CN102631307A - Skin care composition and preparation with effect of removing acnes and acne marks and preparation method of skin care composition - Google Patents
Skin care composition and preparation with effect of removing acnes and acne marks and preparation method of skin care composition Download PDFInfo
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- CN102631307A CN102631307A CN2012100980941A CN201210098094A CN102631307A CN 102631307 A CN102631307 A CN 102631307A CN 2012100980941 A CN2012100980941 A CN 2012100980941A CN 201210098094 A CN201210098094 A CN 201210098094A CN 102631307 A CN102631307 A CN 102631307A
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Abstract
The invention discloses a skin care composition with the effect of removing acnes and acne marks. The composition comprises a phase A, a phase B and a phase C. Experiments prove that the composition has the effect of inhibiting formation of melanin and has obvious effect on inhibiting skin oil excretion; people know such symptoms as acnes and pimples are mostly caused by pathogenic bacteria and the oil excreted by the skin is exactly the best environment for the pathogenic bacteria to grow, so bacteriostasis is not enough and the living environment of the pathogenic bacteria needs to be fundamentally eliminated so as to have the effect of treating acnes and pimples; the composition has the effect of removing acnes by inhibiting oil excretion; the composition has obvious effect on treating acne marks, after the composition is used for three weeks, the acne marks of the patients are obviously improved; and the composition also has obvious effect on removing other scar tissues caused by wounds.
Description
Technical field
The present invention relates to a kind of skin care compositions, specifically a kind of skin care compositions with pox-dispelling function effect, preparation and preparation method thereof.
Background technology
Along with the progress of society, the improving constantly of living standards of the people, cosmetics become the necessary of people's life gradually from luxury goods; The kind of cosmetics is more and more; In recent years, the mask product of showing one's talent in many cosmetics of comforming receives the favor of consumer more and more deeply.
Facial film is that index is on the human body skin surface; Play the product of cleaning and the effect of protection skin; Its works principle is through the parcel of facial film to skin, lets skin and air insulated, makes skin and air insulated; Make keratodermatitis obtain replenishing of moisture contained in the facial film, wetting agent, nutrient and softening agent etc., play the effect of soft skin; Facial film also has adsorption, when peelling off facial film, can remove dirt, oils and fats and acne on the skin simultaneously, careful pore, and the skin that compacts plays good clean skin and skin care effect.
Modern medicine is thought: acne is the result of multifactor comprehensive function.At first, endocrine in the body: mainly be that the androgen secretion level increases, impels sebum secretion to enliven, increase.It is the key factor in the pathogenesis that leather bag sebaceous gland opening gets clogged.Under the situation that hair follicle blocks, propionibacterium acnes is bred in a large number, causes inflammation, forms the most basic infringement inflammatory pimple of acne (comedo).Pilosebaceous unit in obturation is inner, and a large amount of sebums, a large amount of pus cell pilosebaceous unit structural deterioration form tuberosity, cyst and sebaceous cyst, destroys skin at last even forms cicatrix.
Commercially available skin-protection product has and much has acne-removing at present, but thereby it is the effect that plays anti-acne in simple antibacterial short time, but life-time service, relapse rate is higher, and scar tissues such as pockmark pox seal are not had obvious effect.
Summary of the invention
The invention discloses a kind of skin care compositions that skin care presses down fat and pox-dispelling function effect that has.
A purpose more of the present invention is to propose a kind of skin protection dosage form of above-mentioned composition.
The 3rd purpose of the present invention is to propose a kind of method for preparing of above-mentioned skin protection dosage form.
The present invention utilizes advanced biotechnology, in conjunction with the traditional traditional Chinese medical science compatibility theory of China, in line with the principle of heat-clearing and toxic substances removing, blood circulation promoting and blood stasis dispelling, dredging the meridian, successfully develops the volcanic mud facial film with anti-acne seal effect.
