CN105360354A - Feature-beautifying skin-caring grape seed oil and preparation method thereof - Google Patents
Feature-beautifying skin-caring grape seed oil and preparation method thereof Download PDFInfo
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- CN105360354A CN105360354A CN201510832667.2A CN201510832667A CN105360354A CN 105360354 A CN105360354 A CN 105360354A CN 201510832667 A CN201510832667 A CN 201510832667A CN 105360354 A CN105360354 A CN 105360354A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
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Abstract
The invention discloses a feature-beautifying skin-caring grape seed oil and a preparation method thereof. The feature-beautifying skin-caring grape seed oil is prepared from the following raw materials in parts by weight: grape seeds, wax gourd seeds, bitter gourd seeds, oilseed rape pollen, corn pollen, Badam, selenium-enriched malt, peach flowers, evening primrose, bourrache officinale, and lycopene. The product has the advantages of simple preparation method, easy operation, low requirements for equipment, and less investment; with addition of a variety of raw materials, the nutritional ingredients and the skin care effect of the grape seed oil are improved, the nutrient absorption and utilization can be promoted, and the effects of beautifying features, caring skin, enhancing immunity, protecting heart and cerebral vessels, resisting cancer, resisting oxidation and delaying senility are achieved; through combined use of enzymolysis, ultrasonic and organic solvent extraction methods, the oil production rate is obviously improved and reaches 96-98%; through a series of refining such as degumming, deacidification, decolorization and deodorization, the purity of the grape seed oil is greatly improved, the impurity content is less than or equal to 0.02%, the stability is high, and the shelf life is long; and an extract agent is reused, the cost is saved, environmental pollution is low, and the grape seed oil is suitable for industrial production.
Description
Technical field
The present invention relates generally to food technology field, particularly relates to a kind of beauty and skin care grape-kernel oil and preparation method thereof.
Background technology
It is suitable with main oil crops soybean oil content that the oil content of grape pip is about 14 ~ 17%(), belong to the semi-drying grease of unrighted acid, containing a large amount of unrighted acid, content, up to more than 90%, comprises palmitic acid, stearic acid, oleic acid, linoleic acid and micro-leukotrienes, laurate, myristic acid etc.Its main function composition is linoleic acid, for essential fatty acid, content reaches more than 70%, it is one of important composition forming human body cell film and skin, for children's brain and neurodevelopment, and the blood fat maintaining adult balances, reduces cholesterol, prevents thrombosis, the effect such as prevention of arterial sclerosis all plays an important role.In addition, grape-kernel oil is also containing leukotrienes, leukotrienes is similarly essential fatty acid, be there is the characteristic easily being entered brain cell by blood vessel, be the brain-invigorating nutrition of high-quality, nervous system, brain and amphiblestroid growth can be promoted, improve brain function and learning and memory, Improving memory power can be played, prevention senile dementia and allergy effect.Grape-kernel oil contains multiple liposoluble vitamin and various trace elements, there is effects such as improving microcirculation, immunity moderation power, antiallergy, anti-inflammatory, auxiliary therapeutic action is had to Patients with Cardiovascular/Cerebrovascular Diseases and renal disease patient, also can stimulate circulation, cut down fat gradually, play the effect of weight-reducing.The nutritive value of grape-kernel oil and medical function all obtain the abundant affirmation of domestic and international medical circle and nutritionist.
The major way that tradition extracts grape-kernel oil has solvent extraction method, supercritical CO
2extraction, mechanical expression method, aqueous enzymatic method.Simple use is any one method wherein, all can have respective shortcoming, selects the advantage of multiple method, improves extraction conditions, can reduce the use amount of reagent, cost-saving, can not cause residual, also can improve the recovery rate of grape-kernel oil.
Summary of the invention
In order to make up the defect of prior art, the object of this invention is to provide a kind of beauty and skin care grape-kernel oil and preparation method thereof.
A kind of beauty and skin care grape-kernel oil, is made up of the raw material of following weight portion: grape pip 67 ~ 74, wax gourd seed 28 ~ 34, bitter melon seed 28 ~ 34, rape pollen 17 ~ 22, zasiokaurin 17 ~ 22, bar dawn wood 12 ~ 16, product containing organic selenium 12 ~ 16, peach blossom 10 ~ 14, evening primrose 6 ~ 8, Common Borage 6 ~ 8, lycopene 2 ~ 4.
