CN102579304A - Bamboo juice extracting solution and application of bamboo juice extracting solution in preparation of skin care product or cosmetic - Google Patents
Bamboo juice extracting solution and application of bamboo juice extracting solution in preparation of skin care product or cosmetic Download PDFInfo
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- CN102579304A CN102579304A CN2012100832085A CN201210083208A CN102579304A CN 102579304 A CN102579304 A CN 102579304A CN 2012100832085 A CN2012100832085 A CN 2012100832085A CN 201210083208 A CN201210083208 A CN 201210083208A CN 102579304 A CN102579304 A CN 102579304A
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- extracting solution
- succus bambusae
- preparation
- cosmetics
- skin care
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- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- 229940100460 peg-100 stearate Drugs 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- AMCPECLBZPXAPB-UHFFFAOYSA-N propane-1,2,3-triol;sodium Chemical compound [Na].OCC(O)CO AMCPECLBZPXAPB-UHFFFAOYSA-N 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- 229950011392 sorbitan stearate Drugs 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 208000008203 tachypnea Diseases 0.000 description 1
- 206010043089 tachypnoea Diseases 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- QURCVMIEKCOAJU-UHFFFAOYSA-N trans-isoferulic acid Natural products COC1=CC=C(C=CC(O)=O)C=C1O QURCVMIEKCOAJU-UHFFFAOYSA-N 0.000 description 1
- 229940087291 tridecyl alcohol Drugs 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000001243 zingiber officinale rosc. root absolute Substances 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
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Abstract
The invention relates to the field of plant extract and daily cosmetic and discloses bamboo juice extracting solution. A preparation method of the bamboo juice extracting solution comprises the following steps: (1), centrifuging a bamboo juice crude product for 5 to 20 minutes at a high speed of 16,000 to 30,000 rpm; and (2), filtering liquid obtained after high-speed centrifugation by an ultrafiltration membrane. The obtained bamboo juice extracting solution can resist oxidation and inhibit tyrosinase and can be used for preparing a skin care product or the cosmetic, so that the skin care product or the cosmetic has skin whitening and anti-aging effects.
Description
Technical field
The present invention relates to plant extract and daily cosmetics field, specifically is a kind of Succus Bambusae extracting solution, and the application aspect preparation skin care item or cosmetics.
Background technology
Succus Bambusae is that the stem of stem or some other bamboo kind of grass family Phyllostachys phyllostachys nigra (lodd.ex lindl.) munro var.henonis (miff.) spapf et rendle Phyllostachys nigra (Lodd.) munro var henonis (Mitf.) Stapf ex Rendle is with the baking effusive faint yellow clarifying juice that burns.Have removing heat-phlegm, the effect of the arresting convulsion of having one's ideas straightened out is mainly used in the treatment phlegm-heat cough clinically, the yellow tachypnea of expectorant, apoplexy abundant expectoration, cards such as infantile convulsion, tetanus (" Chinese medicine voluminous dictionary ", Shanghai science tech publishing house, second edition, the first volume, the 1241st page).The several amino acids such as the aspartic acid that contain needed by human in the Succus Bambusae, serine, proline, polyphenol compound and trace element such as ferrum, zinc etc.It is reported that Succus Bambusae has stronger antibacterial action, especially to staphylococcus aureus, Bacillus subtillis, escherichia coli etc. all have good inhibitory effect (Wuxi Light Industry Univ.'s journal, Vol 23, No.1,36-39 page or leaf).But up to now, do not see research and the application of Succus Bambusae aspect cosmetics as yet.We find that in to the research of Succus Bambusae Succus Bambusae has antioxidation and restraint of tyrosinase is active, explain that Succus Bambusae can be used as the whitening anti-aging cosmetics additive and is applied in the cosmetics.