A kind of volcanic mud facial film with acne-removing, the active component of this cosmetic composition contains natural minerals mud, and the effect of deep layer cleaning skin is arranged; Other compositions of the composite the present invention of volcanic mud have good facilitation to the metabolism of skin, and they can not only keep moisture of skin here, can also suppress chafing; Removing dead skin cells and oils and fats piles up; Stimulate blood circulation, softening skin, deep clean skin and purification pore; The most important thing is the pox that stays after anti-acne seal cicatrix had and well dispel effect, the scar tissue due to other wounds of skin is also had the effect of smoothing.
The concrete technical scheme that the present invention adopts is:
A kind of skin care compositions with pox-dispelling function effect, said compositions comprise that A phase, B reach the C phase mutually, and said A phase, B reach C mutually and comprise following percentage by weight raw material mutually:
Said compositions also comprises the D phase, and said D comprises following materials by weight percentage mutually:
Antiseptic 0.05～0.2wt%
Essence 0.01～0.2wt%.
A kind of method for preparing said skin care compositions, said step is following:
(1) mixing of Magnesiumaluminumsilicate and water obtains mixture solution, is heated to 60～90 ℃, homogenizing 10～40min;
(2) with B mutually in HANSHENGJIAO be added to mixing in the butanediol in advance, other do not join together in the mixture solution of step (1) with raw material and obtain mixed solution B mutually with B then;
(3) with A mutually all raw materials mix obtain mixed solution A;
(4) mixed solution A, mixed solution B are heated to 60～90 ℃ respectively, mixed solution A is gone among the mixed solution B on homogenizer, 2～5 fens kinds of homogenizing;
(5) cool and be stirred to 30～50 ℃, add C phase raw material, stir.
Be heated to 80 ℃ in the said step (1), homogenizing 20min.
Said step such as above-mentioned comprises that also step (6) adds D phase raw material, stirs.
A kind of skin care formulation with pox-dispelling function effect, said skin care formulation is processed through said method by said compositions.
Said skin care formulation is a facial film.
Described skin care compositions has the purposes in the skin care formulation of pox-dispelling function effect in preparation.
The recommendation method for using of facial film of the present invention:
Directly smear product of the present invention behind the facial cleansing, 5～10g/ time, be as the criterion with comprehensive covering skin, clean behind the reservation 15min and smeared once in 2 days, a week 3 times.
Beneficial effect of the present invention:
Through experiment confirm, the present invention has the effect that suppresses melanin formation; Secretion has significant inhibition effect to skin oil and fat; We know that mostly symptoms such as acne seat skin ulcer are that pathogen causes; And the excretory oils and fats of the skin suitable environment of pathogen growth just; Only antibacterial is not enough, plays the effect of curing acne and seat skin ulcer thereby need on root, eliminate the pathogen living environment, and the present invention plays acne-removing through the secretion of oil-control.The present invention is printed on the obvious treatment effect to pox, used for three weeks after, patient's pox is printed on tangible improvement, the scar tissue that simultaneously other wounds is caused also has significantly dispels effect.
Description of drawings
Fig. 1 uses back melanin situation of change for sample;
Fig. 2 uses back haemachrome situation of change for sample;
Fig. 3 uses back fat content situation of change for sample;
Fig. 4 uses back skin coarseness situation of change for sample;
Fig. 5 uses back skin mean depth situation of change for sample;
Fig. 6 is for using this product 4 all pox printing amount variation diagrams.
The specific embodiment
Each raw material sources of the present invention, see table 1:
Table 1
Volcanic mud is the no stickiness mud of ash to black, contains mineral, generally all is distributed in submarine volcano and volcanic island shallow sea and abyssal floor on every side.Volcanic mud is known raw material at cosmetic field, and those skilled in the art can obtain through commercially available purchase.The present invention does not have specific (special) requirements to the specifications and models of volcanic mud; So long as the volcanic mud additive of cosmetics-stage all can be used for the present invention; The invention discloses the producers that volcanic muds are sold by two families, and verify all through embodiment and can obtain result according to the invention, see table 1; The commercially available volcanic mud product of other producers all can be applicable to the present invention, and other contain the volcanic mud that also can substitute that enriches mineral and meet the cosmetics grade and are used for the present invention as raw material.