A preparation method for beauty and skin care grape-kernel oil, specifically comprises the following steps:
(1) adopt selection by winnowing and vibratory sieve to carry out removal of impurities to grape pip, wax gourd seed and bitter melon seed, make impure amount≤0.35 (w/w), 50 ~ 60 DEG C of oven dry, to water content 2 ~ 4% (w/w), pulverize, cross 100 ~ 120 mesh sieves, obtain grape pip powder;
(2) in rape pollen, zasiokaurin and peach blossom, add the water of rape pollen, zasiokaurin and peach blossom gross weight 2 ~ 3 times amount, 30 ~ 40 DEG C of constant temperature, the ultrasonic immersion of 36 ~ 40KHz 8 ~ 12 hours, grinds with colloid mill, makes particle diameter be 2 ~ 4 μm, obtains pollen jelly;
(3) cleaned in Ba Danmu, product containing organic selenium, evening primrose and Common Borage, little fire is fried to raw fragrant, pulverizes, and crosses 120 ~ 140 mesh sieves, obtains medicine baking soda;
(4) grape pip powder, pollen jelly and medicine baking soda are mixed, add the soft water of grape pip grain weight amount 7 ~ 9 times amount, in 500 ~ 600W microwave treatment, ad pond om is 1.6 ~ 1.8 times of grape pip grain weight amount, leave standstill 140 ~ 160 minutes, add the mixed enzyme of grape pip grain weight amount 0.7 ~ 0.9%, 36 ~ 42 DEG C of ultrasonic enzymolysis 3 ~ 4 hours, add the protease of grape pip grain weight amount 0.6 ~ 0.8%, 40 ~ 44 DEG C of ultrasonic enzymolysis 6 ~ 7 hours, 80 ~ 90 DEG C are ultrasonic 10 ~ 15 minutes, 9000 ~ 10000 revs/min, centrifugal 6 ~ 8 minutes, obtain enzymolysis grape pip slurry;
(5) in enzymolysis grape pip slurry, add the mixed organic solvents of enzymolysis grape pip slurry weight 35 ~ 45%, rock 30 ~ 40 minutes, leave standstill 10 ~ 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 18 ~ 22% is added in lower floor's aqueous phase, rock 20 ~ 30 minutes, leave standstill 10 ~ 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 13 ~ 17% is added in lower floor's aqueous phase, rock 15 ~ 25 minutes, leave standstill 10 ~ 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, merge the organic phase of 3 extractions, 40 ~ 45 DEG C of vacuum rotatings concentrate, remove mixed organic solvents, reuse, obtain grape pip crude oil,
(6) refining: the concentration adding grape pip crude oil weight 0.14 ~ 0.16% in grape pip crude oil is the food-grade aqueous citric acid solution of 70 ~ 75% (w/w), 30 ~ 40 revs/min, stir 40 ~ 50 minutes, leave standstill 20 ~ 30 minutes, the concentration adding grape pip crude oil weight 7 ~ 9% is the NaOH solution of 8 ~ 12% (w/w), under 50 ~ 60 DEG C of water-baths, 20 ~ 30 revs/min, stir 50 ~ 55 minutes, leave standstill 40 ~ 50 minutes, be warming up to 70 ~ 75 DEG C, centrifugal removing water layer, temperature is 94 ~ 98 DEG C, and pressure is 3.2 ~ 3.8KPa, vacuum dehydration, obtains refining grape pip just oil;
(7) in refining grape pip just oil, add the decolorizer of the first weight of oil 3 ~ 5% of refining grape pip, first for refining grape pip oil is heated to 90 ~ 100 DEG C, and decolour 20 ~ 25 minutes, obtain beauty and skin care grape-kernel oil, oil yield is 96 ~ 98%, impurity≤0.02%;
(8) processes becomes soft capsule routinely, and every, containing beauty and skin care grape-kernel oil 5mg, obtains finished product.
The mixed enzyme of described step 4), is made up of the enzyme preparation of following weight portion: cellulase 58 ~ 64, hemicellulase 35 ~ 40, pectase 28 ~ 32, dextranase 23 ~ 25, polygalacturonase 18 ~ 22, amylase 15 ~ 17, lipoxidase 12 ~ 15.
