CN104018369B - Silk intertexture jacquard fabric dyeing - Google Patents
Silk intertexture jacquard fabric dyeing Download PDFInfo
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- CN104018369B CN104018369B CN201410272331.0A CN201410272331A CN104018369B CN 104018369 B CN104018369 B CN 104018369B CN 201410272331 A CN201410272331 A CN 201410272331A CN 104018369 B CN104018369 B CN 104018369B
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Abstract
Silk intertexture jacquard fabric dyeing, belongs to silk intertexture jacquard fabric staining technique field.This technique comprises dye fixing-wash-soap-two roads together to wash-go out cylinder baking step; In dye fixation step, the silk intertexture jacquard fabric through pre-treatment is put into active dye liquor, adopt dye gigging method to dye, dyeing temperature keeps 80 ~ 85 DEG C, and dyeing time is 60 ~ 200 minutes; Active dye liquor adopts orchid to receive uniformly dyeing material 1 ~ 5%owf, HE type dye 1 ~ 5%owf, glauber salt 20 ~ 50g/L, sodium carbonate 5 ~ 20g/L to mix with water and obtain.Technique of the present invention can realize silk fiber in silk intertexture jacquard fabric and cellulose fibre upper one-bath dyeing when contaminating different colours respectively, and the silk intertexture jacquard fabric COLOR FASTNESS of the two-color effect obtained can reach two bath process fastness, simultaneously energy-saving and emission-reduction, obviously shorten the technique used time.
Description
Technical field
Silk intertexture jacquard fabric dyeing, belongs to silk intertexture jacquard fabric staining technique field.
Background technology
Silk intertexture jacquard fabric, can not only embody the softness of silk and smooth, can also embody the next to the skin and comfortable of cellulose fibre simultaneously, promotes grade and class that fabric uses.Be different from silk fiber and cellulose fibre in common silk flosssilk wadding MIXED FABRIC and contaminate the design that can only contaminate same color, in silk intertexture jacquard fabric, also there is the design of double-colored silk intertexture jacquard fabric.The design of double-colored silk intertexture jacquard fabric adopt silk fiber and cellulose fibre respectively on contaminate different colours, namely silk fiber contaminates a kind of color, cellulose fibre contaminates another kind of color.The design of double-colored silk intertexture jacquard fabric can make the jacquard weave region on silk intertexture jacquard fabric have third dimension and stereovision, obtains a kind of silk intertexture jacquard fabric with two-color effect.Silk intertexture jacquard fabric pattern can not wash with water, no matter through how many times washing, can keep all the time as newly, can not bleach or become ash.
Adopt single bath process to solve the inconsistent problem of two kinds of fiber Dry Sacks to the dyeing of silk flosssilk wadding MIXED FABRIC although exist in prior art, when the method can only make silk fiber and cellulose fibre contaminate same color, Dry Sack is consistent.Namely the inconsistent problem of dye-uptake when prior art can only solve improvement two kinds different fiber dye same color.But the one-bath dyeing that cannot realize when silk fiber and cellulose fibre two kinds of fibers contaminate different colours.Applicant finds under study for action: when the silk fiber in silk intertexture jacquard fabric and cellulose fibre above contaminate different colours respectively, because silk fiber and cellulose fibre belong to the fiber without type respectively, two kinds of fibers contaminate condition difference, though active dyestuff is all painted to two kinds of fibers, but upper dye is unstable, impact by dyeing condition is comparatively large, and a traditional bath process is difficult to reach two tone dyeing effect.And neutral dye and direct blend dye one-bath process, chromatogram is incomplete, color is not bright-coloured, COLOR FASTNESS is very poor, and the staining of direct blend dye on two kinds of fibers is also uncontrollable, does not reach weaving face fabric standard.Traditional one-bath dyeing, stability and poor controllability, do not reach two-color effect.
Therefore in prior art when the silk fiber in silk intertexture jacquard fabric and cellulose fibre respectively upper contaminate different colours time, two bath process can only be adopted dye.First immerse the first dye liquor by silk intertexture jacquard fabric to dye to a kind of fiber in silk and cotton, after repeatedly washing, again this fabric is immersed the second dye liquor to dye to the another kind of fiber in silk and cotton, then obtain double-colored silk intertexture jacquard fabric through washing soap washing.Existing two bath process needs the used discarded dye liquor of twice discharge, and also needs repeatedly to wash between two baths.Under mass production conditions, enterprise often consumes thousands of even water resource of up to ten thousand cubes day by day, and existing two bath process not only adds wastewater discharge, also add by water cost and cost for wastewater treatment.Further, its technological process of dyeing of existing two-bath process silk intertexture jacquard fabric is long, time-consuming power consumption, causes the production efficiency of the silk intertexture jacquard fabric of this two-color effect lower, in a disguised form adds production cost.