The Opuntia Streptacantha stem extract is the conventional raw material of skin care field, can obtain through commercially available purchase, also can prepare through subordinate's method, and concrete steps are:
1) with cellulose treatment Opuntia Streptacantha stem,, obtains cell pyrolysis liquid with the degradation of cell wall;
2) with the cell pyrolysis liquid enzyme denaturing, the solution left standstill behind the enzyme denaturing is got supernatant;
3) pH value to 4.2 of adjusting supernatant to wherein adding activated carbon, stirs again, filters, and collects filtrating, obtains Opuntia Streptacantha extract;
Tremella extract is the conventional raw material of skin care field, can obtain through commercially available purchase, also can prepare through subordinate's method, and concrete steps are:
1) soak Tremella with deionized water, the weight ratio of water and Tremella is 100: 1.
2) regulate between pH value to 8.5～9.0, in 85～95 ℃ of isothermal reactions 3～5 hours.
3) stir, filter, sucking filtration is collected filtrating, obtains Tremella extract.
Radix Ophiopogonis extract is the conventional raw material of skin care field, can obtain through commercially available purchase, also can prepare through subordinate's method, and concrete steps are:
1) will shred Radix Ophiopogonis with pulper, soak Radix Ophiopogonis with deionized water, the weight ratio of water and Radix Ophiopogonis is 20: 1.
2) regulate between pH value to 8.5～9.0, in 45～55 ℃ of isothermal reactions 1 hour.
3) stir, filter, sucking filtration is collected filtrating, obtains Radix Ophiopogonis extract.
The preparation of embodiment 1 facial film of the present invention
Raw material and consumption:
Method for preparing:
(1) mixing of Magnesiumaluminumsilicate and water obtains mixture solution, is heated to 70 ℃, homogenizing 15min;
(2) with B mutually in HANSHENGJIAO be added to mixing in the butanediol in advance, other do not join together in the mixture solution of step (1) with raw material and obtain mixed solution B mutually with B then;
(3) the whole mutually raw materials mix of A are obtained mixed solution A;
(4) mixed solution A, mixed solution B are heated to 70 ℃ respectively, mixed solution A is slowly poured among the mixed solution B on homogenizer, 5 fens kinds of homogenizing;
(5) cool and be stirred to 45 ℃, stir speed (S.S.) is: 30r/min, 0.5 ℃/min of rate of temperature fall; Add C phase raw material, stirring gets final product.
(6) add D phase raw material, stir, the suggestion stir speed (S.S.) is: 30r/min, back packing gets final product.
Detect data:
Even mastic or emulsion; Fragrance up to specification; PH value (25 ℃)=7.16 has cold-resistant temperature capacity, and preservation challenge is passed through; According to " diagnostic criteria of cosmetics contact dermatitis and treatment principle " criterion, embodiment 1 preparation facial film has no adverse reaction to human body skin.
The preparation of embodiment 2 mask product of the present invention
Raw material and consumption:
Method for preparing:
(1) Magnesiumaluminumsilicate and water mixing are obtained mixture solution, be heated to 60 ℃, homogenizing 10min;
(2) with B mutually in HANSHENGJIAO be added to mixing in the butanediol in advance, other do not join together in the mixture solution of step (1) with raw material and obtain mixed solution B mutually with B then;
(3) the whole mutually raw materials mix of A are obtained mixed solution A;
(4) mixed solution A, mixed solution B are heated to 80 ℃ respectively, mixed solution A is gone among the mixed solution B on homogenizer, 5 fens kinds of homogenizing;
(5) cool and be stirred to 30 ℃, stir speed (S.S.) is: 30r/min, 0.5 ℃/min of rate of temperature fall; Add C phase raw material, stir;
(6) add D phase raw material, stir, the suggestion stir speed (S.S.) is: 30r/min, back packing gets final product.
Detect data:
Even mastic or emulsion; Fragrance up to specification; PH value (25 ℃)=7.15 has cold-resistant temperature capacity preservation challenge to be passed through; According to " diagnostic criteria of cosmetics contact dermatitis and treatment principle " criterion, the volcanic mud facial film has no adverse reaction to human body skin.
