CN102534747A - Hydrothermal crystal growth furnace capable of accommodating multiple hydrothermal kettles - Google Patents
Hydrothermal crystal growth furnace capable of accommodating multiple hydrothermal kettles Download PDFInfo
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- CN102534747A CN102534747A CN2012100324660A CN201210032466A CN102534747A CN 102534747 A CN102534747 A CN 102534747A CN 2012100324660 A CN2012100324660 A CN 2012100324660A CN 201210032466 A CN201210032466 A CN 201210032466A CN 102534747 A CN102534747 A CN 102534747A
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- crystal growing
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Abstract
The invention provides a hydrothermal crystal growth furnace capable of accommodating multiple hydrothermal kettles. The furnace is characterized in that: the multiple hydrothermal kettles can be accommodated in a single crystal growth furnace, the temperature interference of upper and lower heating zones in hydrothermal equipment is prevented by a temperature isolation plate, and the furnace has a simple structure, controls temperature accurately and is energy-saving and environment-friendly. According to the technical scheme, the novel hydrothermal crystal growth furnace capable of accommodating the multiple hydrothermal kettles comprises a graphite hearth capable of accommodating the multiple hydrothermal kettles, the temperature isolation plate, an electric furnace heating wire, a temperature measurement and control device, a top thermal insulation cover, a thermal insulation filler and a shell.
Description
Technical field
The present invention relates to a kind of development of holding the novel hydrothermal method crystal growing furnace of a plurality of water heating kettles, belong to Hydrothermal Growth crystal technical equipment field.
Background technology
The Hydrothermal Growth crystal is meant: pour mineralizer solution into water heating kettle, the baffle plate with holes in the water heating kettle is divided into two zones with the water heating kettle liner, and lower area is called dissolve area; Place the hydrothermal growth culture material, last zone is called the vitellarium, places seed crystal; Through temperature control technique, make dissolve area be in the condition of high temperature, and the vitellarium is in low-temperature condition; The saturated solution of dissolve area is transported to the vitellarium through the aperture on the baffle plate like this, because temperature reduces, saturated solution becomes supersaturated solution; Oversaturated part will be separated out on seed crystal, make seed crystal constantly grow up.
There are two big defectives at present traditional hydro-thermal crystal growing furnace; First furnace tube can only be placed a water heating kettle; Therefore there is the low and bigger problem of energy consumption of growth efficiency; It two is to go up the heating zone to have the temperature interference problem with following heating zone the decline of heating zone temperature-controlled precision about usually causing.Therefore, if develop a kind of crystal growing furnace of placing a plurality of water heating kettles,
To in energy-conserving and environment-protective, increase substantially growth efficiency.Is but a difficult problem of developing this equipment existence: the temperature control accuracy that how could guarantee all water heating kettles? How just can prevent the temperature interference between heating zone and the following heating zone?
In order to improve the temperature control accuracy of water heating kettle; The present invention intends and adopts the extraordinary graphite material of heat conductance to do furnace tube; In order to prevent or to reduce up and down the temperature of heating zone and interfere; The present invention's plan level between last process furnace silk and following process furnace silk is laid an annular thermal insulative board, and the thermal insulative board material adopts the very poor lagging material of heat conductance.
Summary of the invention
The invention provides a kind of novel hydrothermal method crystal growing furnace that holds a plurality of water heating kettles; Its characteristics are can hold a plurality of water heating kettles in the single crystal growing furnace, and use thermal insulative board to prevent the temperature of heating zone interference up and down in the water heating apparatus, and are simple in structure; Temperature control is accurate, energy-conserving and environment-protective.The present invention adopts following technical scheme: comprising: graphite burner hearth, thermal insulative board, heating electric stove wire, temperature regulating device, top insulation cover, insulation filler and housing.It is characterized in that: use the very high graphite of thermal conductivity coefficient to do furnace tube, this furnace tube can hold a plurality of water heating kettles, peripheral having heaters of furnace tube and measuring and controlling temp system, and well heater uses electric stove wire, globars or Si-Mo rod material.The insulation filler is filled between warming plate and the furnace tube, and the insulation filler is a pearlstone.Warming plate is adjacent at the furnace shell inwall, and thermal insulative board is positioned over up and down between the heating zone, and warming plate and thermal insulative board all adopt pure aluminium silicate, Calucium Silicate powder, Natural manganese dioxide, beryllium oxide, zirconium white, in the silit one or any several kinds.The steel plate of housing after by 3mm processed.Thermometric and temperature controlling system adopt thermopair and temperature controller combination.