The mixed organic solvents of described step 5), is made up of the organic solvent of following weight portion: ethanol 54 ~ 62, isopropyl alcohol 24 ~ 30, n-hexane 16 ~ 20, benzinum 10 ~ 15.
The decolorizer of described step 7), is made up of the decolorizer of following weight portion: carclazyte 33 ~ 37, active carbon 22 ~ 26, zeolite 16 ~ 20, concave convex rod 11 ~ 15.
Wax gourd seed, is rich in hydroxymalonic acid, and long-term eating effectively can suppress carbohydrate-modifying for fatty in body, has the food therapy values such as higher beauty treatment moisturizing and body shaping.
Heat-clearing, can fall fire, in bitter melon seed, removing toxic substances, hypotensive, reducing blood lipid, flat liver improving eyesight, relieving summer-heat, skin-protecting face nursing, and fat-reducing, prevents artery sclerosis.
Rape pollen, anti-aging, Glycerin, brightening, dispelling spots, dispelling, reduces wrinkle, strengthens immunologic function, control brain cardiovascular disease, and fat-reducing, regulates functions of intestines and stomach, promotes sleep, liver protecting, Improving memory power.
Zasiokaurin, improves skin tone, Glycerin, and radioresistance is anticancer, improves digestive function, anti-ageing, protection liver, hypoglycemic, hypotensive, softening blood vessel.
Ba Danmu, beauty and skin care, cardioprotection, improves intestinal health, controls body weight, maintains blood sugar level.
Product containing organic selenium, improves immunity, anticancer, antiviral, adjustment blood pressure, relieving cough and relieving asthma, reducing blood lipid, diuresis defaecation, detumescence, fat-reducing, and detoxicating intestine, relieves summer heat and quench one's thirst, mental-tranquilization, beauty and skin care, desalination color spot.
Peach blossom, promotion of blood circulation, moist skin, improves blood circulation, promote skin-nourishing and oxygen supply, make the lipofuscin element of promotion human senility accelerate excretion, make muscle fine and smooth, flexible, desalination color spot, also can strengthen the resistance against diseases of skin, thus prevent and treat skin disease, of great advantage to skin.
Evening primrose, cosmetic hair-care, strengthens muscles and bones, and dispels rheumatism, treatment hypertension, and reducing blood lipid is hypoglycemic, anti-ageing, protection cardiovascular and cerebrovascular, anti-inflammation, and prevention of osteoporosis is anticancer.
Common Borage, improves skin, reduces wrinkle, regulates endocrine, puts down and comforts mood, and stable neural, anticancer, develop immunitypty, improves arteriosclerosis, heart disease, diabetes, eczema, arthritis.
Lycopene, beauty treatment Eradicates wrinkle, delays senility, suppresses cancer, protect cardiovascular and cerebrovascular, ultra-violet radiation resisting, develop immunitypty, prevention of osteoporosis, hypotensive.
Advantage of the present invention is: a kind of beauty and skin care grape-kernel oil provided by the invention and preparation method thereof, and method is simple, is easy to operation, low for equipment requirements, small investment; Add multiple beauty and skin care raw material, improve nutritional labeling and the skin effect of grape-kernel oil, and absorbing of nutrition can be promoted, reach beauty and skin care, develop immunitypty, protection cardiovascular and cerebrovascular, anticancer, anti-oxidant, the effect delayed senility; By the conbined usage of enzymatic isolation method, ultrasonic method and organic solvent extractionprocess, play the advantage of each method, oil yield is significantly improved, reaches 96 ~ 98%; By coming unstuck, depickling, decolouring and deodorization a series of refinings, the purity of grape-kernel oil is improved greatly, impurity≤0.02%, stability is high, long shelf-life; Extractant recycling rate of waterused is high, cost-saving, and operating environment is polluted low, is applicable to industrialization and produces.
Detailed description of the invention
With specific embodiment, the present invention is described below, but is not limitation of the present invention.
Embodiment 1
A kind of beauty and skin care grape-kernel oil, is made up of the raw material of following weight portion: grape pip 67, wax gourd seed 28, bitter melon seed 28, rape pollen 17, zasiokaurin 17, bar dawn wood 12, product containing organic selenium 12, peach blossom 10, evening primrose 6, Common Borage 6, lycopene 2.