The preparation of embodiment 3 mask product of the present invention
Raw material and consumption:
Method for preparing:
(1) mixing of Magnesiumaluminumsilicate and water obtains mixture solution, is heated to 90 ℃, homogenizing 40min;
(2) with B mutually in HANSHENGJIAO be added to mixing in the butanediol in advance, then with B mutually other raw materials join together in the mixture solution of step (1) and obtain mixed solution B;
(3) the whole mutually raw materials mix of A are obtained mixed solution A;
(4) mixed solution A, mixed solution B are heated to 90 ℃ respectively, mixed solution A is gone among the mixed solution B on homogenizer, 2 fens kinds of homogenizing;
(5) cool and be stirred to 50 ℃, stir speed (S.S.) is: 30r/min, 0.5 ℃/min of rate of temperature fall; Add C phase raw material, stir;
(6) add D phase raw material, stir, packing gets final product.
Detect data:
Even mastic or emulsion; Fragrance up to specification; PH value (25 ℃)=7.18 has cold-resistant temperature capacity, and preservation challenge is passed through; According to " diagnostic criteria of cosmetics contact dermatitis and treatment principle " criterion, the volcanic mud facial film has no adverse reaction to human body skin.
The preparation of embodiment 4 facial films of the present invention
Raw material and consumption:
Method for preparing:
(1) mixing of Magnesiumaluminumsilicate and water obtains mixture solution, is heated to 70 ℃, homogenizing 15min;
(2) with B mutually in HANSHENGJIAO be added to mixing in the butanediol in advance, other do not join together in the mixture solution of step (1) with raw material and obtain mixed solution B mutually with B then;
(3) the whole mutually raw materials mix of A are obtained mixed solution A;
(4) mixed solution A, mixed solution B are heated to 70 ℃ respectively, mixed solution A is slowly poured among the mixed solution B on homogenizer, 5 fens kinds of homogenizing;
(5) cool and be stirred to 45 ℃, stir speed (S.S.) is: 30r/min, 0.5 ℃/min of rate of temperature fall; Add C phase raw material, stirring gets final product.
Detect data:
Even mastic or emulsion; Fragrance up to specification; PH value (25 ℃)=7.16 has cold-resistant temperature capacity, and preservation challenge is passed through; According to " diagnostic criteria of cosmetics contact dermatitis and treatment principle " criterion, embodiment 1 preparation facial film has no adverse reaction to human body skin.
Effect experiment of the present invention
One, experimental principle
Human experimentation, the crowd forms test population by particular experiment, the variation of the dark red pigment of skin, oils and fats and skin texture degree before and after test subject makes and applies some make up, thus the anti-acne of confirming cosmetics is printed effect.And the organoleptic indicator who passes through anti-acne seal effect, thereby the anti-acne of confirming cosmetics is printed effect.
Two, experimental apparatus and sample
Instrument: dermal melanin and haemachrome tester (Mexameter MX18, German CK electronics corporation produces); Skin oil and fat tester
SM815 (Mexameter MX18, German CK electronics corporation produces): the multi-functional skin mirror of MicroSkinII image analysis system.
Three, experiment crowd and testing time
The volunteer who participates in this detection totally 30 people, sex composition at random, the age was at 20～30 years old.If there is 1 people untoward reaction to occur, then stop test during this time; The result does not find untoward reaction.
Volunteer service time: smeared once in 2 days.
Four, experimental technique
Before the experimenter smears sample, will try the experiment position earlier and clean, smear sample after drying.Experimenter's forehead (branch left and right sides two parts) is cycle labeling successively: tried region samples group and blank zone.
The experimenter make continuously apply some make up after the same weekly time carry out data acquisition.
Add up each data of gathering, the line data unitary analysis of going forward side by side.
Five, interpretation of result
1, melanin
(1) melanin content mutation analysis
Melanin content was reflected in test period, Experimental Area melanin content change with time.
As shown in Figure 1: sample was using for 1～4 week, and melanin content is on a declining curve.