The novel hydrothermal method crystal growing furnace that can hold a plurality of water heating kettles uses step to comprise:
1. a plurality of water heating kettles are positioned in the graphite furnace tube, cover the top insulation cover.
2. will go up temperature control inserts in the graphite furnace tube with following temperature-control heat couple.
3. the temperature control program is set, and through 6 hours intensification, last heating zone arrived holding temperature with following heating zone, and the temperature of following heating zone is higher than the heating zone.
4. passed through certain soaking time, cooling process has been set, let the body of heater cool to room temperature.
5. open the top insulation cover, hang out water heating kettle.
Description of drawings
Accompanying drawing 1 is for holding the novel hydrothermal method crystal growing furnace front view of a plurality of water heating kettles.Wherein 1 is housing, and 2 is last process furnace silk, and 3 is warming plate, and 4 is last heating zone thermopair, and 5 is water heating kettle, and 6 are following process furnace silk, and 7 are following heating zone thermopair, and 8 is the graphite furnace tube.
Accompanying drawing 2 is for holding the novel hydrothermal method crystal growing furnace vertical view of a plurality of water heating kettles.Wherein 1 is housing, and 2 is warming plate, and 3 is the graphite furnace tube, and 4 is water heating kettle, and 5 are the insulation filler, and 6 is thermal baffle.
Embodiment
Instance 1:
1. with the Lithium Hydroxide MonoHydrate hydrothermal mineralization agent of 1mol/L, zinc oxide culture material and zinc oxide seed crystal are put into water heating kettle.
2. the water heating kettle with a plurality of good seals is positioned in the graphite burner hearth pore hole, covers the top insulation cover.
3. will go up in temperature control and the following temperature-control heat couple insertion graphite furnace tube and carry out thermometric.
4. the temperature control program is set, and through 6 hours intensification, last heating zone and following heating zone arrived the holding temperature of 400 degrees centigrade and 450 degrees centigrade respectively.
5. passed through 14 days insulation growth time, cooling process has been set, let body of heater and autoclave cool to room temperature.
6. open the top insulation cover, hang out a plurality of water heating kettles.
7. open water heating kettle, can obtain grown layer thickness is the Zinc oxide single crystal behind the 2mm.
Instance 2:
1. with the sodium hydroxide mineralizer of 3mol/L, quartzy culture material and quartzy seed crystal are put into water heating kettle.
2. the water heating kettle with a plurality of good seals is positioned in the graphite burner hearth pore hole, covers the top insulation cover.
3. will go up in temperature control and the following temperature-control heat couple insertion graphite furnace tube and carry out thermometric.
4. the temperature control program is set, and through 12 hours intensification, last heating zone and following heating zone arrived the holding temperature of 400 degrees centigrade and 440 degrees centigrade respectively.
5. passed through 30 days insulation growth time, cooling process has been set, let body of heater and autoclave cool to room temperature.
6. open the top insulation cover, hang out a plurality of water heating kettles.
7. open water heating kettle, can obtain grown layer thickness is the quartzy monocrystalline behind the 2cm.
Should be noted that above-described embodiment just explains the present invention with 2 examples; It should not be a limitation of the present invention; Be familiar with all knowing of this technology simultaneously, can carry out in the text the not various improvement of description to the present invention, and these improve the spirit and the scope that can not depart from this patent.
Claims (5)
1. the novel hydrothermal method crystal growing furnace that can hold a plurality of water heating kettles comprises: graphite burner hearth, thermal insulative board, heating electric stove wire, measuring and controlling temp device, top insulation cover, insulation filler and housing.