A preparation method for beauty and skin care grape-kernel oil, specifically comprises the following steps:
(1) adopt selection by winnowing and vibratory sieve to carry out removal of impurities to grape pip, wax gourd seed and bitter melon seed, make impure amount≤0.35 (w/w), 50 DEG C of oven dry, to water content 2% (w/w), pulverize, cross 100 mesh sieves, obtain grape pip powder;
(2) in rape pollen, zasiokaurin and peach blossom, add the water of rape pollen, zasiokaurin and peach blossom gross weight 2 times amount, 30 DEG C of constant temperature, the ultrasonic immersion of 36KHz 8 hours, grinds with colloid mill, makes particle diameter be 2 μm, obtains pollen jelly;
(3) cleaned in Ba Danmu, product containing organic selenium, evening primrose and Common Borage, little fire is fried to raw fragrant, pulverizes, and crosses 120 mesh sieves, obtains medicine baking soda;
(4) grape pip powder, pollen jelly and medicine baking soda are mixed, add the soft water of grape pip grain weight amount 7 times amount, in 500W microwave treatment, ad pond om is 1.6 times of grape pip grain weight amount, leave standstill 140 minutes, add the mixed enzyme of grape pip grain weight amount 0.7%, 36 DEG C of ultrasonic enzymolysis 3 hours, add the protease of grape pip grain weight amount 0.6%, 40 DEG C of ultrasonic enzymolysis 6 hours, 80 DEG C are ultrasonic 10 minutes, 9000 revs/min, centrifugal 6 minutes, obtain enzymolysis grape pip slurry;
(5) in enzymolysis grape pip slurry, add the mixed organic solvents of enzymolysis grape pip slurry weight 35%, rock 30 minutes, leave standstill 10 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 18% is added in lower floor's aqueous phase, rock 20 minutes, leave standstill 10 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 13% is added in lower floor's aqueous phase, rock 15 minutes, leave standstill 10 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, merge the organic phase of 3 extractions, 40 DEG C of vacuum rotatings concentrate, remove mixed organic solvents, reuse, obtain grape pip crude oil,
(6) refining: the concentration adding grape pip crude oil weight 0.14% in grape pip crude oil is the food-grade aqueous citric acid solution of 70% (w/w), 30 revs/min, stir 40 minutes, leave standstill 20 minutes, the concentration adding grape pip crude oil weight 7% is the NaOH solution of 8% (w/w), under 50 DEG C of water-baths, 20 revs/min, stir 50 minutes, leave standstill 40 minutes, be warming up to 70 DEG C, centrifugal removing water layer, temperature is 94 DEG C, and pressure is 3.2KPa, vacuum dehydration, obtains refining grape pip just oil;
(7) in refining grape pip just oil, add the decolorizer of the first weight of oil 3% of refining grape pip, first for refining grape pip oil is heated to 90 DEG C, and decolour 20 minutes, obtain beauty and skin care grape-kernel oil, oil yield is 96%, impurity≤0.02%;
(8) processes becomes soft capsule routinely, and every, containing beauty and skin care grape-kernel oil 5mg, obtains finished product.
The mixed enzyme of described step 4), is made up of the enzyme preparation of following weight portion: cellulase 58, hemicellulase 35, pectase 28, dextranase 23, polygalacturonase 18, amylase 15, lipoxidase 12.
The mixed organic solvents of described step 5), is made up of the organic solvent of following weight portion: ethanol 54, isopropyl alcohol 24, n-hexane 16, benzinum 10.
The decolorizer of described step 7), is made up of the decolorizer of following weight portion: carclazyte 33, active carbon 22, zeolite 16, concave convex rod 11.
Embodiment 2
A kind of beauty and skin care grape-kernel oil, is made up of the raw material of following weight portion: grape pip 71, wax gourd seed 33, bitter melon seed 31, rape pollen 19, zasiokaurin 19, bar dawn wood 14, product containing organic selenium 14, peach blossom 12, evening primrose 7, Common Borage 7, lycopene 3.
