CN102628224A - One-bath, multi-color dyeing method for multi-component superfine fibers - Google Patents
One-bath, multi-color dyeing method for multi-component superfine fibers Download PDFInfo
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- CN102628224A CN102628224A CN2012100981639A CN201210098163A CN102628224A CN 102628224 A CN102628224 A CN 102628224A CN 2012100981639 A CN2012100981639 A CN 2012100981639A CN 201210098163 A CN201210098163 A CN 201210098163A CN 102628224 A CN102628224 A CN 102628224A
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Abstract
The invention relates to a one-bath, multi-color dyeing method for multi-component superfine fibers. At present, the two-bath, two-step method is usually adopted as the dyeing method for multi-component superfine fibers, the flow is long, the production cost is high, a great deal of time and energy are consumed, and the production efficiency is low. Colors are matched according to the coloring laws of dyes and fibers, i.e., with superfine polyester fibers, superfine polyester-cotton compound fibers and cationic dyeable superfine polyester fibers as materials and disperse dye, acid dye and cationic dye as dyes, multi-color schemes are combined and mixed; and by means of the sequential arrangement of feeding, the preparation and usage of anti-setting agent and a multi-stage heating process realizing the separate dyeing of the fibers corresponding to the dyes, the one-bath, multi-color dyeing of the multi-component superfine fibers are realized. The products dyed by the method disclosed by the invention have two or more different colors and good washing fastness and rubbing fastness, and are vivid, the dyeing effect is equal to the dyeing effect of the two-bath method, however, the dyeing process is simplified, and the consumption of chemicals, water and steam is reduced.
Description
Technical field
The present invention relates to one of a kind of multicomponent superfine fibre and bathe the polychromatic dyeing method, particularly a kind of one of yin, yang ionic dye co-bathing dyeing that uses is bathed process for realizing multi-color dying, is applicable to the multicolour cloth dyeing of blending of multicomponent superfine fibre or intertexture.
Background technology
The superfine fibre fiber number is superfine, and specific area is big, and capillary effect is good, has good gloss and moisture absorption and looses moistly, is widely used in multiple fields such as clean wiping cloth, high quality artificial skin, filtration, health care, labour protection.
Present superfine fibre is main with terylene, polyamide composite filaments mainly.Terylene adopts disperse dyeing usually; Polyamide fibre can adopt acidity, neutrality and REACTIVE DYES direct dyeing, also can adopt disperse dyeing.In recent years, because the development of cation-modified terylene, the cationic-dyeable terylene is external except that using terephthalic acid (TPA) and glycol monomethyl in polycondensation process; Introduced again and contained sulfonic monomer, therefore, DISPERSE DYES can on dye; Tinctorial yield is higher than terylene, cation dyes also can on dye.Terylene, cationic-dyeable terylene and wash normally two one-bath two-step process of bright and beautiful coloration of textile materials method, but these method flows are long, production cost is high, time-consuming power consumption, and production efficiency is low.
Therefore, how to utilize one to bathe one-step method, realize that polychrome is dyed in the same bath of DISPERSE DYES, ACID DYES and cation dyes; Solve the yin, yang ionic dye with bathing sedimentation problem, accomplish both to improve multi-level tone, can improve the utilization rate of dyestuff again; Energy-conserving and environment-protective are current urgent problems.
Summary of the invention
The purpose of this invention is to provide a kind of cycle lack, can match colors, fastness is good, the multicomponent superfine fibre of energy-and time-economizing one bathe the polychromatic dyeing method.
For this reason; Technical scheme of the present invention is so to realize: one of a kind of multicomponent superfine fibre is bathed the polychromatic dyeing method; May further comprise the steps: 1) match colors according to the painted rule of dyestuff and fiber: with super fine polyester silk, superfine polyamide compound silk and cationic-dyeable super fine polyester silk is raw material; With DISPERSE DYES, ACID DYES and cation dyes is dyestuff, combination allotment three look schemes and Liu Bai scheme; 2) feed intake: throw in the dye vat of calgon to high temperature-pressure dyeing machine; Be warming up to 60 ℃ then; Regulate the pH value to 4.5-5 with acetic acid and sodium acetate, throw fabric, join in the dye vat successively by the order of ACID DYES, DISPERSE DYES, antiprecipitant, cation dyes; 3) intensification dyeing stage by stage: heat up after the capping and divide three phases, the phase I, 60 ℃-80 ℃, programming rate is 1 ℃/min, 80 ℃ of insulation 8-12min; Second stage, 80 ℃-100 ℃, programming rate is 1 ℃/2min, 100 ℃ of insulation 8-12min; The 3rd section, 100 ℃-120 ℃, programming rate is 1 ℃/min, 120 ℃ of continuous 25-35min that dye, and the continuous back that finishes of dying lowers the temperature the raffinate of in the time of 65-75 ℃, draining with the speed of 3 ℃/min; 4) post processing comprises and soaps, washes three times, softness, dehydration, drying etc.
