CN102551040B - Method of preparing functional food by taking cordyceps sinensis and ganoderma lucidum spore powder as materials - Google Patents
Method of preparing functional food by taking cordyceps sinensis and ganoderma lucidum spore powder as materials Download PDFInfo
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- CN102551040B CN102551040B CN2011104579378A CN201110457937A CN102551040B CN 102551040 B CN102551040 B CN 102551040B CN 2011104579378 A CN2011104579378 A CN 2011104579378A CN 201110457937 A CN201110457937 A CN 201110457937A CN 102551040 B CN102551040 B CN 102551040B
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Abstract
The invention relates to a method of preparing a functional food by taking cordyceps sinensis and ganoderma lucidum spore powder as materials, and the method comprises the following steps: (1) placing cordyceps sinensis and ganoderma lucidum spore powder in a low-temperature ultrafine pulverizer for crushing cell walls, thus obtaining crushed cell wall products; (2) placing the crushed cell wall products in ethanol and extracting for 10-24 hours; (3) separating the ethanol extract, settling and drying to obtain large-molecule composite, and carrying out cryoconcentration and freeze drying on clear liquid, thus obtaining a small-molecule composite; (4) resolving the large-molecule composite in deionized water, thus obtaining a clear liquid; (5) placing the clear liquid in a membrane separation device for large-molecule active matter separation and purification, thus obtaining a purified concentrated solution; (6) freeze-drying the purified concentrated solution to obtain the large-molecule composite; and (7) mixing the large-molecule composite with the small-molecule composite uniformly, thus obtaining the product. Compared with the prior art, the method has the advantages of greatly improving the efficiency of the product and the like.
Description
Technical field
The invention belongs to the health food technology field, especially relating to a kind of is the preparation method that raw material is made functional food with Cordyceps sinensis, lucidum spore powder.
Background technology
Cordyceps sinensis and glossy ganoderma are widely used in medicine and health products as the traditional rare Chinese herbal medicine of China.But these products and consumer buy the autonomous decoction of medicinal material, all exist following a series of problem:
1, owing to Cordyceps sinensis, lucidum spore powder all exist cell membrane, so the existence of cell membrane can influence the medicinal material extraction ratio of effective constituents.
2, Cordyceps sinensis and lucidum spore powder all have water-soluble and fat-soluble two effective constituents, and the extraction of traditional Chinese medicine is all carried based on high-temperature water, therefore, liposoluble constituent have been caused the extraction waste.
3, all contain big molecular activity composition in Cordyceps sinensis and the lucidum spore powder, and these compositions all have unique 3-D solid structure, these structures are bases of its effect activity.And traditional traditional Chinese medicine extraction method all is that high temperature extracts, high temperature concentrates, the process of high temperature drying, and these processes can cause the destruction of macromolecular structure, thus loss of activity.
Summary of the invention
Purpose of the present invention be exactly provide in order to overcome the defective that above-mentioned prior art exists a kind of high product significantly effect be the preparation method of the functional food of raw material with Cordyceps sinensis, lucidum spore powder.
Purpose of the present invention can be achieved through the following technical solutions: a kind of is the preparation method of the functional food of raw material with Cordyceps sinensis, lucidum spore powder, it is characterized in that this method may further comprise the steps:
(1) Cordyceps sinensis and lucidum spore powder are placed fracturing cell walls in the low temperature ultrafine crusher by weight 1: 1.6, obtain the breaking-wall cell product;
(2) the breaking-wall cell product places and extracts 10-24h in the ethanol, obtains ethanol extract, the w/v of described breaking-wall cell product ethanol 1: 6;
(3) ethanol extract is separated, obtains clear liquid and precipitation, the precipitation freeze drying get thick molecular complex, clear liquid low temperature concentrated frozen dry little molecular complex;
(4) place deionized water to dissolve thick molecular complex, and centrifugal clear liquid, the w/v of described thick molecular complex and deionized water 1: 8 of getting;
(5) place membrane separation plant to carry out big molecular activity separating substances purifying step (4) gained clear liquid, get the purifying concentrate;
(6) freeze drying of purifying concentrate is got macromolecular complex;
(7) the little molecular complex that obtains of macromolecular complex that step (6) is obtained and step (3) mixes, and promptly gets product.