Early stage, patent CN 100391370C report utilized steam distillation to replace traditional baking legal system to be equipped with Succus Bambusae, but did not have follow-up processing.Chinese patent 201010501441.1 utilizes cooking process to extract rough Succus Bambusae, utilizes high speed centrifugation and membrane filtration that thick Succus Bambusae is handled then.But this patent has changed the technology of traditional method baking, have any different slightly with traditional Succus Bambusae, and it does not have detailed description and parameter to membrane filtration.Chinese patent 200810097525.6 utilizes Succus Bambusae to prepare a kind of skin toning agent, the treatment dermatomycosis.Do not find that so far Succus Bambusae is used for the patent of cosmetics aspect.
Summary of the invention
The present invention aims to provide a kind of Succus Bambusae extracting solution.
The present invention also is used to prepare cosmetics or skin care item with above-mentioned Succus Bambusae extracting solution, but restraint of tyrosinase and antioxidation, Pear Power and anti-aging effects.
This Succus Bambusae extracting solution, method for preparing may further comprise the steps:
(1) with Succus Bambusae semifinished product high speed centrifugation 5～20 minutes under 16000～30000rpm;
(2) liquid that obtains behind the high speed centrifugation obtains the Succus Bambusae extracting solution through ultrafiltration membrance filter.
In the step (2), the molecular weight that sees through of said ultrafilter membrane is 10000～200000, and the material of ultrafilter membrane is a hollow-fibre membrane, PS membrane, polyvinylidene fluoride film or ceramic membrane.
The said Succus Bambusae semifinished product of step (1) is through traditional baking method preparation.
Through the Succus Bambusae extracting solution that said method obtains, form clarification, transparent, and also stable, have antioxidation and restraint of tyrosinase activity, can be used as the whitening anti-aging cosmetics additive and be applied in cosmetics or the skin care item.Resulting cosmetics or skin care item Pear Power and anti-aging effects.
The addition of Succus Bambusae extracting solution in cosmetics or skin care item is 0.01wt%～20wt%, is preferably 0.1wt%～3wt%.
The method that the present invention prepares the Succus Bambusae extracting solution is simple, and the Succus Bambusae extracting solution is used to prepare cosmetics or skin care item, for Succus Bambusae provides new purposes.
Description of drawings
Fig. 1 is that embodiment 3 variable concentrations Succus Bambusae extracting solution are to free radical scavenging activity.
Fig. 2 for embodiment 9 smear contain Succus Bambusae extracting solution cream after 20 days the dermal melanin value change the numerical value comparison diagram relatively.
Fig. 3 for embodiment 9 smear contain Succus Bambusae extracting solution cream after 20 days L-value change the numerical value comparison diagram relatively.
The specific embodiment
Embodiment 1
Select the living phyllostachys nigra (lodd.ex lindl.) munro var.henonis (miff.) spapf et rendle of same place of production 2-4 or other kind, pole footpath bamboo appearance is near, removes branch and leaf; Joint is removed at two ends, is cut into 30cm length, wards off into the wide bamboo bar of 2cm; Get about 1000g and weigh, put in the altar, reach the bottom all around and enclose sternly with Linesless charcoal by traditional method; Connect a container down and collect the juice that oozes out, till baking to juice is most (traditional method), obtain the Succus Bambusae semifinished product.
The Succus Bambusae semifinished product of collecting is relatively more muddy, is prone to generate deposition, must further handle.
The Succus Bambusae semifinished product was carried out centrifugal 12 minutes rotating speed 16000-20000 rev/min with high speed centrifuge.The supernatant that obtains after centrifugal filters with hollow-fibre membrane (molecular weight that sees through is 100,000 dalton), obtains the Succus Bambusae extracting solution of clear.
The method that this patent adopts high speed centrifugation to add ultrafiltration obtains clarification, transparent, stable Succus Bambusae product.With the front the thick product of Succus Bambusae carry out with high speed centrifuge centrifugal, rotating speed 16000-20000 rev/min.Through membrane filtration, used membrane material can be a hollow-fibre membrane to product after centrifugal again, and PS membrane or polyvinylidene fluoride film etc. also can be selected inoranic membrane such as ceramic membrane for use.The selection of film is good seeing through 100,000 molecular weight.Through behind the membrane filtration, can obtain the bamboo juice of clear.
