CN102524464A - Preparation method of dendrobe health-care Pu'er tea cream - Google Patents
Preparation method of dendrobe health-care Pu'er tea cream Download PDFInfo
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Abstract
The invention discloses a preparation method of dendrobe health-care Pu'er tea cream and belongs to the field of food and drug technology. Different-specific-year Pu'er tea in 1 year, 5 years, 10 years and 20 years is used as a tea cream ingredient main body through reasonable proportioning, the mouth feeling advantages of tea in different specific years are sufficiently utilized, and the singleness of the mouth feeling of the Pu'er tea cream prepared by single raw materials is overcome, so the mouth feeling of the tea cream is purer and milder, and the fragrance is richer. In addition, polysaccharide effective ingredients of the dendrobe are extracted and are added into the tea cream at a proper proportion, the mouth feeling of the tea cream is enhanced, and meanwhile, the health-care function of the tea cream is enriched.
Description
Technical field
The invention belongs to the health products preparing technical field, specifically relate to a kind of preparation method of stem of noble dendrobium health-care pu'er tea cream.
Background technology
Dendrobium candidum (Dendrobium officinale Kimura et Migo), herbaceous plant grows nonparasitically upon another plant for the orchid family is perennial.The stem of noble dendrobium can be divided into tens of kinds on yellow grass, Jin Chai, horsewhip etc., and dendrobium candidum is the superfine product of the stem of noble dendrobium, and iron is green gains the name because of epidermis is for it.Dendrobium candidum has unique medical value, and its medicinal part is fresh or dry stem, and its main component is a polysaccharide, " in the Chinese pharmacopoeia record its reinforcing stomach reg fluid, nourishing Yin and clearing heat effect are arranged.
Pu'er cooked tea is to be that raw material is processed through after fermentation with the big-leaf species in yunnan solar dried green tea, has body-care effects such as reducing blood lipid uric acid, fat-reducing, prevention diabetes and hypertrophy of the prostate, anti-inflammation.
Main chemical compositions Tea Polyphenols in quality of tea leaves and the tealeaves, amino acid, soluble sugar etc. are closely related.Tea Polyphenols is to be the different phenols of main body and the general name of derivative thereof with the catechin, because oxidation has taken place in storage for it, has generated the material that influences at the bottom of millet paste soup look, flavour and the leaf, impels the quality that becomes to sample tea to change.The existence of soluble sugar and conversion in the tealeaves have direct influence to the soup look and the flavour of tealeaves, and remote-effects are the main matter that forms the sweet and pure flavor of millet paste to the fragrance of tealeaves.Under hydrothermal; The macromolecular glucide of a part can further be cracked into monose; Soluble sugar content is increased to some extent; Simultaneously soluble sugar also can interact with amino acid, polyphenol compound under the effect of heat, and to generate color and luster pleasing and have the material of the fragrance of a flower, so soluble sugar is dynamic change under certain wet heat condition.Degraded can take place and transform in the amino acid in the tealeaves, can interact that to generate color and luster pleasing and have volatile aroma substance with polyphenol compound and carbohydrate, participates in tea color and forms with fragrance, and amino acid also is to constitute the bright important substance of feeling well and distinguishing the flavor of of millet paste simultaneously.