The temperature of the described low temperature ultrafine crusher of step (1) is subzero 10 ℃-subzero 20 ℃, and breakdown products is crossed 500 mesh sieves and obtained the breaking-wall cell product in the low temperature ultrafine crusher.
The volumetric concentration of the described ethanol of step (2) is 50-70%.
The cryodesiccated cryogenic temperature of the described precipitation of step (3) is subzero 35 ℃, and baking temperature is 35 ℃; The thickening temperature of described clear liquid low temperature concentrated frozen drying is 8 ℃-16 ℃, and freezing temperature is subzero 35 ℃, and dry temperature is 35 ℃.
The molecular weight of the described membrane separation plant of step (5) is 10k.
The cryodesiccated cryogenic temperature of the described purifying concentrate of step (6) is subzero 35 ℃, and baking temperature is 35 ℃.
Compared with prior art, the present invention is a raw material with Cordyceps sinensis, lucidum spore powder, and by raw material is carried out broken wall treatment, alcohol extract, the processing of low temperature concentrate drying etc. can saboteur's structures, keep the activity of raw material, significantly the effect of high product.
The specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
A kind of is the preparation method of the functional food of raw material with Cordyceps sinensis, lucidum spore powder, and this method may further comprise the steps:
(1) Cordyceps sinensis and lucidum spore powder were mixed by weight 1: 1.6 places the interior fracturing cell walls of low temperature ultrafine crusher, the temperature of low temperature ultrafine crusher is subzero 10 ℃-subzero 20 ℃, and breakdown products is crossed 500 mesh sieves and obtained the breaking-wall cell product in the low temperature ultrafine crusher;
(2) the breaking-wall cell product places and extracts 10-24h in the ethanol, obtains ethanol extract, the w/v of described breaking-wall cell product ethanol 1: 6, and the volumetric concentration of ethanol is 50-70%;
(3) ethanol extract is separated, obtains clear liquid and precipitation, wherein be deposited in subzero 35 ℃ freezing after, in 35 ℃ of dry thick molecular complexes, clear liquid concentrates in 8 ℃-16 ℃, in subzero 35 ℃ of freezing backs at 35 ℃ of dry little molecular complexes;
(4) place deionized water to dissolve thick molecular complex, and centrifugal clear liquid, the w/v of described thick molecular complex and deionized water 1: 8 of getting;
(5) step (4) gained clear liquid being placed molecular weight is that the membrane separation plant of 10k carries out big molecular activity separating substances purifying, the purifying concentrate;
(6) freeze drying of purifying concentrate is got macromolecular complex, cryogenic temperature is subzero 35 ℃, and baking temperature is 35 ℃;
(7) the little molecular complex that obtains of macromolecular complex that step (6) is obtained and step (3) mixes, and promptly gets product.
Product of the present invention is analyzed and is compared as follows with the commercially available prod:
| Title | Polysaccharide | Adenosine | Sweet mellow wine | Triterpene |
| Embodiment 1 product | 50％ | 0.69mg/g | 11.9％ | 11.6％ |
| The commercially available prod | 20％ | 0.27mg/g | 6.1％ | 1.5％ |
This shows that preparation technology of the present invention follows high to the recovery rate of functional component.
Product efficacy is researched and analysed comparison
At the immunocompetence effect of Cordyceps sinensis, glossy ganoderma, carried out relevant animal experiment.Relatively find with product 50mg/kg of the present invention and commercially available prod 500mg/kg dosage, body is improved phagocytic index, induce macrophage to produce TNF-α and have the effect of equity mutually.
This shows, through the preparation of this technology, the effect of high product significantly.