A preparation method for beauty and skin care grape-kernel oil, specifically comprises the following steps:
(1) adopt selection by winnowing and vibratory sieve to carry out removal of impurities to grape pip, wax gourd seed and bitter melon seed, make impure amount≤0.35 (w/w), 55 DEG C of oven dry, to water content 3% (w/w), pulverize, cross 110 mesh sieves, obtain grape pip powder;
(2) in rape pollen, zasiokaurin and peach blossom, add the water of rape pollen, zasiokaurin and peach blossom gross weight 2.5 times amount, 35 DEG C of constant temperature, the ultrasonic immersion of 38KHz 10 hours, grinds with colloid mill, makes particle diameter be 3 μm, obtains pollen jelly;
(3) cleaned in Ba Danmu, product containing organic selenium, evening primrose and Common Borage, little fire is fried to raw fragrant, pulverizes, and crosses 130 mesh sieves, obtains medicine baking soda;
(4) grape pip powder, pollen jelly and medicine baking soda are mixed, add the soft water of grape pip grain weight amount 9 times amount, in 550W microwave treatment, ad pond om is 1.7 times of grape pip grain weight amount, leave standstill 150 minutes, add the mixed enzyme of grape pip grain weight amount 0.8%, 39 DEG C of ultrasonic enzymolysis 3.5 hours, add the protease of grape pip grain weight amount 0.7%, 42 DEG C of ultrasonic enzymolysis 6.5 hours, 85 DEG C are ultrasonic 13 minutes, 9500 revs/min, centrifugal 7 minutes, obtain enzymolysis grape pip slurry;
(5) in enzymolysis grape pip slurry, add the mixed organic solvents of enzymolysis grape pip slurry weight 40%, rock 35 minutes, leave standstill 13 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 20% is added in lower floor's aqueous phase, rock 25 minutes, leave standstill 13 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 15% is added in lower floor's aqueous phase, rock 20 minutes, leave standstill 13 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, merge the organic phase of 3 extractions, 43 DEG C of vacuum rotatings concentrate, remove mixed organic solvents, reuse, obtain grape pip crude oil,
(6) refining: the concentration adding grape pip crude oil weight 0.15% in grape pip crude oil is the food-grade aqueous citric acid solution of 73% (w/w), 35 revs/min, stir 45 minutes, leave standstill 25 minutes, the concentration adding grape pip crude oil weight 8% is the NaOH solution of 10% (w/w), under 55 DEG C of water-baths, 25 revs/min, stir 53 minutes, leave standstill 45 minutes, be warming up to 73 DEG C, centrifugal removing water layer, temperature is 96 DEG C, and pressure is 3.6KPa, vacuum dehydration, obtains refining grape pip just oil;
(7) in refining grape pip just oil, add the decolorizer of the first weight of oil 4% of refining grape pip, first for refining grape pip oil is heated to 95 DEG C, and decolour 23 minutes, obtain beauty and skin care grape-kernel oil, oil yield is 97%, impurity≤0.02%;
(8) processes becomes soft capsule routinely, and every, containing beauty and skin care grape-kernel oil 5mg, obtains finished product.
The mixed enzyme of described step 4), is made up of the enzyme preparation of following weight portion: cellulase 61, hemicellulase 38, pectase 30, dextranase 24, polygalacturonase 20, amylase 16, lipoxidase 13.
The mixed organic solvents of described step 5), is made up of the organic solvent of following weight portion: ethanol 57, isopropyl alcohol 27, n-hexane 18, benzinum 13.
The decolorizer of described step 7), is made up of the decolorizer of following weight portion: carclazyte 35, active carbon 24, zeolite 18, concave convex rod 13.
Embodiment 3
A kind of beauty and skin care grape-kernel oil, is made up of the raw material of following weight portion: grape pip 74, wax gourd seed 34, bitter melon seed 34, rape pollen 22, zasiokaurin 22, bar dawn wood 16, product containing organic selenium 16, peach blossom 14, evening primrose 8, Common Borage 8, lycopene 4.