Different its quality of Pu'er cooked tea of fermentation year number is different, is actually the result of oxidation, degraded or the polymerization of polyphenols in the Pu'er tea.The composition to the Pu'er cooked tea of different year in " GC-MS of the non-volatile material of different storage time Pu'er teas analyze " literary composition such as Zhou Li is studied; There is notable difference fragrance, flavour and the Tang Se aspect of different storage time Pu'er teas: the Pu'er tea Chen Xiang in 1 year is not obvious; The mellow inlet of flavour is still puckery and be with tart flavour slightly; The soup look orange, and the dysoxidation of 1 year Pu'er tea inclusion is described, and 5 years tea and differing greatly between the tea in 10 years; And it is less relatively to have deposited between the Pu'er tea of 5 years and 10 years difference, has the characteristic feature of Aged Pu 'er Tea tea.But the tea of different year had unique separately flavor component, contained the longipinene of fragrant in the Pu'er tea in 1 year, the butanedioic acid, 2 of banksia rose flavor, 4-dimethylbenzaldehyde, 2 of peppermint camphor perfume, 3-dimethylnaphthalene, 2,6-diisopropyl naphthalene; Contain Chen Xiang materials such as 5-methylol-2 furan carboxyaldehyde, furans alcohol in 5 years Pu'er teas; Contain banksia rose materials such as 2-tolyl aldehyde, lignoceric acid in 10 years Pu'er teas.These materials are the important component that form 1 year, 5 years, the 10 years different flavours of Pu'er tea.
Tea cream is a kind of portable instant capacity tea-drinking article, and it is the tea stain that water-insoluble can not appear in the tea cream that quality is high.Pu'er tea ointment is the component content that extracts in the Pu'er tea, and elaboration in the tea that warp purifies, concentrated, dry working procedure processing such as (moulding) forms has very high nutritive value, article drink value and vast market prospect.Compare with traditional Pu'er tea, the good portability of tea cream, passes during brewing is succinct, convenient, healthy; The mouthfeel gentleness is thick and heavy, has the sensation of the old tea of article drink, and stereovision is abundant.
Patent 02122517.6 has been introduced the tea cream that the water of tea powder that a kind of weight ratio is 20%-70% and 30%-80% is formed, and has added milk, butter and sweetener therein.Patent 200410022145.8 has been introduced a kind of tea cream and production method thereof, 1 part of one-tenth is sampled tea to put in 11 parts of boiling water soak, and enduring slowly through getting angry to boil with slow fire, boils after leaving standstill again, and crosses and filters tea juice; Tea juice through slow fire endure slowly hot lotion, moulding obtains finished product.Patent 200810026343.X has introduced a kind of honey tea cream preparation method, and a certain proportion of honey, tealeaves, ginger, dried orange peel are modulated into cream through corresponding technology.Patent 200710066025.1 has been introduced a kind of Pu'er tea ointment and production technology thereof, and mainly adopt spontaneous fermentation 1 year, 2-3, tea is assorted more than 3 years, through the living Pu'er tea ointment that adds water boil, concentrates, oven dry is processed.Patent 200710066028.5 has been introduced a kind of aged Pu'er tea ointment, method for making and purposes, passes through infusion, concentrates, dehydrates the paste that obtains with Pu'er cooked tea more than 10 years or the Pu'er raw tea more than 15 years.Patent 200810058102.3 has been introduced and has been utilized warm water ultrasonic extraction and squeezing, cryogenic vacuum to concentrate the Pu'er tea paste that obtains low-temperature extraction.
The raw material that has related to tea cream in these patents is chosen and production technology, and it is single raw material that raw material is chosen what take usually, has only the raw material of the Pu'er raw tea that relates to different year in the patent 200710066025.1 composite, but the time is chosen and only has been confined in 3 years; The raw material that adds other is arranged in production of tea cream, but do not relate to the application of medicinal plant in tea cream as yet, particularly medicinal plant is combined with Pu'er cooked tea, enrich the effect of tea cream, do not see the report that success is arranged in the prior art as yet.
Summary of the invention
The objective of the invention is to deficiency, a kind of preparation method of stem of noble dendrobium health-care pu'er tea cream is provided, combine with the Pu'er cooked tea of different year, improve the health-care efficacy of tea cream mouthfeel, enhanced products through dendrobium candidum to prior art.
The object of the invention is achieved through following technical scheme.