Summary of the invention
Silk flosssilk wadding the technical problem to be solved in the present invention of the present invention is: overcome the deficiencies in the prior art, silk intertexture jacquard fabric dyeing is provided, this energy saving technology reduces discharging, obviously shortens the technique used time, can realize silk fiber in silk intertexture jacquard fabric and cellulose fibre upper one-bath dyeing when contaminating different colours respectively, and the silk intertexture jacquard fabric COLOR FASTNESS of the two-color effect obtained obviously is better than the fabric that two bath process obtains.
The technical solution adopted for the present invention to solve the technical problems is: this silk intertexture jacquard fabric dyeing, and comprise dye fixing-wash together-soap-two road washing-adjust ph-go out cylinder baking step, concrete operations are as follows:
Dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 80 ~ 85 DEG C, and dyeing time is 60 ~ 200 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of described dye liquor is: adopt orchid to receive uniformly dyeing material 0.1 ~ 2.5%owf, HE type dye 0.05 ~ 4%owf, glauber salt 40 ~ 60g/L, sodium carbonate 5 ~ 8g/L and mix with water and obtain;
Described silk intertexture jacquard fabric is that silk fiber and the jacquard weave of cellulose fibre intertexture form.
The collocation method of described dye liquor is: adopt orchid to receive uniformly dyeing material 2.0%owf, HE type dye 1.5%owf, glauber salt 50g/L, sodium carbonate 5g/L mixes with water, acquisition dye liquor.
In described staining procedure, dyeing temperature keeps 80 DEG C, and dyeing time is 120 minutes.
Described cellulose fibre is cotton fiber, tencel fiber or viscose.
The washing temperature of described washing is together 45 ~ 60 DEG C, effluent discharge after cleaning, and repeats above operation 1 ~ 3 time.
Described concrete steps of soaping are: by the aqueous cleaning silk intertexture jacquard fabric adding 1 ~ 4g/L ten diamino benzene sulfonic acid sodium, water temperature 90 ~ 95 DEG C, and cleaning terminates rear effluent discharge, and repeats above step 2 ~ 4 time.
The concrete steps of described two road washings are: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 90 ~ 95 DEG C, terminate rear effluent discharge, and repeat above step 2 ~ 4 time.
The concrete steps of described adjust ph are: add aqueous solution soaking silk intertexture jacquard fabric, and the acetic acid adding 0.5 ~ 4g/L regulates aqueous solution pH to 7, terminates rear effluent discharge, and repeats above step 2 ~ 4 time.
Described go out cylinder dry bake out temperature be 100 ~ 110 DEG C.
Be described as follows of the present invention: applicant adopts hair Lan Nasu (LANASOL) dyestuff containing alpha-brominated acrylamide active group and the HE type REACTIVE DYES containing a two chloro-s-triazine active group in step 1).Lan Nasu (LANASOL) dyestuff is a kind of reactive dye for wool containing bromo acrylamide group, adopts dyeing wool fabric on Lan Nasu (LANASOL) dyestuff in prior art more.When applicant finds that uniformly dyeing material contaminates silk fiber to adopt orchid to receive: the blue uniformly dyeing material of receiving of the hair containing alpha-brominated acrylamide active group can make the silk fiber of upper dye have good light fastness and wet fastness, amino in silk fiber and the bromopropene amide groups generation covalent bonds in dyestuff, but simultaneously orchid receives uniformly dyeing material and can not go up dye cellulose fibre (as cotton fiber, tencel fiber or viscose), makes silk fiber a kind of color of upper dye separately; HE type REACTIVE DYES containing a two chloro-s-triazine active group only on contaminate cellulose fibre, the hydroxyl in cellulose fibre and the active group in dyestuff form firmly covalent bonds, and not on contaminate silk fiber, make cellulose fibre to contaminate another kind of color.
Preferably, in the present invention orchid used receive element (LANASOL) dyestuff be Hensel step (Huntsman) company produce.The present invention's HE type dye used is that Yongguang Chemical Industry Co., Ltd., Taiwan produces.Described orchid receives element (LANASOL) dyestuff and contains bromo acrylamide group; Described HE type REACTIVE DYES contains a two chloro-s-triazine active group.The silk intertexture jacquard fabric after pre-treatment described in dye fixation step, its pre-treating method is existing conventional pre-treating method.