2, haemachrome
(1) content of hemachrome mutation analysis
Content of hemachrome was reflected in test period, Experimental Area content of hemachrome change with time.
As shown in Figure 2: sample is after using for two weeks, and haemachrome obviously is reduction trend.
3, oils and fats
(1) fat content
The fat content variation is reflected in test period Experimental Area fat content change with time.Its value is big more, and fat content is big more, otherwise fat content is more little.
As shown in Figure 3: sample is after using for 1～4 week, and the fat content of test zone is reduction trend.
4, skin texture situation of change:
Skin coarseness (Skin Roughness SR)
Be in all sections of skin, with the difference between maximum gray scale peak value and the minimal gray peak value on the straight line.This parameter is the maximum height of skin surface unevenness.
The skin coarseness changes of contents was reflected in test period, Experimental Area skin coarseness change with time.Its value is big more, and skin coarseness is big more, otherwise skin coarseness is more little.
As shown in Figure 4: sample is after using for 1～4 week, and the skin coarseness of test zone is reduction trend.
Mean depth (Skin Smoothness Depth SSD)
Average distance between two peak values of feeling the pulse with the finger-tip mark skin mound peak (maximum gradation value curve) and sulci of skin minimum point (minimal gray curve).It is the average distance between skin surface contour line peak and the wrinkle of skin bottom line minimum point.
The variation of skin mean depth is reflected in test period Experimental Area skin mean depth change with time.Its value is big more, and the skin mean depth is big more, otherwise the skin mean depth is more little.
As shown in Figure 5: sample is after using for 1～4 week, and the skin mean depth of test zone is reduction trend.
Conclusion: sample used in 1～4 week, the skin texture of the sample sets effect that has some improvement, be embodied in the experimenter facial be the effect of skin care and wrinkle removal.
5, the organoleptic indicator of anti-acne seal effect
The pox seal is to be retained in the scar tissue on the skin after the position detumescences such as acne, acne.
Method: the pox seal of range estimation number experimenter face, statistical method adopts the overall statistic analytical method, maps.
Know that by Fig. 6 after (vertical coordinate is represented 30 people face pox seal sums among Fig. 6) sample used for three weeks, its action effect to the pox seal improved significantly.
To above-mentioned improvement, the inventor proposes the present invention might have too to the scar tissue that other wounds of removing the pox seal are brought to dispel and print and smooth effect, so carried out following experiment.
Six, the effect of scar eliminating experiment
1, experimental technique
Before the experimenter smears sample, earlier experimenter's arm experiment position (cicatrix place) is cleaned, smeared sample after drying.
The experimenter smears dosage in each test block be 3～10g/ time, smeared once in one day, and THICKNESS CONTROL requires to cover fully the cicatrix place about 2mm.Experimental session, the experimenter can not smear any cosmetics at the experiment position.
The experimenter make continuously apply some make up after the same weekly time carry out data acquisition.Used for 4 weeks.
Add up each data of gathering, the line data unitary analysis of going forward side by side.
2, experiment crowd and testing time
The volunteer who participates in this detection totally 30 people, sex composition at random, the age was at 20～45 years old.Requirement is the people that cicatrix is arranged on the arm, and the cicatrix area is controlled at 4.0～50.0cm
2, the cicatrization time is no more than 10 years, and short-term does not specifically limit for a long time, old cicatrix or newly form cicatrix and can be selected in.If there is 1 people untoward reaction to occur, then stop test during this time; The result does not find untoward reaction, and it is better newly to form the cicatrix removal effect, fairly simple wound such as slight scald, and falling down the cicatrix that stays that causes also has removal effect.
3, judgment criteria
Effectively be that the cicatrix area reduces 20% at least, skin scar place color shoals; Invalid is that cicatrix area and cicatrix place skin color have no variation; Healing is that cicatrix disappears.
4, experimental result
Effective percentage is 93.33% in 30 examples, when invalid 6.67%, and cure rate 63.33%.
Conclusion: this product has positive effect to scar eliminating.