A kind of preparation method of stem of noble dendrobium health-care pu'er tea cream may further comprise the steps:
(1) preparation Pu'er cooked tea extract:
1. take by weighing 10～20 parts of the Pu'er cooked teas in 1 year of ageing by weight, 10 parts～20 parts of the Pu'er cooked teas in 5 years, 30～40 parts of 30～40 parts of the Pu'er cooked teas in 10 years and the Pu'er cooked teas in 20 years of ageing; Mixing is subsequent use;
2. get the Pu'er cooked tea of mixing,, remove and deash with 4～6 times clear water drip washing; Place then under 40 ± 5 ℃ of conditions and dry, subsequent use after pulverizing;
3. the Pu'er cooked tea powder is with 9～13 times pure water, 40～50 ℃ of isoperibol refluxed lixiviate 15 minutes, leaves standstill suction filtration to the room temperature, and I must filtrate; Filter residue is used 9～13 times pure water boiling reflux lixiviate 10 minutes again, leaves standstill suction filtration after the room temperature, filtrate II; Merging filtrate I and II in-0.070 ± 0.01Mpa vacuum, are concentrated into 1/4 of original volume under 70～80 ℃ the temperature, obtain the Pu'er cooked tea concentrated extracting solution;
(2) Dendrobium officinale polysaccharide extracts:
1. the fresh stem with dendrobium candidum dries, and under 40 ± 5 ℃ of conditions, dries, and is subsequent use after pulverizing;
2. get Dendrobium and boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature with 40～60 times pure water, filtrate II I; Filter residue boiled lixiviate 1 hour with 30～40 times pure water again, left standstill suction filtration to the room temperature, and IV must filtrate; Merging filtrate III and IV in-0.070 ± 0.01Mpa vacuum, are concentrated into 1/10 of original volume under 70～80 ℃ the temperature, obtain the dendrobium candidum concentrated extracting solution;
(3) preparation tea cream:
Take by weighing 80～90 parts of Pu'er cooked tea concentrated extracting solutions and 10～20 parts of dendrobium candidum concentrated extracting solutions by weight, mix; In temperature is freeze drying 20～30 hours under-40 ℃～-30 ℃ conditions, after melt and be pressed into paste and promptly obtain required stem of noble dendrobium health-care pu'er tea cream.
The present invention compared with prior art has the following advantages:
1, the Pu'er cooked tea of choosing same kind different year carries out rational proportion; The time span is bigger, has made full use of mouthfeel advantage in the different year tealeaves, has overcome the monotonicity of the Pu'er tea ointment mouthfeel of single feedstock production; Make that the mouthfeel of tea cream is pureer and milder, fragrance is more strong fragrant;
2, the abundant active ingredient of having utilized dendrobium candidum has incorporated active ingredient in the tea cream well, when strengthening tea cream mouthfeel, has enriched the health care of tea cream;
3, tealeaves adopts different extracting modes respectively with medicinal plant, when guaranteeing to produce the realization simplicity, keeps active ingredient separately dramatically.
The specific embodiment
Through embodiment the present invention is done to specify further below, but embodiment is not the qualification to technical scheme of the present invention that all should belong to protection scope of the present invention based on the conversion that training centre of the present invention is done.
Embodiment 1
(1) Pu'er cooked tea extract:
1. take by weighing 10 years Pu'er cooked teas of 5 years Pu'er cooked teas of 1 year Pu'er cooked tea of 0.5kg, 1kg, 1.5kg and 20 years Pu'er cooked teas of 2kg, be mixed into 5kg Pu'er tea raw material;
2. use 20kg pure water drip washing tea raw material;
3. with the low temperature drying under 40 ± 5 ℃ of conditions of the tea raw material after the drip washing,, be ground into the end with pulverising mill until twisting into pieces with hand;
4. powder sample is joined in the 50kg pure water, 45 ℃ of isoperibol refluxed lixiviate 15 minutes, leave standstill suction filtration to the room temperature, I must filtrate; Filter residue is joined in 50kg part pure water, and suction filtration to the room temperature is left standstill in boiling reflux lixiviate 10 minutes, filtrate II, merging filtrate I and II obtain the Pu'er cooked tea extract;
5. with the Pu'er cooked tea extract in-0.070 ± 0.01Mpa vacuum, 80 ℃ temperature is concentrated into 1/4 of original volume, obtains about 20kg Pu'er cooked tea concentrated extracting solution.