Applicant finds in actual production: on double-colored silk intertexture jacquard fabric in dye process, there is the problem that two kinds of colors that silk fiber and cellulose fibre above contaminate respectively are infected with mutually sometimes, namely silk fiber is infected with the color that cellulose fibre contaminates, cellulose fibre is infected with the color that silk fiber contaminates.This problem easily causes that the double-colored contrast effect of silk intertexture jacquard fabric is outstanding, fabric color not just, the stereoscopic visual effect of fabric jacquard weave is poor.Applicant finds to affect the factor whether two kinds of fibers be infected with mutually after deliberation: the middle orchid of dyeing temperature, dye liquor receives the degree (unit %owf) of uniformly dyeing material and HE type REACTIVE DYES, the selection of auxiliary component and consumption.Applicant finally determines that the optimum process condition that two kinds of fibers can be avoided mutually to be infected with is after deliberation: dyeing temperature keeps 80 ~ 85 DEG C, and dyeing time is 60 ~ 200 minutes; Adopt orchid to receive uniformly dyeing material 0.1 ~ 2.5%owf, HE type dye 0.05 ~ 4%owf, glauber salt 40 ~ 60g/L, sodium carbonate 5 ~ 8g/L to mix with water and obtain.In step 1), optimum dyeing temperature Yin Lanna uniformly dyeing material contaminating silk fiber is 80 DEG C, and optimum dyeing temperature HE type REACTIVE DYES contaminating cotton fiber is 80 DEG C.It is all larger that orchid receives the dependency to glauber salt of uniformly dyeing material and HE type dye, especially orchid receives uniformly dyeing material at more than 0.5%owf, glauber salt consumption can not lower than 50g/L, the main technological parameter that dyes is all consistent, so dye to two fibers with bath, reach differential upper dye and the object be not infected with mutually.Dyeing time 60 ~ 200 minutes, refers to the dye gigging process total used time into silk intertexture jacquard fabric, immerses dye liquor and starts timing, be separated into end with silk intertexture jacquard fabric and dye liquor with silk intertexture jacquard fabric.Dyeing temperature refers to the temperature of dye liquor, and in dyeing course, dyeing temperature is steady state value, and optimum dyeing temperature range is 80 ~ 85 DEG C.Temperature is too high, and REACTIVE DYES can be hydrolyzed, and affect the dye-uptake of dyestuff, temperature is too low, and dyestuff reaction is slow, causes dye-uptake low, firm not with the reaction bonded of fiber, affects COLOR FASTNESS, and the problem be mutually infected with can occur.And study through applicant and find that this technological temperature condition is when upper dye is using cotton fiber, tencel fiber or viscose as cellulose fibre, between the fabric silk fiber obtained and cellulose fibre, upper dye color is neither infected with mutually, and COLOR FASTNESS is optimum.
In the present invention, %owf is the degree of dyestuff, refers to the consumption of dyestuff during dyeing and the ratio of fabric weight; Such as: the fabric contaminating 100 kilograms, dye dosage is the dyestuff that 4%owf contaminates these fabric needs: 100x0.04=4 kilograms in other words.The usual method for expressing in this area is % (owf) or (%owf), in order to avoid occurring that bracket causes the ambiguity of protection domain in the claims, is therefore abbreviated as %owf in this patent.
Compared with prior art, the beneficial effect that silk intertexture jacquard fabric dyeing of the present invention has is:
1, dyeing of the present invention can shorten the technique used time, thus enhances productivity.Because existing textile dyeing field mostly is customer order production model.Customer order production model and enterprise are according to the customer requirement upper silk intertexture jacquard fabric having contaminated fixed qty at the appointed time; Therefore in textile dyeing field, the raising of dyeing rate plays important effect for the raising market competitiveness.Existing two bath process technique total used time is more than 6 hours.And present invention process total used time is 2 ~ 3 hours, the technique used time contaminating double-colored silk intertexture jacquard fabric compared to existing technology shortens one times, improves dyeing rate, reduces production cost.