As required; Can also add suitably that antiseptic that cosmetics are suitable for such as isothiazolone (addition is 0.05wt%～0.5% or adds according to standard) or polyhydric alcohol such as 1,3 butylene glycol (addition is 0.05wt%～10wt% or adds according to standard) back is subsequent use as product.
The method for preparing of Succus Bambusae semifinished product is with embodiment 1.
The Succus Bambusae semifinished product was carried out centrifugal 8 minutes rotating speed 25000-30000 rev/min with high speed centrifuge.The supernatant that obtains after centrifugal filters with ceramic membrane (molecular weight that sees through is 100,000 dalton), obtains the Succus Bambusae extracting solution of clear.
The aptitude tests of DPPH free radical are removed in embodiment 3 Succus Bambusaes
1, and 1-diphenyl-2-trinitrophenyl-hydrazine (1,1-Diphenyl-2-picrylhydrazyl radical2, (2,4,6-trinitrophenyl) hydrazyl DPPH) is a kind of stable nitrogen center organic free radical to 2-Diphenyl-1-.The DPPH method was suggested in 1958, was widely used in ground quantitative determination Biosample, the classification material is good and the oxidation resistance of food.This method is according to the DPPH free radical single electron to be arranged, and has the last one to absorb at the 517nm place, and its alcoholic solution is the characteristic of purple.When free radical scavenger exists; Owing to its absorption being faded away with its single electron pairing; Its fading extent becomes quantitative relationship with the electron amount of its acceptance; Thereby available spectrophotometer carries out the rapid quantitative analysis, detects the free radical scavenging situation, thus the oxidation resistance of assess sample.Its ability representes that with clearance rate clearance rate is big more, shows that then its oxidation resistance is strong more.
Sample treatment: Succus Bambusae solution is amber transparency liquid, and the characteristic faint scent is arranged, and it is subsequent use when carrying out the antioxidation experiment Succus Bambusae extracting solution stock solution to be diluted to variable concentrations with pure water in proportion.
Test method:
1) testing sample solution 2ml (embodiment 2 Succus Bambusae samples) is added in the test tube;
2) add 2mlDPPH alcoholic solution, mixing;
3) lucifuge is reacted 30min under the room temperature at the dark place;
4) measure absorbance A bs at the 525nm place;
5) each concentration triplicate test is averaged as fitting data to guarantee the accuracy of experimental result at last.
Clearance rate I (%)=[1-(T-T0)/(C-C0)] * 100%
In the formula:
T0:2ml water or DMSO add 2ml DPPH solution absorbency; The sample solvent contrast;
The T:2ml sample liquid adds 2ml DPPH solution absorbency;
The C:2ml sample liquid adds the alcoholic acid absorbance of 2ml95%, positive control;
C0:2ml water or DMSO add the alcoholic acid absorbance of 2ml95%, positive control solvent control;
Calculate clearance rate according to top formula, the big more oxidation resistance of clearance rate is strong more.
Result of the test:
Half suppression ratio (IC
50) calculating:
C
50Value defined is that clearance rate is the concentration of 50% o'clock required antioxidant.
To the free radical scavenging activity mapping and carry out match, result such as Fig. 1 read and calculate IC with the Succus Bambusae of variable concentrations
50Value.As can be seen from the figure, the IC50 of the DPPH free radical scavenging of Succus Bambusae is 1.25%, has very high antioxidant activity.
In recent years research proof pigmentation is to generate enzyme by the melanin in the melanocyte in the UV-activated epidermis, and chromogenesis is caused.In the melanin generative process, tryrosinase changes into DOPA, DOPA quinone with tyrosine, through non-oxydasis and polymerization generate macromolecular melanin (Tianjin Normal University's journal, 2002,22,17-21).Therefore the activity through restraint of tyrosinase can limit the melanin generation, improves the pigmentation of skin.