2. like right 1 described crystal growing furnace, it is characterized in that: furnace tube adopts the graphite material of high thermal conductivity coefficient.
3. like right 1 described hydrothermal method crystal growing furnace, it is characterized in that: can place a plurality of water heating kettles in the furnace tube.
4. like right 1 described hydrothermal method crystal growing furnace, it is characterized in that: go up and set up thermal insulative board between process furnace silk and the following process furnace silk to reduce the heat conduction of going up between temperature control district and the following temperature control.
5. like right 1 described hydrothermal method crystal growing furnace, it is characterized in that: the material of thermal insulative board is a pure aluminium silicate, Calucium Silicate powder, Natural manganese dioxide, beryllium oxide, zirconium white, in the silit one or any several kinds.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100324660A CN102534747A (en) | 2012-02-13 | 2012-02-13 | Hydrothermal crystal growth furnace capable of accommodating multiple hydrothermal kettles |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100324660A CN102534747A (en) | 2012-02-13 | 2012-02-13 | Hydrothermal crystal growth furnace capable of accommodating multiple hydrothermal kettles |
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| CN102534747A true CN102534747A (en) | 2012-07-04 |
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| CN2012100324660A Pending CN102534747A (en) | 2012-02-13 | 2012-02-13 | Hydrothermal crystal growth furnace capable of accommodating multiple hydrothermal kettles |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106149045A (en) * | 2016-08-25 | 2016-11-23 | 中国有色桂林矿产地质研究院有限公司 | A kind of spherical high-pressure reactor for hydrothermal method crystal growth |
| CN108014718A (en) * | 2017-12-14 | 2018-05-11 | 西南交通大学 | A kind of high throughput Hydrothermal Synthesiss and surface processing device |
| CN111437780A (en) * | 2020-03-20 | 2020-07-24 | 安徽大学 | Hydrothermal solvent heat parallel synthesis device |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2559657Y (en) * | 2002-08-27 | 2003-07-09 | 中国科学院福建物质结构研究所 | Double controlling temperature crystal grower furnace |
| CN2680347Y (en) * | 2004-03-19 | 2005-02-23 | 桂林矿产地质研究院 | Autoclave with heat insulation barrier layer |
| CN201416045Y (en) * | 2009-05-11 | 2010-03-03 | 北京石晶光电科技股份有限公司 | Autoclave heating system for growing artificial crystal by a hydro-thermal method |
| CN102108543A (en) * | 2009-12-29 | 2011-06-29 | 北京有色金属研究总院 | Multi-stage side heater in vertical gradient freezing crystal growing furnace |
-
2012
- 2012-02-13 CN CN2012100324660A patent/CN102534747A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2559657Y (en) * | 2002-08-27 | 2003-07-09 | 中国科学院福建物质结构研究所 | Double controlling temperature crystal grower furnace |
| CN2680347Y (en) * | 2004-03-19 | 2005-02-23 | 桂林矿产地质研究院 | Autoclave with heat insulation barrier layer |
| CN201416045Y (en) * | 2009-05-11 | 2010-03-03 | 北京石晶光电科技股份有限公司 | Autoclave heating system for growing artificial crystal by a hydro-thermal method |
| CN102108543A (en) * | 2009-12-29 | 2011-06-29 | 北京有色金属研究总院 | Multi-stage side heater in vertical gradient freezing crystal growing furnace |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106149045A (en) * | 2016-08-25 | 2016-11-23 | 中国有色桂林矿产地质研究院有限公司 | A kind of spherical high-pressure reactor for hydrothermal method crystal growth |
| CN108014718A (en) * | 2017-12-14 | 2018-05-11 | 西南交通大学 | A kind of high throughput Hydrothermal Synthesiss and surface processing device |
| CN111437780A (en) * | 2020-03-20 | 2020-07-24 | 安徽大学 | Hydrothermal solvent heat parallel synthesis device |
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Application publication date: 20120704 |