2, dyeing of the present invention has the effect of energy-saving and emission-reduction.In textile dyeing technical field, enterprise's consumption of water every day day can reach thousands of, upper ten thousand stere.The larger specific gravity of production cost is accounted for by the expense of water consumption.The present invention can adopt one-bath dyeing, obtains double-colored silk intertexture jacquard fabric.The comparable existing two bath process technique of water consumption of the present invention save 40 ~ 50% use water.In textile dyeing technical field, discharge of wastewater is the major pollutants in production process, and enterprise needs a large amount of fund of cost to carry out wastewater treatment, can discharge.The present invention adopts one-bath dyeing, only need discharge the discarded dye liquor of once finishing using; And in prior art, adopt two-bath process to need twice discharge to finish using discarded dye liquor.The discharging of waste liquid amount of technique of the present invention decreases half than prior art compared to existing technology, decreases wastewater treatment capacity, improves economic benefit.
3, technique of the present invention not only may be used for, in silk intertexture jacquard fabric, silk fiber and celluse fiber one-bath contaminate same color, also can be used for the color that in silk intertexture jacquard fabric, on silk fiber and celluse fiber one-bath, dye two kinds is different.The silk intertexture jacquard fabric that the present invention obtains goes up dye two kinds of different colours respectively due to silk and cotton two kinds of fibers, and fabric has heterochromatic stereoeffect.And through the silk intertexture jacquard fabric dyeing that testing identity technique of the present invention obtains, make dyeing and color controlling simple, abundant exhibiting textile design style, color, flower pattern effect, the heterochromatic stereoeffect of outstanding high-grade silk intertexture jacquard fabric, increase novel degree, meet dyeing and finishing process matched therewith demand and the market demand of novel fabric.Adopt the double-colored silk intertexture jacquard fabric that technique of the present invention contaminates, the color contrast that the color that silk fiber contaminates and cellulose fibre contaminate is clear, and the color that two kinds of fibers contaminate is without being mutually infected with phenomenon.The silk intertexture jacquard fabric of the two-color effect that technique of the present invention obtains, its COLOR FASTNESS can reach the fabric that two bath process obtains, and the fabric that the present invention obtains all has excellent performance in fastness to rubbing, washing fastness, fastness to perspiration and fastness to soaping.
Detailed description of the invention
Embodiment 1 ~ 5 is detailed description of the invention of silk intertexture jacquard fabric dyeing of the present invention.Wherein embodiment 1 is most preferred embodiment.Embodiment and comparative example orchid used receive element (LANASOL) dyestuff be Hensel step (Huntsman) company produce.The present invention's HE type dye used is Yongguang Chemical Industry Co., Ltd., Taiwan's production.In embodiment and comparative example, pre-treating method is existing conventional pre-treating method.
embodiment 1
Blue flash orange dyed by the silk intertexture jacquard fabric that will silk fiber and cotton fiber jacquard weave be adopted to interweave in the present embodiment, its method as follows:
1) dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 80 DEG C, and dyeing time is 120 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of dye liquor is: orchid receives uniformly dyeing material 2.0%owf, and HE type dye 1.5%owf, glauber salt 50g/L, sodium carbonate 5g/L mix with water and obtain; This formula can make silk fiber contaminate blue, and cotton fiber contaminates orange;
2) washing together: add water and be warming up to 45 DEG C, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 3 time;
3) soap: by the aqueous cleaning silk intertexture jacquard fabric adding 3g/L ten diamino benzene sulfonic acid sodium, water temperature 95 DEG C, cleaning terminates rear effluent discharge, and repeats above step 4 time;
4) two road washings: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 95 DEG C, terminate rear effluent discharge, and repeat above step 2 time;
5) regulate PH: add aqueous solution soaking silk intertexture jacquard fabric, the acetic acid adding 1 ~ 2g/L regulates solution ph to 7, terminates rear effluent discharge, and repeats above step 3 time;
7) fabric goes out cylinder and dries: silk intertexture jacquard fabric goes out cylinder and dries at 100 ~ 110 DEG C, to obtain final product.
embodiment 2
It is golden that bright red sudden strains of a muscle dyed by the silk intertexture jacquard fabric that will silk fiber and cotton fiber jacquard weave be adopted to interweave in the present embodiment, its method as follows:
1) dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 85 DEG C, and dyeing time is 80 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of dye liquor is: orchid receives uniformly dyeing material 2.0%owf, and HE type dye 4%owf, glauber salt 50g/L, sodium carbonate 8g/L mix with water and obtain; This formula can make silk fiber contaminate to obtain large red, and cotton fiber contaminates golden;
2) washing together: add water and be warming up to 60 DEG C, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 2 time;
3) soap: by the aqueous cleaning silk intertexture jacquard fabric adding 2g/L ten diamino benzene sulfonic acid sodium, water temperature 90 DEG C, cleaning terminates rear effluent discharge, and repeats above step 2 time;
4) two road washings: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 95 DEG C, terminate rear effluent discharge, and repeat above step 2 time;
5) regulate PH: add aqueous solution soaking silk intertexture jacquard fabric, the acetic acid adding 3 ~ 4g/L regulates solution ph to 7, terminates rear effluent discharge, and repeats above step 3 time;
6) fabric goes out cylinder and dries: silk intertexture jacquard fabric goes out cylinder and dries at 100 ~ 110 DEG C, to obtain final product.