Claims (3)
1. one kind is the preparation method of the functional food of raw material with Cordyceps sinensis, lucidum spore powder, it is characterized in that this method may further comprise the steps:
(1) Cordyceps sinensis and lucidum spore powder are placed fracturing cell walls in the low temperature ultrafine crusher by weight 1:1.6, obtain the breaking-wall cell product;
(2) the breaking-wall cell product places and extracts 10-24h in the ethanol, obtains ethanol extract, the w/v 1:6 of described breaking-wall cell product ethanol;
(3) ethanol extract is separated, obtains clear liquid and precipitation, the precipitation freeze drying get thick molecular complex, clear liquid low temperature concentrated frozen dry little molecular complex;
(4) place deionized water to dissolve thick molecular complex, and centrifugal clear liquid, the w/v 1:8 of described thick molecular complex and deionized water of getting;
(5) place membrane separation plant to carry out big molecular activity separating substances purifying step (4) gained clear liquid, get the purifying concentrate;
(6) freeze drying of purifying concentrate is got macromolecular complex;
(7) the little molecular complex that obtains of macromolecular complex that step (6) is obtained and step (3) mixes, and promptly gets product;
The temperature of the described low temperature ultrafine crusher of step (1) is subzero 10 ℃-subzero 20 ℃, and breakdown products is crossed 500 mesh sieves and obtained the breaking-wall cell product in the low temperature ultrafine crusher;
The cryodesiccated cryogenic temperature of the described precipitation of step (3) is subzero 35 ℃, and baking temperature is 35 ℃; The thickening temperature of described clear liquid low temperature concentrated frozen drying is 8 ℃-16 ℃, and freezing temperature is subzero 35 ℃, and dry temperature is 35 ℃;
The molecular weight of the described membrane separation plant of step (5) is 10k.
2. according to claim 1 a kind of be the preparation method of the functional food of raw material with Cordyceps sinensis, lucidum spore powder, it is characterized in that the volumetric concentration of the described ethanol of step (2) is 50-70%.
3. according to claim 1 a kind of be the preparation method of the functional food of raw material with Cordyceps sinensis, lucidum spore powder, it is characterized in that the cryodesiccated cryogenic temperature of the described purifying concentrate of step (6) is subzero 35 ℃, baking temperature is 35 ℃.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011104579378A CN102551040B (en) | 2011-12-31 | 2011-12-31 | Method of preparing functional food by taking cordyceps sinensis and ganoderma lucidum spore powder as materials |
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| CN2011104579378A CN102551040B (en) | 2011-12-31 | 2011-12-31 | Method of preparing functional food by taking cordyceps sinensis and ganoderma lucidum spore powder as materials |
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| CN102551040A CN102551040A (en) | 2012-07-11 |
| CN102551040B true CN102551040B (en) | 2013-07-24 |
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| CN103054909B (en) * | 2013-02-04 | 2014-09-10 | 福建仙芝楼生物科技有限公司 | Capsule for alleviating physical fatigue and preparation method thereof |
| CN103749813A (en) * | 2013-12-25 | 2014-04-30 | 段敬东 | Ganoderma lucidum health tea |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101138351A (en) * | 2007-10-13 | 2008-03-12 | 刘洪娟 | Glossy ganoderma battercake |
| CN101239081A (en) * | 2007-02-06 | 2008-08-13 | 周窑生 | Composition for treating cancer and preparation thereof |
| CN101485450A (en) * | 2009-02-20 | 2009-07-22 | 陈淑燕 | Health food containing Cordyceps sinensis and glossy ganoderma spore powder |
| CN101849691A (en) * | 2010-02-26 | 2010-10-06 | 湖北中烟工业有限责任公司 | Chinese medicinal health-care drink and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101019899A (en) * | 2007-03-05 | 2007-08-22 | 澄江县明达园艺有限责任公司 | Buccal tablet of aweto or aweto extract |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101239081A (en) * | 2007-02-06 | 2008-08-13 | 周窑生 | Composition for treating cancer and preparation thereof |
| CN101138351A (en) * | 2007-10-13 | 2008-03-12 | 刘洪娟 | Glossy ganoderma battercake |
| CN101485450A (en) * | 2009-02-20 | 2009-07-22 | 陈淑燕 | Health food containing Cordyceps sinensis and glossy ganoderma spore powder |
| CN101849691A (en) * | 2010-02-26 | 2010-10-06 | 湖北中烟工业有限责任公司 | Chinese medicinal health-care drink and preparation method thereof |
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