-10-24 | 贵州黔香园油脂有限公司 | A kind of selenium-rich tea oil |
| CN113171419A (en) * | 2021-05-13 | 2021-07-27 | 湖南省康多利油脂有限公司 | Selenium-rich tea oil emulsion eczema patch for external application |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101755927A (en) * | 2010-02-03 | 2010-06-30 | 湖北黄袍山绿色产品有限公司 | Edible fortified tea oil for pregnant woman and preparation method thereof |
-
2012
- 2012-05-05 CN CN 201210137102 patent/CN102669304B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101755927A (en) * | 2010-02-03 | 2010-06-30 | 湖北黄袍山绿色产品有限公司 | Edible fortified tea oil for pregnant woman and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 刘学: "《油茶籽油加工的研究进展》", 《粮食科技与经济》 * |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103060080B (en) * | 2013-01-06 | 2013-11-20 | 湖南金浩茶油股份有限公司 | Preparation method of blood-fat-reducing camellia oil |
| CN103060080A (en) * | 2013-01-06 | 2013-04-24 | 湖南金浩茶油股份有限公司 | Preparation method of blood-fat-reducing camellia oil |
| CN103283870A (en) * | 2013-06-27 | 2013-09-11 | 管天球 | Tea oil for preventing and treating constipation |
| CN103283870B (en) * | 2013-06-27 | 2014-03-26 | 管天球 | Tea oil for preventing and treating constipation |
| CN103636815A (en) * | 2013-11-21 | 2014-03-19 | 青岛佰众化工技术有限公司 | High-grade health care edible oil with characteristic of long term storage |
| CN103636816B (en) * | 2013-12-06 | 2015-12-09 | 太和县庄老汉杂粮有限公司 | A kind of sesame oil with antihypertensive healthcare effect |
| CN103636816A (en) * | 2013-12-06 | 2014-03-19 | 太和县庄老汉杂粮有限公司 | Sesame oil with functions of blood pressure lowering and health caring |
| CN104839720A (en) * | 2015-05-31 | 2015-08-19 | 安庆市孝柱食品科技有限公司 | Tea oil oral liquid |
| CN105767232A (en) * | 2016-04-05 | 2016-07-20 | 长沙理工大学 | Selenium-rich health grease and preparation method thereof |
| CN105767232B (en) * | 2016-04-05 | 2019-11-08 | 长沙理工大学 | A kind of selenium-enriched health care grease and preparation method thereof |
| CN106035756A (en) * | 2016-08-16 | 2016-10-26 | 安徽康生源生态农业有限公司 | Selenium-enriched tea oil and preparation technology thereof |
| CN106509159A (en) * | 2016-10-12 | 2017-03-22 | 贵州省黎平县黔香园油脂有限公司 | Preparation method of camellia oil for middle-aged and elderly people |
| CN107279319A (en) * | 2017-07-19 | 2017-10-24 | 贵州黔香园油脂有限公司 | A kind of selenium-rich tea oil |
| CN107227200A (en) * | 2017-07-20 | 2017-10-03 | 贵州黔香园油脂有限公司 | A kind of selenium-rich tea oil of suitable mid-aged population |
| CN113171419A (en) * | 2021-05-13 | 2021-07-27 | 湖南省康多利油脂有限公司 | Selenium-rich tea oil emulsion eczema patch for external application |
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