Test method:
1) sets up sample cell, sample control tube, positive control, negative control.
2) in sample cell and sample control tube, respectively add 1ml embodiment 1 Succus Bambusae extracting solution, positive and negative control pipe replaces with phosphate buffer (pH:6.8).
3) in sample cell and positive control pipe, add 0.5ml tryrosinase solution (the enzyme 125U/ML of unit alive); Sample contrast and negative control pipe replace with the 0.5ml phosphate buffer; All test tubes of jolting make the abundant mixing of sample and tryrosinase, and 37 ℃ of tanks were hatched 10 minutes.
4) 0.03% tyrosine solution of adding 2ml reacted 10 minutes.Promptly be engraved in the 475nm place and measure absorbance.
Suppression ratio I (%)=[1-(T-T0)/(C-C0)] * 100%
In the formula:
T0: sample contrast
T: sample
C: positive control
C0: negative control
Result of the test:
| Test number (TN) | 1 | 2 | 3 | Meansigma |
| Suppression ratio | ||||
| 60％ | 62％ | 60％ | 60.7％ |
Laboratory sample was placed after 3 days, and solution colour does not still change, and explains that Succus Bambusae has secular restraint of tyrosinase effect.Can find out that from result of the test Succus Bambusae has potential skin whitening effect.
Application-the astringent of embodiment 5 Succus Bambusaes in cosmetics
Get embodiment 2 resulting Succus Bambusae extracting solution and be used to prepare astringent, fill a prescription as follows:
| Sequence number | The INCI title | Adding proportion wt% |
| 1 | Water | 71.5-94.11 |
| 2 | Glycerol | 3～10 |
| 3 | Betanin | 1～5 |
| 4 | Propylene glycol/two imidazolidinyl urea/methyl hydroxybenzoate/iodo propinyl butyl methylamine acid esters | 0.25～0.8 |
| 5 | Dicaprylyl carbonate | 0.05～0.3 |
| 6 | Glycyrrhizic acid dipotassium | 0.02-0.3 |
| 7 | PCA sodium | 0.01-0.2 |
| 8 | Polyquaternary ammonium salt-51 | 0.01-0.2 |
| 9 | Ethylhexyl glycerol | 0.1-1 |
| 10 | Hyaluronate sodium | 0.01-0.1 |
| 11 | The PEG-40 castor oil hydrogenated | 0.05-0.5 |
| 12 | Aminomethyl propanol | 0.01-0.1 |
| 13 | The EDTA disodium | 0.01-0.1 |
| 14 | Essence | 0.01-0.1 |
| 15 | Fructus oleae europaeae (OLEA EUROPAEA) fruit oil | 0.01-0.2 |
| 16 | The Succus Bambusae extracting solution | 0.01-20 |
Application-the essence of embodiment 6 Succus Bambusaes in cosmetics and skin care item
Get embodiment 1 or 2 resulting Succus Bambusae extracting solution are used to prepare essence, prescription as follows:
| Sequence number | The INCI title | Adding proportion wt% |
| 1 | Water | 50-90 |
| 2 | The glycerol polyacrylate | 5-15 |
| 3 | Glycerol | 1-5 |
| 4 | The algae extract | 2-5 |
| 5 | Propylene glycol | 1-3 |
| 6 | Propylene glycol/diazolidinyl urea/methyl hydroxybenzoate/iodine propilolic alcohol butyl mephenesin Carbamate | 0.2-0.8 |
| 7 | The Fructus oleae europaeae fruit oil | 0.1-1 |
| 8 | Xanthan gum | 0.01-0.2 |
| 9 | The PEG-40 castor oil hydrogenated | 0.05-0.5 |
| 10 | Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer | 0.01-1 |
| 11 | Aminomethyl propanol | 0.01-0.5 |
| 16 | Hyaluronate sodium | 0.01-0.1 |