As further technical scheme; In the step 1) in the three look schemes: the color of super fine polyester silk is by dying acquisition on the DISPERSE DYES; The color of superfine polyamide compound silk is obtained by DISPERSE DYES and ACID DYES colorant match, and the color of cationic-dyeable super fine polyester silk is obtained by DISPERSE DYES and cation dyes colorant match; Stay in the white scheme, stay and do not use DISPERSE DYES when white, staying white part is the super fine polyester silk.
As further technical scheme, step 2) middle fabric input is preceding need be in advance through opening fibre.
As further technical scheme; Step 2) in; The composition of each material is following in the dye vat: ACID DYES 0.1 ~ 4% (o.w.f), DISPERSE DYES 0.1 ~ 8% (o.w.f), cation dyes 0.1 ~ 6% (o.w.f), antiprecipitant 0.4ml/L, calgon 1g/L, sodium acetate 1g/L and acetic acid; The used percentage (o.w.f) of above-mentioned dyestuff is to be the percentage of benchmark with the fabric weight, and bath raio is 1:10-25.
As further technical scheme, work in the step 3) that to dye temperature be 60 ℃, throw in ACID DYES, DISPERSE DYES running 8-12min earlier after, then throw in antiprecipitant, throw in cation dyes again behind the running 4-8min, above-mentioned dyestuff dissolves before input.
Preparation in the face of color matching and antiprecipitant is elaborated down.
1. three looks: super fine polyester silk (abbreviation terylene) dyes kind of the color " A " of winning with DISPERSE DYES; Go up color at superfine polyamide compound silk (brocade washed in abbreviation) and superpose with disperseing color " A-", go up by cation dyes C and color " A+ " stack at cationic-dyeable super fine polyester silk (being called for short sun washs) by ACID DYES color B.Fiber is seen table 1 with the corresponding colour developing relation of dyestuff.
The colour developing principle of table 1 fiber and dyestuff
In the table, the expression of color " A-" and color " A+ " with color " A " though form and aspect identical, slightly variant on the depth.
2. stay white: terylene stays white (promptly not using DISPERSE DYES), wash the brocade with ACID DYES polyamide fibre is caught first kind of color, with cation dyes to cationic-dyeable super fine polyester wire coloring.Fiber is seen table 2 with the corresponding colour developing relation of dyestuff.
The colour developing principle of table 2 fiber and dyestuff
The preparation of antiprecipitant: it is mixed by 7: 12: 1 mass ratioes by paregal O (AEO O-25), dispersant IW (AEO), dispersant A ES (sodium sulfate of polyethenoxy ether of fatty alcohol).Earlier paregal O and dispersant IW are poured in the water in proportion, heating is warming up to about 60 while stirring, AES is added wherein again, stirs, and AES is dissolved fully, and is for use.
The present invention utilizes the different component polyester fiber with dying principle to ACID DYES, DISPERSE DYES and dispersible cationic dyestuff on different in bathing, and then produces the multi-level color Overlay.Process is added antiprecipitant, is utilized conditioning agent adjustment pH value in the time of 60 ℃; Add cation dyes, DISPERSE DYES and ACID DYES, intensification fixation, the several steps of soaping; Adopt rational allotment scheme, blanking time and intensification control, dyestuff is formed on the variety classes polyester fiber stablize chemical bond and fixation.The present invention dyes unique multi-level color effect with simple technology, and loose colour degree of offering sacrifice to gods with hogs and sheep is good, and reduces the energy and discharge of wastewater, saves production cost.