(2) Dendrobium officinale polysaccharide extracts
1. take by weighing the fresh stem of 1kg dendrobium candidum, dry, low temperature drying under 40 ± 5 ℃ of conditions until twisting into pieces with hand, is ground into the end with pulverising mill;
2. powder sample is joined in the 40kg pure water, boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature, filtrate II I; Filter residue is joined in the 40kg pure water, boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature, the IV that must filtrate, merging filtrate III and IV obtain the dendrobium candidum extract.
3. with the dendrobium candidum extract in-0.070 ± 0.01Mpa vacuum, 80 ℃ temperature is concentrated into 1/10 of original volume, obtains about 7kg dendrobium candidum concentrated extracting solution.
(3) extract is composite
With 4kg Pu'er cooked tea concentrated extract, 1kg dendrobium candidum concentrated extract mixing, obtain tea cream stoste.
(4), melt again and be pressed into the Pu'er tea paste that paste can obtain containing iron sheet stem of noble dendrobium active ingredient with the freeze drying 30 hours under-40 ℃ of conditions of temperature of tea cream stoste.Utilize oven method that resultant tea cream is dried under 105 ± 5 ℃ of temperature, calculate water content, tea cream water content is 10%.
Get 5g embodiment 1 gained tea cream, can be dissolved in rapidly in 90 ℃, the hot water of 300ml, can be dissolved in fully in 1 minute in 50 ℃, the warm water of 300ml.Millet paste soup look red after the dissolving is dense bright; Fragrance Chen Xiang is strong, and persistence is high; It is pure and strong to enter the mouth, and promotes the production of body fluid sense better.
(18～24g) carry out the foundation of diabetic mice model, obtain diabetic mice with normal mouse.It is divided into positive controls (diabetic mice), medicine feed group I (50mg/kg.d at random; The dendrobium candidum concentrated extracting solution), medicine feed group II (50mg/kg.d; The Pu'er cooked tea concentrated extracting solution), medicine feed group III (50mg/kg.d, stem of noble dendrobium Pu'er tea paste), irritating the stomach amount is 0.1ml/10g.d.Blank (normal mouse) and positive controls are all irritated stomach with physiological saline, and irritating the stomach amount is 0.1ml/10g.d, feeds 20d altogether, and every 4d measures a blood glucose value.After feed finishing, mouse takes off cervical vertebra puts to death, and dissects, and gets liver, cleans with ice physiological saline, wipes away driedly, weighs, active with SOD in the kit measurement murine liver tissue.The concrete data of gained are as shown in the table:
Can find out that from table the blood glucose value of diabetic mice all has in various degree decline, and wherein medicine feed group III decline effect is the most obvious; The SOD enzymatic activity increases to some extent in the same murine liver tissue, and promptly it removes the free radical activity ability increases, and antidotal effect is arranged, and finds that equally medicine feed group III effect is best, and therefore, the stem of noble dendrobium Pu'er tea paste that obtains is than the better health care of one-component tool.
Embodiment 2
(1) Pu'er cooked tea extract:
1. take by weighing 10 years Pu'er cooked teas of 5 years Pu'er cooked teas of 1 year Pu'er cooked tea of 0.5kg, 1kg, 1.5kg and 20 years Pu'er cooked teas of 2kg, be mixed into 5kg Pu'er tea raw material;
2. use 25kg pure water drip washing tea raw material;
3. with the low temperature drying under 40 ± 5 ℃ of conditions of the tea raw material after the drip washing,, be ground into the end with pulverising mill until twisting into pieces with hand;
4. powder sample is joined in the 45kg pure water, 45 ℃ of isoperibol refluxed lixiviate 15 minutes, leave standstill suction filtration to the room temperature, I must filtrate; Filter residue is joined in 45kg part pure water, and suction filtration to the room temperature is left standstill in boiling reflux lixiviate 10 minutes, filtrate II, merging filtrate I and II obtain the Pu'er cooked tea extract;
5. with the Pu'er cooked tea extract in-0.070 ± 0.01Mpa vacuum, 70 ℃ temperature is concentrated into 1/4 of original volume, obtains about 18kg Pu'er cooked tea concentrated extracting solution.