embodiment 3
In the present embodiment, the silk viscose glue intertexture jacquard fabric adopting silk fiber and viscose jacquard weave to interweave is dyed blue flash cream-coloured, its method as follows:
1) dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 80 DEG C, and dyeing time is 100 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of dye liquor is: orchid receives uniformly dyeing material 2.50%owf, and HE type dye 0.05%owf, glauber salt 60g/L, sodium carbonate 6g/L mix with water and obtain; This formula can make silk fiber contaminate green, and viscose contaminates cream-coloured;
2) washing together: add water and be warming up to 60 DEG C, silk viscose glue intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 2 time;
3) soap: by the aqueous cleaning silk intertexture jacquard fabric adding 3g/L ten diamino benzene sulfonic acid sodium, water temperature 95 DEG C, cleaning terminates rear effluent discharge, and repeats above step 2 time;
4) two road washings: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 95 DEG C, terminate rear effluent discharge, and repeat above step 3 time;
5) regulate PH: add aqueous solution soaking silk viscose glue intertexture jacquard fabric, the acetic acid adding 2 ~ 3g/L regulates solution ph to 7, terminates rear effluent discharge, and repeats above step 3 time;
6) fabric goes out cylinder and dries: silk viscose glue intertexture jacquard fabric goes out cylinder and dries at 100 ~ 110 DEG C, to obtain final product.
embodiment 4
The silk intertexture jacquard fabric that will silk fiber and tencel fiber jacquard weave be adopted to interweave in the present embodiment is dyed rhodo and is dodged silver color, its method as follows:
1) dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 85 DEG C, and dyeing time is 90 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of dye liquor is: orchid receives uniformly dyeing material 0.1%owf, and HE type dye 3.75%owf, glauber salt 60g/L, sodium carbonate 6g/L mix with water and obtain; This formula can make silk fiber obtain rose, and tencel fiber contaminates to obtain silver color;
2) washing together: add water and be warming up to 60 DEG C, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 4 time;
3) soap: by the aqueous cleaning silk intertexture jacquard fabric adding 1g/L ten diamino benzene sulfonic acid sodium, water temperature 95 DEG C, cleaning terminates rear effluent discharge, and repeats above step 3 time;
4) two road washings: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 90 DEG C, terminate rear effluent discharge, and repeat above step 2 time;
5) regulate PH: add aqueous solution soaking silk intertexture jacquard fabric, the acetic acid adding 0.5 ~ 1g/L regulates solution ph to 7, terminates rear effluent discharge, and repeats above step 3 time;
6) fabric goes out cylinder and dries: silk intertexture jacquard fabric goes out cylinder and dries at 100 ~ 110 DEG C, to obtain final product.
embodiment 5
The silk intertexture jacquard fabric that will silk fiber and cotton fiber jacquard weave be adopted to interweave in the present embodiment is dyed tangerine look and is dodged grey, its method as follows:
1) dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 80 DEG C, and dyeing time is 110 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of dye liquor is: orchid receives uniformly dyeing material 0.325%owf, and HE type dye 1.25%owf, glauber salt 40g/L, sodium carbonate 5g/L mix with water and obtain; This formula can make silk fiber obtain tangerine look, and cotton fiber contaminates to obtain grey;
2) washing together: add water and be warming up to 60 DEG C, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 3 time;
3) soap: by the aqueous cleaning silk intertexture jacquard fabric adding 4g/L ten diamino benzene sulfonic acid sodium, water temperature 95 DEG C, cleaning terminates rear effluent discharge, and repeats above step 2 time;
4) two road washings: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 90 ~ 95 DEG C, terminate rear effluent discharge, and repeat above step 2 time;
5) regulate PH: add aqueous solution soaking silk intertexture jacquard fabric, the acetic acid adding 1 ~ 2g/L regulates solution ph to 7, terminates rear effluent discharge, and repeats above step 3 time;
6) fabric goes out cylinder and dries: silk intertexture jacquard fabric goes out cylinder and dries at 100 ~ 110 DEG C, to obtain final product.
comparative example
Comparative example 1 ~ 4 is comparative examples that applicant designs to contrast technical scheme of the present invention, and concrete operations are as follows.It is all identical with embodiment 1 ~ 5 that comparative example dye gigging used equipment, orchid receive uniformly dyeing material, HE type dye, glauber salt, sodium carbonate.
comparative example 1
In this comparative example, method of operating is with embodiment 1, but step 2) ~ 6) parameter different from embodiment 1.