| 17 | Essence | 0.01-1 |
| 18 | The Succus Bambusae extracting solution | 0.01-20 |
Application-the emulsion of embodiment 7 Succus Bambusaes in cosmetics
Get embodiment 2 resulting Succus Bambusae extracting solution and be used to prepare emulsion, fill a prescription as follows:
| Sequence number | The INCI title | Adding proportion wt% |
| 1 | Water | 50-95 |
| 2 | Butanediol | 1-10 |
| 3 | Parleam | 1-10 |
| 4 | Polydimethylsiloxane | 0.5-5 |
| 5 | Glyceryl stearate/PEG-100 stearate | 1-5 |
| 6 | Sorbitan stearate | 1-5 |
| 7 | Phenoxyethanol | 0.1-1 |
| 8 | The glycerol polyacrylate | 0.01-1 |
| 9 | The smart PEG-20 esters of three mountain Yu | 0.1-1 |
| 10 | The brown seed fat of wood Shandong star fruit | 0.01-1 |
| 11 | Cetearyl alcohol | 0.01-1 |
| 12 | Tocopherol acetas | 0.05-0.5 |
| 13 | Carbomer | 0.05-0.5 |
| 14 | Essence | 0.01-0.2 |
| 15 | Aminomethyl propanol | 0.001-0.3 |
| 16 | Xanthan gum | 0.01-1 |
| 17 | The EDTA disodium | 0.01-0.1 |
| 18 | Hyaluronate sodium | 0.01-0.1 |
| 19 | Methylisothiazolinone | 0.001-0.1 |
| 20 | The Succus Bambusae extracting solution | 0.01-20 |
Application-the cream of embodiment 8 Succus Bambusaes in cosmetics
Get embodiment 1 or 2 resulting Succus Bambusae extracting solution are used to prepare cream, prescription as follows:
| Sequence number | The INCI title | Adding proportion wt% |
| 1 | Water | 30-80 |
| 2 | 1, ammediol | 2-20 |
| 3 | Glycerol | 2-10 |
| 4 | The cetearyl alcohol ethylhexoate | 2-10 |
| 5 | Parleam | 1-10 |
| 6 | Polydimethyl siloxanes/polydimethy siloxanes alcohol | 1-10 |
| 7 | The glycerol sodium polyacrylate | 1-5 |
| 8 | The Fructus oleae europaeae fruit oil | 0.5-5 |
| 9 | PEG-20 methyl glucose sesquistearate | 0.5-5 |
| 10 | The smart PEG-20 esters of three mountain Yu | 1-5 |
| 11 | The tridecyl alcohol trimellitate | 0.5-5 |
| 12 | Stearic acid | 0.1-5 |
| 13 | Glyceryl stearate | 0.1-5 |
| 14 | Methyl glucose sesquistearate | 0.1-5 |
| 15 | Ethanol | 0.1-5 |
| 16 | Phenoxyethanol | 0.1-1 |
| 17 | Adermykon | 0.1-1 |
| 18 | Essence | 0.01-0.5 |
| 19 | Ferulic acid | 0.01-0.5 |
| 20 | Sodium polyacrylate | 0.1-1 |
| 21 | Glycyrrhizic acid dipotassium | 0.01-0.5 |
| 22 | The EDTA disodium | 0.01-0.3 |
| 23 | Aminobenzene methanol | 0.01-0.5 |
| 24 | Bisabolol/ginger-root extract | 0.01-1 |
| 25 | Hyaluronate sodium | 0.01-1 |
| 26 | The Succus Bambusae extracting solution | 0.01-20 |
The experiment of whitening of embodiment 9 human bodies
The Succus Bambusae of using among the present invention can be used as the effect property raw material of whitening with anti-aging cosmetics, and its type of service does not have specific (special) requirements, and it can be used for water preparation, cream, and emulsion is in the cosmetics of various different dosage forms such as elite.Should whitening with the invention human body, what use in the experiment is cream, and prescription is that the prescription in the application example 8 is formed, and wherein Succus Bambusae extracting solution content is 3wt%.