On the method for the invention reaches in same dye bath dyestuff and fiber corresponding independent, dye, realize that of multicomponent superfine fibre bathes polychromatic dyeing; The product that obtains after the dyeing has good washing fastness and fastness to rubbing; And bright in colour, Color is identical with two-bath process, but has simplified dyeing process; Reduced the consumption of chemicals, water, steam, and a kind of processing method easily is provided for polychrome superfine fibre Products Development.The present invention mainly is applicable to a bath polychromatic dyeing of superfine fibre, is applicable to that equally also of multicomponent chemical fiber bathes polychromatic dyeing.
Below in conjunction with the Figure of description and the specific embodiment the present invention is further described.
Description of drawings
Fig. 1 is trichrome stain process curve figure of the present invention.
Fig. 2 is white dyeing curve map for the present invention stays.
Fig. 3 is the former state full face.
Fig. 4 is a former state reverse side photo.
Fig. 5 stays the positive effect after white for former state.
Fig. 6 stays the reverse side effect after white for former state.
The specific embodiment
Material therefor of the present invention is a multicomponent superfine fibre tufted blanket, and shown in Fig. 3 full face, Fig. 4 reverse side photo, its composition is seen table 3.
Table 3 tufted blanket composition
| The position | Raw material |
[0033]
| A left side 4 rows | 1. network yarn (washing DTY entirely) 150D/288F half light |
| In 4 row | 2. superfine polyamide compound silk 175D/72F * 16 |
| Right 2 rows | 3. cationic-dyeable super fine polyester silk 150D/288F |
| Base material | Terylene |
The first step, colour planning:
(1) three look
(2) stay white
| The position | The design look | DISPERSE DYES | ACID DYES | Cation dyes |
| A left side 4 rows | White | Do not have | ? | ? |
| In 4 row | Blue | ? | Acid blue 80 0.5% | ? |
| Right 2 rows | Red | ? | ? | Cationic Red X-GRL 1% |
In second step, open fibre: 1. open fibre: liquid caustic soda (38Be ') 20g/L; Clever 1g/L deoils; 100 ℃ * 50min.
The 3rd step, dyeing.Antiprecipitant 0.6ml/L, calgon 1g/L is the pH stabilizing agent with sodium acetate 1/L, regulates pH=5 with acetic acid, bath raio 1: 20.
The technology of trichrome stain is following: throw in the dye vat of calgon to high temperature-pressure dyeing machine, be warming up to 60 ℃, throw fabric; Regulate the pH value with acetic acid and sodium acetate, the dyestuff that has dissolved is added by process sequence in the dye vat of high temperature-pressure dyeing machine successively, add ACID DYES, DISPERSE DYES earlier; Treat to add antiprecipitant behind the machine cycle 10min; Rerun and add the dyeing that heats up stage by stage after cation dyes, the capping, phase I, 60 ℃-80 ℃ behind the 5min; Programming rate is 1 ℃/min, 80 ℃ of insulation 10min; Second stage, 80 ℃-100 ℃, programming rate is 1 ℃/2min, 100 ℃ of insulation 10min; The 3rd section, 100 ℃-120 ℃, programming rate is 1 ℃/min, 120 ℃ of continuous dying 30 minutes, and the continuous back that finishes of dying lowers the temperature with 3 ℃/minute speed, and the raffinate of in the time of 70 ℃, draining is soaped, and washes three times, and the three color process curve is as shown in Figure 1.
Stay white technology following: to throw in the dye vat of calgon to high temperature-pressure dyeing machine, be warming up to 60 ℃, throw fabric; Regulate the pH value with acetic acid and sodium acetate, the dyestuff that has dissolved is added by process sequence in the dye vat of high temperature-pressure dyeing machine successively, add ACID DYES earlier, treat the machine cycle; Add antiprecipitant behind the 5min, rerun and add behind the 5min dyeing that heats up stage by stage after cation dyes, the capping, phase I; 60 ℃-80 ℃, programming rate is 1 ℃/min, 80 ℃ of insulation 10min; Second stage, 80 ℃-100 ℃, programming rate is 1 ℃/2min, 100 ℃ of insulation 40min, the continuous back that finishes of dying lowers the temperature with 3 ℃/minute speed, and the raffinate of in the time of 70 ℃, draining is soaped, and washes three times, and the three color process curve is as shown in Figure 1.Stay white process curve as shown in Figure 2.
The 4th step, softness: softener 2～3%; PH 5.0; 70 ℃ * 10min.Stay white effect Fig. 5, shown in Figure 6.
(4) dyeing COLOR FASTNESS
Adopt GB/T3921-2008 textile color stability test method, the friction and the soaping fastness of test dyeing tufted blanket.Its result sees table 4, shown in the table 5.