(2) Dendrobium officinale polysaccharide extracts
1. take by weighing the fresh stem of 1kg dendrobium candidum, dry, low temperature drying under 40 ± 5 ℃ of conditions until twisting into pieces with hand, is ground into the end with pulverising mill;
2. powder sample is joined in 50kg part pure water, boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature, filtrate II I; Filter residue is joined in 50kg part pure water, boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature, the IV that must filtrate, merging filtrate III and IV obtain the dendrobium candidum extract.
3. with the dendrobium candidum extract in-0.070 ± 0.01Mpa vacuum, 80 ℃ temperature is concentrated into 1/10 of original volume, obtains about 8kg dendrobium candidum concentrated extracting solution.
(3) extract is composite
With 4.5kg Pu'er cooked tea concentrated extract, 0.5kg dendrobium candidum concentrated extract mixing, obtain tea cream stoste.
(4) with the freeze drying 30 hours under-35 ℃ of conditions of temperature of tea cream stoste; Melt again and be pressed into the Pu'er tea paste that paste can obtain containing iron sheet stem of noble dendrobium active ingredient; Utilize oven method that resultant tea cream is dried under 105 ± 5 ℃ of temperature, calculate water content, tea cream water content is 15%.
Get 5g embodiment 2 gained tea cream, can be dissolved in rapidly in 90 ℃ of 300ml hot water, can be dissolved in fully in 50 ℃ of 300ml warm water in 1 minute.Millet paste soup color depth after the dissolving is red, and glow is exquisitely carved; Fragrance Chen Xiang is strong fragrant, and persistence is higher; Inlet promotes the production of body fluid sense better along sliding, pure and mild.
Carry out according to the method in the specific embodiment 1, measure the activity of blood glucose value and SOD, the concrete data of gained are as shown in the table:
Same discovery, the stem of noble dendrobium Pu'er tea paste that obtains is than the better health care of one-component tool.
Embodiment 3
(1) Pu'er cooked tea extract:
1. take by weighing 10 years Pu'er cooked teas of 5 years Pu'er cooked teas of 1 year Pu'er cooked tea of 1kg, 1kg, 1.5kg and 20 years Pu'er cooked teas of 1.5kg, be mixed into 5kg Pu'er tea raw material;
2. use 20kg pure water drip washing tea raw material;
3. with the low temperature drying under 40 ± 5 ℃ of conditions of the tea raw material after the drip washing,, be ground into the end with pulverising mill until twisting into pieces with hand;
4. powder sample is joined in the 65kg pure water, 45 ℃ of isoperibol refluxed lixiviate 15 minutes, leave standstill suction filtration to the room temperature, I must filtrate; Filter residue is joined in 65kg part pure water, and suction filtration to the room temperature is left standstill in boiling reflux lixiviate 10 minutes, filtrate II, merging filtrate I and II obtain the Pu'er cooked tea extract;
5. with the Pu'er cooked tea extract in-0.070 ± 0.01Mpa vacuum, 70 ℃ temperature is concentrated into 1/4 of original volume, obtains about 25kg Pu'er cooked tea concentrated extracting solution.
(2) Dendrobium officinale polysaccharide extracts
1. take by weighing the fresh stem of 1kg dendrobium candidum, dry, low temperature drying under 40 ± 5 ℃ of conditions until twisting into pieces with hand, is ground into the end with pulverising mill;
2. powder sample is joined in the 60kg pure water, boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature, filtrate II I; Filter residue is joined in the 60kg pure water, boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature, the IV that must filtrate, merging filtrate III and IV obtain the dendrobium candidum extract.