A preparation method for beauty and skin care grape-kernel oil, specifically comprises the following steps:
(1) adopt selection by winnowing and vibratory sieve to carry out removal of impurities to grape pip, wax gourd seed and bitter melon seed, make impure amount≤0.35 (w/w), 60 DEG C of oven dry, to water content 4% (w/w), pulverize, cross 120 mesh sieves, obtain grape pip powder;
(2) in rape pollen, zasiokaurin and peach blossom, add the water of rape pollen, zasiokaurin and peach blossom gross weight 3 times amount, 40 DEG C of constant temperature, the ultrasonic immersion of 40KHz 12 hours, grinds with colloid mill, makes particle diameter be 4 μm, obtains pollen jelly;
(3) cleaned in Ba Danmu, product containing organic selenium, evening primrose and Common Borage, little fire is fried to raw fragrant, pulverizes, and crosses 140 mesh sieves, obtains medicine baking soda;
(4) grape pip powder, pollen jelly and medicine baking soda are mixed, add the soft water of grape pip grain weight amount 9 times amount, in 600W microwave treatment, ad pond om is 1.8 times of grape pip grain weight amount, leave standstill 160 minutes, add the mixed enzyme of grape pip grain weight amount 0.9%, 42 DEG C of ultrasonic enzymolysis 4 hours, add the protease of grape pip grain weight amount 0.8%, 44 DEG C of ultrasonic enzymolysis 7 hours, 90 DEG C are ultrasonic 15 minutes, 10000 revs/min, centrifugal 8 minutes, obtain enzymolysis grape pip slurry;
(5) in enzymolysis grape pip slurry, add the mixed organic solvents of enzymolysis grape pip slurry weight 45%, rock 40 minutes, leave standstill 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 22% is added in lower floor's aqueous phase, rock 30 minutes, leave standstill 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 17% is added in lower floor's aqueous phase, rock 25 minutes, leave standstill 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, merge the organic phase of 3 extractions, 45 DEG C of vacuum rotatings concentrate, remove mixed organic solvents, reuse, obtain grape pip crude oil,
(6) refining: the concentration adding grape pip crude oil weight 0.16% in grape pip crude oil is the food-grade aqueous citric acid solution of 75% (w/w), 40 revs/min, stir 50 minutes, leave standstill 30 minutes, the concentration adding grape pip crude oil weight 9% is the NaOH solution of 12% (w/w), under 60 DEG C of water-baths, 30 revs/min, stir 55 minutes, leave standstill 50 minutes, be warming up to 75 DEG C, centrifugal removing water layer, temperature is 98 DEG C, and pressure is 3.8KPa, vacuum dehydration, obtains refining grape pip just oil;
(7) in refining grape pip just oil, add the decolorizer of the first weight of oil 5% of refining grape pip, first for refining grape pip oil is heated to 100 DEG C, and decolour 25 minutes, obtain beauty and skin care grape-kernel oil, oil yield is 98%, impurity≤0.02%;
(8) processes becomes soft capsule routinely, and every, containing beauty and skin care grape-kernel oil 5mg, obtains finished product.
The mixed enzyme of described step 4), is made up of the enzyme preparation of following weight portion: cellulase 64, hemicellulase 40, pectase 32, dextranase 25, polygalacturonase 22, amylase 17, lipoxidase 15.
The mixed organic solvents of described step 5), is made up of the organic solvent of following weight portion: ethanol 62, isopropyl alcohol 30, n-hexane 20, benzinum 15.
The decolorizer of described step 7), is made up of the decolorizer of following weight portion: carclazyte 37, active carbon 26, zeolite 20, concave convex rod 15.
Comparative example
Commercially available common glucose seed oil.
The leading indicator of embodiment grape-kernel oil:
According to national grape-kernel oil standard (GB/T22478-2008), prepared by grape-kernel oil to this technology of employing and detects.The leading indicator of embodiment grape-kernel oil is in table 1.
Table 1: the leading indicator of embodiment grape-kernel oil
| Project | GB | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Color and luster | Light green or light yellow | Qualified | Qualified | Qualified |
| Smell, flavour | Smell, mouthfeel are good | Qualified | Qualified | Qualified |
| Transparency | Clarification, transparent | Qualified | Qualified | Qualified |
| Acid number (KOH)/(mg/g) | ≤0.6 | 0.22 | 0.22 | 0.22 |
| Moisture and volatile matter content/(%) | ≤0.1 | 0.02 | 0.01 | 0.01 |
| Impurity/(%) | ≤0.05 | 0.02 | 0.02 | 0.01 |
| Saponified matter content/(%) | ≤0.005 | 0.003 | 0.002 | 0.002 |
| Peroxide value/(mmol/kg) | ≤5 | 1.2 | 1.1 | 1.1 |
As can be seen from Table 1, the grape-kernel oil of embodiment meets national standard, and edible safety is healthy, and health care is good.