Table 4 crock fastness experimental result
| Sample | Dry friction | Wet friction |
| Stay white sample | 5 | 4~5 |
| Three look samples | 5 | 4 |
Annotate: the crock fastness test is the reverse side of dyeing tufted blanket sample
The table 5 look experimental result of soaping
| COLOR FASTNESS | Stay white sample | Three look samples |
| The former state variable color | 4~5 | 4~5 |
| Triacetate staining | 4~5 | 4~5 |
| Bleach cotton staining | 4~5 | 4~5 |
| Polyamide fiber staining | 4~5 | 4~5 |
| Polyester fiber staining | 5 | 4~5 |
| Polyacrylonitrile fibre staining | 4~5 | 4~5 |
| Viscose staining | 4~5 | 4~5 |
Claims (5)
1. one of a multicomponent superfine fibre bathe the polychromatic dyeing method; May further comprise the steps: 1) match colors according to the painted rule of dyestuff and fiber: with super fine polyester silk, superfine polyamide compound silk and cationic-dyeable super fine polyester silk is raw material; With DISPERSE DYES, ACID DYES and cation dyes is dyestuff, combination allotment three look schemes and Liu Bai scheme; 2) feed intake: throw in the dye vat of calgon to high temperature-pressure dyeing machine; Be warming up to 60 ℃ then; Regulate the pH value to 4.5-5 with acetic acid and sodium acetate, throw fabric, join in the dye vat successively by the order of ACID DYES, DISPERSE DYES, antiprecipitant, cation dyes; 3) intensification dyeing stage by stage: heat up after the capping and divide three phases, the phase I, 60 ℃-80 ℃, programming rate is 1 ℃/min, 80 ℃ of insulation 8-12min; Second stage, 80 ℃-100 ℃, programming rate is 1 ℃/2min, 100 ℃ of insulation 8-12min; The 3rd section, 100 ℃-120 ℃, programming rate is 1 ℃/min, 120 ℃ of continuous 25-35min that dye, and the continuous back that finishes of dying lowers the temperature the raffinate of in the time of 65-75 ℃, draining with the speed of 3 ℃/min; 4) post processing.
2. one of multicomponent superfine fibre according to claim 1 is bathed the polychromatic dyeing method; It is characterized in that; In the said step 1) in the three look schemes: the color of super fine polyester silk is by dying acquisition on the DISPERSE DYES; The color of superfine polyamide compound silk is obtained by DISPERSE DYES and ACID DYES colorant match, and the color of cationic-dyeable super fine polyester silk is obtained by DISPERSE DYES and cation dyes colorant match; Stay in the white scheme, stay and do not use DISPERSE DYES when white, staying white part is the super fine polyester silk.
3. one of multicomponent superfine fibre according to claim 1 and 2 is bathed the polychromatic dyeing method, it is characterized in that said step 2) in, need before the fabric input in advance through opening fibre.
4. one of multicomponent superfine fibre according to claim 1 and 2 is bathed the polychromatic dyeing method; It is characterized in that; Said step 2) in; The composition of each material is following in the dye vat: ACID DYES 0.1～4%, DISPERSE DYES 0.1～8%, cation dyes 0.1～6%, antiprecipitant 0.4ml/L, calgon 1g/L, sodium acetate 1g/L and acetic acid; bath raio is 1: 10-25, the used percentage of above-mentioned dyestuff are to be the percentage of benchmark with the fabric weight, and described antiprecipitant is the compound that paregal O, dispersant IW, dispersant A ES are formed by 7: 12: 1 mass ratio.
5. one of multicomponent superfine fibre according to claim 4 is bathed the polychromatic dyeing method; It is characterized in that, in the said step 3), work that to dye temperature be 60 ℃; After throwing in ACID DYES, DISPERSE DYES running 8-12min earlier; Then throw in antiprecipitant, throw in cation dyes again behind the running 4-8min, above-mentioned dyestuff dissolves before input.
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| CN113550157A (en) * | 2021-08-23 | 2021-10-26 | 福建漳平协龙高新化纤有限公司 | Multi-component jacquard material one-bath process multicolor dyeing method |
| CN115717339A (en) * | 2022-11-23 | 2023-02-28 | 福建省新宏港纺织科技有限公司 | One-bath dyeing process for multi-material shoe material fabric |
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