9.1, experimenter crowd
Healthy volunteer 15 people, 25～40 years old age.
9.2, appraisal procedure and judging quota
9.2.1 the use of given the test agent
Use from molding jig in experimenter's forearm inboard to be divided into the four measuring zone, measure its melanin value, L-value respectively.Measure at melanin value, L-value with quadrat method near wrist portion.The experimenter sooner or later smears given the test agent in the forearm inboard every day,, must not smear as blank value near the wrist position, uses continuously 20 days.Blank cream (cream that does not promptly contain Succus Bambusae) is smeared in the stack of experimenter's left forearm, and right forearm is smeared the cream (embodiment 8) that contains Succus Bambusae extracting solution 3wt%.
9.2.2 experimental data acquisition
The skinanalysis apparatus Mexameter MX18 of CK company (melanin and haemachrome test probe) detection of skin melanin, Colorimeter CL400 (skin color test probe) detection of skin colour of skin uniformity coefficient.
9.3, assessment result
Melanin is the common standard that we judge the skin black and white, and the colour of skin is got over brilliant white, and melanin value is low more.Can know by Fig. 2; In two sample uses, melanin value all descends to some extent, when experiment finished by the 20th day; The result that sample is smeared in the contrast both sides; Can find out obviously that the sample melanin reduction of smearing Succus Bambusae 3% can have effect preferably greater than blank to controlling melanic generation so smear Succus Bambusae 3%.
L-value is an index of definition color, and we are used for defining the uniform luminance of the colour of skin on skin color.The more even brilliant white of the colour of skin, L-value is high more.As can be seen from Figure 3, in two sample uses, the L-value of skin increases always; When experiment finished by the 20th day; Compare a side of smearing sample Succus Bambusae 3%, smear less that a side L-value of blank cream promotes, improve skin brightness effect is preferably arranged so smear 3% pair of Succus Bambusae.
Claims (9)
1. Succus Bambusae extracting solution is characterized in that method for preparing may further comprise the steps:
(1) with Succus Bambusae semifinished product high speed centrifugation 5～20 minutes under 16000～30000rpm;
(2) liquid that obtains behind the high speed centrifugation obtains the Succus Bambusae extracting solution through ultrafiltration membrance filter.
2. the described Succus Bambusae extracting solution of claim 1 is characterized in that, the molecular weight that sees through of the said ultrafilter membrane of step (2) is 10000～200000.
3. claim 1 or 2 described Succus Bambusae extracting solution is characterized in that the material of said ultrafilter membrane is a hollow-fibre membrane, PS membrane, polyvinylidene fluoride film or ceramic membrane.
4. the described Succus Bambusae extracting solution of claim 1 is characterized in that, the said Succus Bambusae semifinished product of step (1) is through the method preparation of baking.
5. the application of each described Succus Bambusae extracting solution of claim 1～4 aspect the preparation skin care item.
6. each described Succus Bambusae extracting solution of claim 1～4 is in the skin care item of preparation restraint of tyrosinase or the application aspect the cosmetics.
7. the application of each described Succus Bambusae extracting solution of claim 1～4 aspect preparation Skin whitening care cosmetics or cosmetics.
8. the application of each described Succus Bambusae extracting solution of claim 1～4 aspect preparation antioxidative skin care item or cosmetics.
9. the application of each described Succus Bambusae extracting solution of claim 1～4 aspect antidotal skin care item of preparation or cosmetics.
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| CN108619405A (en) * | 2018-05-11 | 2018-10-09 | 江西缔缘康生物科技有限公司 | A kind of novel bamboo leaching preparation process |
| CN108553392A (en) * | 2018-07-04 | 2018-09-21 | 钟鹏 | A kind of preparation method of whitening spot-removing moisturizing aloe cold cream |
| CN112220893A (en) * | 2020-11-18 | 2021-01-15 | 苏州禾研生物技术有限公司 | Application of plant additive with oxygen and sugar dual-resistance in preparation of composition with anti-saccharification effect |
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