The skincare effect of embodiment and comparative example grape-kernel oil:
Effective: the symptoms such as acne, acne, elasticity weaken, tarnish, hypodermis minimizing, Dermatochalasia, hyperpigmentation, color spot alleviate;
Invalid: the symptoms such as acne, acne, elasticity weaken, tarnish, hypodermis minimizing, Dermatochalasia, hyperpigmentation, color spot are constant or more serious.
Instructions of taking: every day 2 times, each 1, every 5mg.
Stochastic choice has the patient 400 of acne symptom, is divided into 4 groups at random, often organizes 100 people; Stochastic choice has the patient 400 of senile symptom, is divided into 4 groups at random, often organizes 100 people; Stochastic choice has the patient 400 of color spot symptom, is divided into 4 groups at random, often organizes 100 people; All patients deliberately do not use the skin care item solving skin problem in tested period, only carry out conventional skin care every day, for each person every day each table grapes seed oil 10mg, and the tested time is 30 days, takes pictures and contrast in tested front and back; The beauty and skin care of embodiment and comparative example grape-kernel oil the results are shown in Table 2.
Table 2: the beauty and skin care result of embodiment and comparative example grape-kernel oil
Can find out from table 2, obviously comparatively comparative example is strong to the improvement of the skin problem of acne symptom, senile symptom and color spot symptom and the situation of alleviation for the beauty and skin care grape-kernel oil of embodiment, there is obvious skincare effect, long-term edible meeting improve gradually to skin, reaches the effect delayed senility.
Claims (5)
1. a beauty and skin care grape-kernel oil, it is characterized in that, be made up of the raw material of following weight portion: grape pip 67 ~ 74, wax gourd seed 28 ~ 34, bitter melon seed 28 ~ 34, rape pollen 17 ~ 22, zasiokaurin 17 ~ 22, bar dawn wood 12 ~ 16, product containing organic selenium 12 ~ 16, peach blossom 10 ~ 14, evening primrose 6 ~ 8, Common Borage 6 ~ 8, lycopene 2 ~ 4.
2. the preparation method of beauty and skin care grape-kernel oil according to claim 1, is characterized in that, comprise the following steps:
(1) adopt selection by winnowing and vibratory sieve to carry out removal of impurities to grape pip, wax gourd seed and bitter melon seed, make impure amount≤0.35 (w/w), 50 ~ 60 DEG C of oven dry, to water content 2 ~ 4% (w/w), pulverize, cross 100 ~ 120 mesh sieves, obtain grape pip powder;
(2) in rape pollen, zasiokaurin and peach blossom, add the water of rape pollen, zasiokaurin and peach blossom gross weight 2 ~ 3 times amount, 30 ~ 40 DEG C of constant temperature, the ultrasonic immersion of 36 ~ 40KHz 8 ~ 12 hours, grinds with colloid mill, makes particle diameter be 2 ~ 4 μm, obtains pollen jelly;
(3) cleaned in Ba Danmu, product containing organic selenium, evening primrose and Common Borage, little fire is fried to raw fragrant, pulverizes, and crosses 120 ~ 140 mesh sieves, obtains medicine baking soda;
(4) grape pip powder, pollen jelly and medicine baking soda are mixed, add the soft water of grape pip grain weight amount 7 ~ 9 times amount, in 500 ~ 600W microwave treatment, ad pond om is 1.6 ~ 1.8 times of grape pip grain weight amount, leave standstill 140 ~ 160 minutes, add the mixed enzyme of grape pip grain weight amount 0.7 ~ 0.9%, 36 ~ 42 DEG C of ultrasonic enzymolysis 3 ~ 4 hours, add the protease of grape pip grain weight amount 0.6 ~ 0.8%, 40 ~ 44 DEG C of ultrasonic enzymolysis 6 ~ 7 hours, 80 ~ 90 DEG C are ultrasonic 10 ~ 15 minutes, 9000 ~ 10000 revs/min, centrifugal 6 ~ 8 minutes, obtain enzymolysis grape pip slurry;