Seven, conclusion
Comprehensive above test result draws, and its volunteer is after being to use sample:
Basic detection index from skin: oils and fats, dark red pigment and skin texture degree judge that the skin condition of its sample sets target area has the effect of improvement.
Vision index directly perceived from skin: pox seal is judged, the state that can significantly improve target skin of its sample sets, and the prolongation of the time of using with the volunteer, it improves effect and gradually is and increases progressively trend.
The inventor utilizes the product of embodiment 2～4 to experimentize again, and the result is identical with embodiment 1, does not give unnecessary details at this.
Claims (9)
1. the skin care compositions with pox-dispelling function effect is characterized in that, said compositions comprises that A phase, B reach the C phase mutually, and said A phase, B reach C mutually and comprise following percentage by weight raw material mutually:
2. the skin care compositions with anti-acne seal effect according to claim 1 is characterized in that said compositions also comprises the D phase, and said D comprises following materials by weight percentage mutually:
Antiseptic 0.05～0.2wt%
Essence 0.01～0.2wt%.
3. a method for preparing the said skin care compositions of claim 1 is characterized in that, said step is following:
(1) mixing of Magnesiumaluminumsilicate and water obtains mixture solution, is heated to 60～90 ℃, homogenizing 10～40min;
(2) with B mutually in HANSHENGJIAO be added to mixing in the butanediol in advance, other do not join together in the mixture solution of step (1) with raw material and obtain mixed solution B mutually with B then;
(3) with A mutually all raw materials mix obtain mixed solution A;
(4) mixed solution A, mixed solution B are heated to 60～90 ℃ respectively, mixed solution A is gone among the mixed solution B on homogenizer, 2～5 fens kinds of homogenizing;
(5) cool and be stirred to 30～50 ℃, add C phase raw material, stir.
4. method for preparing according to claim 3 is characterized in that, is heated to 80 ℃ in the said step (1), homogenizing 20min.
5. a method for preparing the said skin care compositions of claim 2 is characterized in that, said step such as claim 5 are said, comprises that also step (6) adds D phase raw material, stirs.
6. the skin care formulation with pox-dispelling function effect is characterized in that, said skin care formulation is processed through the said method of claim 4 by the said compositions of claim 1.
7. the skin care formulation with pox-dispelling function effect is characterized in that, said skin care formulation is processed through the said method of claim 5 by the said compositions of claim 2.
8. according to claim 6 or 7 described skin care formulations, it is characterized in that said skin care formulation is a facial film.
9. claim 1 or 2 described skin care compositionss have the purposes in the skin care formulation of pox-dispelling function effect in preparation.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210098094.1A CN102631307B (en) | 2012-04-05 | 2012-04-05 | Skin care composition and preparation with effect of removing acnes and acne marks and preparation method of skin care composition |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210098094.1A CN102631307B (en) | 2012-04-05 | 2012-04-05 | Skin care composition and preparation with effect of removing acnes and acne marks and preparation method of skin care composition |
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| CN102631307A true CN102631307A (en) | 2012-08-15 |
| CN102631307B CN102631307B (en) | 2014-06-04 |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1263761A (en) * | 1999-02-03 | 2000-08-23 | 黑龙江东实天然美容品有限公司 | Volcano and spring mineral mask |
| CN102000006A (en) * | 2010-12-03 | 2011-04-06 | 北京工商大学 | Skin care composite and preparation with function of eliminating facial redness and preparation methods thereof |
-
2012
- 2012-04-05 CN CN201210098094.1A patent/CN102631307B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1263761A (en) * | 1999-02-03 | 2000-08-23 | 黑龙江东实天然美容品有限公司 | Volcano and spring mineral mask |
| CN102000006A (en) * | 2010-12-03 | 2011-04-06 | 北京工商大学 | Skin care composite and preparation with function of eliminating facial redness and preparation methods thereof |
Non-Patent Citations (2)
| Title |
|---|
| 佚名: "MG美即火山泥面膜", 《HTTP://COSME.PCLADY.COM.CN/PRODUCT/93356.HTML》 * |
| 阿芳: "AVON护肤全体验", 《产品&商机》 * |
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