Blue flash orange dyed by the silk intertexture jacquard fabric that will silk fiber and cotton fiber jacquard weave be adopted to interweave in the present embodiment, its method as follows:
1) dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 80 DEG C, and dyeing time is 120 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of dye liquor is: orchid receives uniformly dyeing material 2.0%owf, and HE type dye 1.5%owf, glauber salt 30g/L, sodium carbonate 3g/L mix with water and obtain;
2) washing together: add water and be warming up to 80 DEG C, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 3 time;
3) soap: add water and be warming up to 80 DEG C, add 3g/L ten diamino benzene sulfonic acid soda soap lotion and stir, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 4 time;
4) two road washings: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 80 DEG C, terminate rear effluent discharge, and repeat above step 2 time;
5) regulate PH: add aqueous solution soaking silk intertexture jacquard fabric, the acetic acid adding 1 ~ 2g/L regulates solution ph to 7, terminates rear effluent discharge, and repeats above step 3 time;
6) fabric goes out cylinder and dries: silk intertexture jacquard fabric goes out cylinder and dries at 115 ~ 120 DEG C, to obtain final product.
comparative example 2
In this comparative example, method of operating is with embodiment 1, but in step 1), dyestuff used is different from embodiment 1.
In the present embodiment, the silk intertexture jacquard fabric adopting silk fiber and cotton fiber jacquard weave to interweave is dyed blue flash orange, wherein:
1) dye fixing: the silk intertexture jacquard fabric after pre-treatment is being put into the coloring agent configured, is slowly being warming up to 98 DEG C from 40 DEG C, adopts dye gigging method to dye to silk intertexture jacquard fabric, dyeing time 120 minutes, effluent discharge;
The collocation method of dye liquor is: neutral dye 2.0%owf, and direct blend dye 1.5%owf, acetic acid 1g/L mix with water and obtain.
comparative example 3
In this comparative example, method of operating is with embodiment 1, but in step 1), technological parameter is different from embodiment 1.
In the present embodiment, the silk intertexture jacquard fabric adopting silk fiber and cotton fiber jacquard weave to interweave is dyed blue flash orange, wherein:
1) dye fixing: the silk intertexture jacquard fabric after pre-treatment is being put into the coloring agent configured, keeps temperature 70 C, adopts dye gigging method to dye to silk intertexture jacquard fabric, dyeing time 240 minutes, effluent discharge under 70 DEG C of constant temperature;
The collocation method of dye liquor is: orchid receives uniformly dyeing material 2.0%owf, and HE type dye 1.5%owf, glauber salt 50g/L, sodium carbonate 5g/L mix with water and obtain.
comparative example 4
Two bath process is adopted in this comparative example.
Blue flash orange dyed by the silk intertexture jacquard fabric that will silk fiber and cotton fiber jacquard weave be adopted to interweave in the present embodiment, its method as follows:
1) dye fixing: the silk intertexture jacquard fabric after pre-treatment is being put into the coloring agent configured, keep temperature 80 DEG C, the cotton fiber of dye gigging method to silk intertexture jacquard fabric is adopted to dye under 80 DEG C of constant temperature, dyeing time 180 minutes, effluent discharge;
The collocation method of dye liquor is: HE type dye 1.5%owf, glauber salt 50g/L, sodium carbonate 5g/L mix with water and obtain;
2) washing together: add water and be warming up to 60 DEG C, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 3 time;
3) two road washings: clean after being warming up to 95 DEG C, terminate rear effluent discharge, and repeat above step 2 time;
4) dye fixing: the silk intertexture jacquard fabric after pre-treatment is being put into the coloring agent configured, keep temperature 80 DEG C, the silk fiber of dye gigging method to silk intertexture jacquard fabric is adopted to dye under 80 DEG C of constant temperature, dyeing time 180 minutes, effluent discharge;
The collocation method of dye liquor is: it is the lauryl ether phosphate kalium salt of 1g/L that orchid receives uniformly dyeing material 2.0%owf anion surfactant, and glauber salt 50g/L, sodium carbonate 5g/L mix with water and obtain;
5) washing together: add water and be warming up to 60 DEG C, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 3 time;
6) soap: add water and be warming up to 95 DEG C, add 3g/L ten diamino benzene sulfonic acid soda soap lotion and stir, silk intertexture jacquard fabric is cleaned, terminates rear effluent discharge, and repeat above step 4 time;
7) two road washings: clean after being warming up to 95 DEG C, terminate rear effluent discharge, and repeat above step 2 time;
8) regulate PH: add aqueous solution soaking silk intertexture jacquard fabric, the acetic acid adding 1 ~ 2g/L regulates solution ph to 7, terminates rear effluent discharge, and repeats above step 3 time;
9) fabric goes out cylinder and dries: silk intertexture jacquard fabric goes out cylinder and dries at 100 ~ 110 DEG C, to obtain final product.