(5) in enzymolysis grape pip slurry, add the mixed organic solvents of enzymolysis grape pip slurry weight 35 ~ 45%, rock 30 ~ 40 minutes, leave standstill 10 ~ 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 18 ~ 22% is added in lower floor's aqueous phase, rock 20 ~ 30 minutes, leave standstill 10 ~ 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, the mixed organic solvents of lower floor's aqueous phase weight 13 ~ 17% is added in lower floor's aqueous phase, rock 15 ~ 25 minutes, leave standstill 10 ~ 15 minutes, the organic phase on the aqueous phase of lower floor and upper strata is separated, merge the organic phase of 3 extractions, 40 ~ 45 DEG C of vacuum rotatings concentrate, remove mixed organic solvents, reuse, obtain grape pip crude oil,
(6) refining: the concentration adding grape pip crude oil weight 0.14 ~ 0.16% in grape pip crude oil is the food-grade aqueous citric acid solution of 70 ~ 75% (w/w), 30 ~ 40 revs/min, stir 40 ~ 50 minutes, leave standstill 20 ~ 30 minutes, the concentration adding grape pip crude oil weight 7 ~ 9% is the NaOH solution of 8 ~ 12% (w/w), under 50 ~ 60 DEG C of water-baths, 20 ~ 30 revs/min, stir 50 ~ 55 minutes, leave standstill 40 ~ 50 minutes, be warming up to 70 ~ 75 DEG C, centrifugal removing water layer, temperature is 94 ~ 98 DEG C, and pressure is 3.2 ~ 3.8KPa, vacuum dehydration, obtains refining grape pip just oil;
(7) in refining grape pip just oil, add the decolorizer of the first weight of oil 3 ~ 5% of refining grape pip, first for refining grape pip oil is heated to 90 ~ 100 DEG C, and decolour 20 ~ 25 minutes, obtain beauty and skin care grape-kernel oil, oil yield is 96 ~ 98%, impurity≤0.02%;
(8) processes becomes soft capsule routinely, and every, containing beauty and skin care grape-kernel oil 5mg, obtains finished product.
3. the preparation method of beauty and skin care grape-kernel oil according to claim 2, it is characterized in that, the mixed enzyme of described step 4), is made up of the enzyme preparation of following weight portion: cellulase 58 ~ 64, hemicellulase 35 ~ 40, pectase 28 ~ 32, dextranase 23 ~ 25, polygalacturonase 18 ~ 22, amylase 15 ~ 17, lipoxidase 12 ~ 15.
4. the preparation method of beauty and skin care grape-kernel oil according to claim 2, it is characterized in that, the mixed organic solvents of described step 5), is made up of the organic solvent of following weight portion: ethanol 54 ~ 62, isopropyl alcohol 24 ~ 30, n-hexane 16 ~ 20, benzinum 10 ~ 15.
5. the preparation method of beauty and skin care grape-kernel oil according to claim 2, is characterized in that the decolorizer of described step 7) is made up of the decolorizer of following weight portion: carclazyte 33 ~ 37, active carbon 22 ~ 26, zeolite 16 ~ 20, concave convex rod 11 ~ 15.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107586606A (en) * | 2017-10-11 | 2018-01-16 | 吉林师范大学博达学院 | A kind of extraction preparation method of grape-kernel oil |
| CN109181844A (en) * | 2018-09-14 | 2019-01-11 | 许昌鑫瑞德化工科技有限公司 | A kind of modified vegetable and animals oils extracting method |
| CN111481475A (en) * | 2020-06-03 | 2020-08-04 | 傅建斌 | Edible lipstick capable of improving female hormone and preparation method thereof |
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| CN103820203A (en) * | 2013-12-12 | 2014-05-28 | 常州现代农业科技发展有限公司 | Process for extracting tea seed oil, tea saponin and protein powder from tea seeds |
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| CN103820203A (en) * | 2013-12-12 | 2014-05-28 | 常州现代农业科技发展有限公司 | Process for extracting tea seed oil, tea saponin and protein powder from tea seeds |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107586606A (en) * | 2017-10-11 | 2018-01-16 | 吉林师范大学博达学院 | A kind of extraction preparation method of grape-kernel oil |
| CN109181844A (en) * | 2018-09-14 | 2019-01-11 | 许昌鑫瑞德化工科技有限公司 | A kind of modified vegetable and animals oils extracting method |
| CN111481475A (en) * | 2020-06-03 | 2020-08-04 | 傅建斌 | Edible lipstick capable of improving female hormone and preparation method thereof |
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