3. with the dendrobium candidum extract in-0.070 ± 0.01Mpa vacuum, 80 ℃ temperature is concentrated into 1/10 of original volume, obtains about 10kg dendrobium candidum concentrated extracting solution.
(3) extract is composite
With 8.5kg Pu'er cooked tea concentrated extract and 1.5kg dendrobium candidum concentrated extract mixing, obtain tea cream stoste.
(4) with the freeze drying 20 hours under-30 ℃ of conditions of temperature of tea cream stoste; Melt again and be pressed into the Pu'er tea paste that paste can obtain containing iron sheet stem of noble dendrobium active ingredient; Utilize oven method that resultant tea cream is dried under 105 ± 5 ℃ of temperature, calculate water content, tea cream water content is 20%.
Get 5g embodiment 3 gained tea cream, can be dissolved in rapidly in 90 ℃ of 300ml hot water, can be dissolved in fully in 50 ℃ of 300ml warm water in 1 minute.Millet paste soup look glow after the dissolving is exquisitely carved; Fragrance Chen Xiang is strong, and persistence is high, and fragrance purity is higher; It is pure and mild to enter the mouth, and promotes the production of body fluid and feels.
Carry out according to the method in the specific embodiment 1, measure the activity of blood glucose value and SOD, the concrete data of gained are as shown in the table:
Same discovery, the stem of noble dendrobium Pu'er tea paste that obtains is than the better health care of one-component tool.
Claims (1)
1. the preparation method of a stem of noble dendrobium health-care pu'er tea cream may further comprise the steps:
(1) preparation Pu'er cooked tea extract:
1. take by weighing 10～20 parts of the Pu'er cooked teas in 1 year of ageing by weight, 10 parts～20 parts of the Pu'er cooked teas in 5 years, 30～40 parts of 30～40 parts of the Pu'er cooked teas in 10 years and the Pu'er cooked teas in 20 years of ageing; Mixing is subsequent use;
2. get the Pu'er cooked tea of mixing,, remove and deash with 4～6 times clear water drip washing; Place then under 40 ± 5 ℃ of conditions and dry, subsequent use after pulverizing;
3. the Pu'er cooked tea powder is with 9～13 times pure water, 40～50 ℃ of isoperibol refluxed lixiviate 15 minutes, leaves standstill suction filtration to the room temperature, and I must filtrate; Filter residue is used 9～13 times pure water boiling reflux lixiviate 10 minutes again, leaves standstill suction filtration after the room temperature, filtrate II; Merging filtrate I and II in-0.070 ± 0.01Mpa vacuum, are concentrated into 1/4 of original volume under 70～80 ℃ the temperature, obtain the Pu'er cooked tea concentrated extracting solution;
(2) Dendrobium officinale polysaccharide extracts:
1. the fresh stem with dendrobium candidum dries, and under 40 ± 5 ℃ of conditions, dries, and is subsequent use after pulverizing;
2. get Dendrobium and boiled lixiviate 1 hour, leave standstill suction filtration to the room temperature with 40～60 times pure water, filtrate II I; Filter residue boiled lixiviate 1 hour with 30～40 times pure water again, left standstill suction filtration to the room temperature, and IV must filtrate; Merging filtrate III and IV in-0.070 ± 0.01Mpa vacuum, are concentrated into 1/10 of original volume under 70～80 ℃ the temperature, obtain the dendrobium candidum concentrated extracting solution;
(3) preparation tea cream:
Take by weighing 80～90 parts of Pu'er cooked tea concentrated extracting solutions and 10～20 parts of dendrobium candidum concentrated extracting solutions by weight, mix; In temperature is freeze drying 20～30 hours under-40 ℃～-30 ℃ conditions, after melt and be pressed into paste and promptly obtain required stem of noble dendrobium health-care pu'er tea cream.
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