performance test is tested
Fastness to rubbing fastness is tested with reference to standard GB/T/T3920-2008, water-fastness COLOR FASTNESS is tested with reference to standard GB/T/T5713 ~ 1997, fastness to perspiration is tested with reference to standard GB/T/T3922-1995, and fastness to soaping is tested with reference to standard GB/T/T3921-2008.The performance test results is in table 1.Technique total used time is total used time of step in embodiment and comparative example, and by recording embodiment, technique time started of comparative example and technique end time respectively, both differences are technique total used time; Weigh operating efficiency with technique total used time, technique total used time, shorter operating efficiency was higher.Technique total water consumption is the total water consumption of all processing steps, terminates rear water meter show value, the difference of both calculating, is table 1 technique total water consumption, cubic unit rice m by observed and recorded technological operation front water meter show value, technique
3.Weigh the water-saving ability of silk flosssilk wadding intertexture garment material with technique total water consumption, the lower water-saving ability of technique total water consumption is higher.
The performance test results of table 1 embodiment 1 ~ 5 and comparative example 1 ~ 4
。
Can be found out by table 1, the fastness to rubbing of embodiment 1 ~ 5, water-fastness COLOR FASTNESS, fastness to perspiration and fastness to soaping excellent performance, be all better than comparative example 1 ~ 4.Implementing comparative example 4 adopts two-bath process to dye, and Color is better than comparative example 1 ~ 3, but the technique of comparative example 4 total used time and technique total water consumption are apparently higher than embodiment 1 ~ 5, and comparative example 4 twice discharge dyeing waste water and embodiment 1 ~ 5 need be discharged once.Therefore the dyeing used time of the present invention is few, energy consumption is low, and energy-saving and emission-reduction and the effect reduced costs all are better than the two-bath process of comparative example 4.
Visual observations is carried out to the silk intertexture jacquard fabric that embodiment 1 ~ 5 and comparative example 1 ~ 4 obtain, in comparative example 2 step 1), dyestuff used is different from embodiment, dyes in one bath double-colored silk intertexture jacquard fabric cannot be realized, after bathing, not only wet rubbing fastness, the performance of water-fastness COLOR FASTNESS are poor compared with embodiment for two kinds of dyestuffs one, and there is the phenomenon that dye-uptake is inconsistent and be mutually infected with in two kinds of fibers during fabric inspection officer visual observations in comparative example 2.In comparative example 3 step 1), technological parameter is different from embodiment.During staining conditions on the silk intertexture jacquard fabric that fabric inspection officer visual observations comparative example 3 finally obtains on silk fiber and cellulose fibre, find that the color that two kinds of fibers contaminate has and be significantly mutually infected with phenomenon.Step 2 in comparative example 1) ~ 6) parameter different from embodiment 1, the fabric obtained is poor compared with the embodiment of the present invention with in fastness to soaping at fastness to perspiration, therefore illustrate in technical scheme of the present invention step 2) ~ 6) parameter limit there is practical significance, contribute to the combination property improving double-colored silk intertexture jacquard fabric.
The above is only preferred embodiment of the present invention, and be not restriction invention being made to other form, any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the Equivalent embodiments of equivalent variations.But everyly do not depart from technical solution of the present invention content, any simple modification, equivalent variations and the remodeling done above embodiment according to technical spirit of the present invention, still belong to the protection domain of technical solution of the present invention.
Claims (4)
1. silk intertexture jacquard fabric dyeing, is characterized in that, comprise dye fixing-wash together-soap-two road washing-adjust ph-go out cylinder baking step, concrete operations are as follows:
Dye fixing: the silk intertexture jacquard fabric through pre-treatment is put into the dye liquor configured, adopt dye gigging method to dye, dyeing temperature keeps 80 ~ 85 DEG C, and dyeing time is 60 ~ 200 minutes; Terminate to total dyeing time, effluent discharge;
The collocation method of described dye liquor is: adopt orchid to receive uniformly dyeing material 0.1 ~ 2.5%owf, HE type dye 0.05 ~ 4%owf, glauber salt 40 ~ 60g/L, sodium carbonate 5 ~ 8g/L and mix with water and obtain;
Described silk intertexture jacquard fabric is that silk fiber and the jacquard weave of cellulose fibre intertexture form;
The washing temperature of described washing is together 45 ~ 60 DEG C, effluent discharge after cleaning, and repeats above operation 1 ~ 3 time;
Described concrete steps of soaping are: by the aqueous cleaning silk intertexture jacquard fabric adding 1 ~ 4g/L ten diamino benzene sulfonic acid sodium, water temperature 90 ~ 95 DEG C, and cleaning terminates rear effluent discharge, and repeats above step 2 ~ 4 time;
The concrete steps of described two road washings are: by heating rate 2 ~ 3 DEG C/min, clean after being warming up to 90 ~ 95 DEG C, terminate rear effluent discharge, and repeat above step 2 ~ 4 time;
The concrete steps of described adjust ph are: add aqueous solution soaking silk intertexture jacquard fabric, and the acetic acid adding 0.5 ~ 4g/L regulates aqueous solution pH to 7, terminates rear effluent discharge, and repeats above step 2 ~ 4 time;
Described go out cylinder dry bake out temperature be 100 ~ 110 DEG C.
2. silk intertexture jacquard fabric dyeing according to claim 1, is characterized in that: the collocation method of described dye liquor is: adopt orchid to receive uniformly dyeing material 2.0%owf, HE type dye 1.5%owf, glauber salt 50g/L, sodium carbonate 5g/L mix with water, acquisition dye liquor.
3. silk intertexture jacquard fabric dyeing according to claim 1, it is characterized in that: in described staining procedure, dyeing temperature keeps 80 DEG C, dyeing time is 120 minutes.
4. silk intertexture jacquard fabric dyeing according to claim 1, is characterized in that: described cellulose fibre is cotton fiber, tencel fiber or viscose.
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| CN104264357A (en) * | 2014-10-16 | 2015-01-07 | 嘉兴金凯悦针织面料有限公司 | 55% Lyocell fiber, 25% cotton and 20% spun silk single-sided jacquard fabrics and production method thereof |
| CN104611959B (en) * | 2015-02-03 | 2017-01-11 | 广州元禄信息科技有限公司 | Method for preparing novel one-bath-multicolor batik silk fabric |
| CN106638037A (en) * | 2016-12-28 | 2017-05-10 | 淄博大染坊丝绸集团有限公司 | Semi-color weaving and dyeing process of silk and cotton interwoven jacquard fabric |
| CN107366113B (en) * | 2017-07-18 | 2020-08-18 | 广州科联精密机器股份有限公司 | Method for printing and dyeing post-treatment of textile by using textile printing and dyeing post-treatment machine |
| CN108130760B (en) * | 2017-12-28 | 2020-06-09 | 淄博大染坊丝绸集团有限公司 | Dyeing and finishing manufacturing process of single-warp-yarn cotton satin |
| CN108130754A (en) * | 2017-12-28 | 2018-06-08 | 淄博大染坊丝绸集团有限公司 | A kind of pure cotton double-layer jacquard dyeing and finishing method |
| CN109023641B (en) * | 2018-08-01 | 2020-03-31 | 淄博大染坊丝绸集团有限公司 | Production method of ultra-deep color polyester interwoven fabric |
| CN111235919B (en) * | 2020-04-15 | 2022-10-11 | 淄博大染坊丝绸集团有限公司 | Dyeing and finishing process of real silk wormwood satin |
| CN113914115B (en) * | 2021-10-22 | 2024-05-10 | 青岛大学 | One-bath two-step dyeing process for silk/polyester mixed fabric |
| CN115212622A (en) * | 2022-07-21 | 2022-10-21 | 瓮福（集团）有限责任公司 | Method for cleaning pressure filter in phosphogypsum washing process |
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